CN106359567A - Fresh keeping agent containing essential oil, for fruits, and application - Google Patents
Fresh keeping agent containing essential oil, for fruits, and application Download PDFInfo
- Publication number
- CN106359567A CN106359567A CN201610738641.6A CN201610738641A CN106359567A CN 106359567 A CN106359567 A CN 106359567A CN 201610738641 A CN201610738641 A CN 201610738641A CN 106359567 A CN106359567 A CN 106359567A
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- essential oil
- plants essential
- fruit
- antistaling agent
- agent containing
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- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 239000004302 potassium sorbate Substances 0.000 description 1
- 235000010241 potassium sorbate Nutrition 0.000 description 1
- 229940069338 potassium sorbate Drugs 0.000 description 1
- 230000003389 potentiating effect Effects 0.000 description 1
- 108090000765 processed proteins & peptides Proteins 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000005871 repellent Substances 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000006228 supernatant Substances 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 239000004577 thatch Substances 0.000 description 1
- WJCNZQLZVWNLKY-UHFFFAOYSA-N thiabendazole Chemical compound S1C=NC(C=2NC3=CC=CC=C3N=2)=C1 WJCNZQLZVWNLKY-UHFFFAOYSA-N 0.000 description 1
- MGSRCZKZVOBKFT-UHFFFAOYSA-N thymol Natural products CC(C)C1=CC=C(C)C=C1O MGSRCZKZVOBKFT-UHFFFAOYSA-N 0.000 description 1
- 229960000790 thymol Drugs 0.000 description 1
- 125000003639 thymyl group Chemical group C1(=CC(C)=CC=C1C(C)C)* 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 201000008827 tuberculosis Diseases 0.000 description 1
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 description 1
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 description 1
- 235000012141 vanillin Nutrition 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B7/00—Preservation of fruit or vegetables; Chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by group A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by group A23B7/08 or A23B7/10 in the form of liquids or solids
- A23B7/154—Organic compounds; Microorganisms; Enzymes
- A23B7/155—Microorganisms; Enzymes ; Antibiotics
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B7/00—Preservation of fruit or vegetables; Chemical ripening of fruit or vegetables
- A23B7/14—Preserving or ripening with chemicals not covered by group A23B7/08 or A23B7/10
- A23B7/153—Preserving or ripening with chemicals not covered by group A23B7/08 or A23B7/10 in the form of liquids or solids
- A23B7/154—Organic compounds; Microorganisms; Enzymes
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Microbiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a fresh keeping agent containing essential oil, for fruits, and an application. The fresh keeping agent for fruits is characterized by being compounded from lysozyme, tea polyphenols, nisin, essential oil A, essential oil B, Vc and distilled water in a certain proportion. According to the fresh keeping agent for fruits, disclosed by the invention, the essential oil is optimized to be used as a main component of the fresh keeping agent, so that the fresh keeping agent has excellent effects of bacteriostasis and oxidation resistance and is applied to corrosion resistance and fresh keeping of the fruits, the fresh keeping and storage period of the fruits can be greatly prolonged, the fruits are guaranteed to maintain original quality in the fresh keeping period, and the quality of the fruits is effectively guaranteed. The fresh keeping agent for the fruits, disclosed by the invention is simple in compounding method, and convenient to apply; and the fresh keeping agent is completely compounded from natural components, and harmful chemical substances are not added, so that the fresh keeping agent is safe and environmental-friendly, and has an important industrial value.
Description
Technical field
The present invention relates to fruit freshness preserving technical field, specifically a kind of preferred plants essential oil is main as antistaling agent
Composition, can greatly prolong the fresh-retaining preserving phase of fruit, the quality of fruit is effectively ensured, and compound method is simple, and application is convenient,
The fruit antistaling agent containing plants essential oil of safety and environmental protection and application.
Background technology
Fruit can occur physiological disease and fungal disease during storing, and leads to fruit to rot and lose edibility, by
The economic loss that this causes is huge.According to statistics, the fresh fruit having 10%-30% every year in developed country is lost in postharvest decay,
And lacking the developing country of storing refrigerating equipment, its rotten loss amount is then up to 40%-50%.Fresh fruit and vegetable are being adopted
In the process of circulation, the main cause of loss can be summarized as afterwards: physiological (fruit and vegerable own physiological is decayed), (pathogenic microorganism of pathology
Cause rotten), (mechanical damage, ambient temperature and humidity are not suitable for) of physics and the synergism of three.
The fruit disease typically infection in harvesting, transport, falls ill during storage.The physical methods such as low temperature, controlled atmosphere, decompression are normal
It is used for fruit postharvest storage.It was verified that these methods can slow down Fruit physiology aging to a great extent, reduce disease
Occur, reach certain anti-corrosive fresh-keeping effect.However, they can not entirely prevent the invasion and attack to fruit for the microbial pathogens.Newly
In fresh fruit postharvest storage, deterioration is influenced by factors, but by rotting of causing of disease be adopt after in loss
One of key factor.Therefore, for effective loss reducing after fruit harvesting, using physical measure fiting chemicals such as low temperature more than people
Pesticide is preventing and treating postharvest diseases of fruit.However, life-time service chemical agent can lead to pathogenic bacteria to develop immunity to drugs, more seriously,
The high concentration chemical agent frequently using in production causes persticide residue increase on fruit can threaten human health.It is reported that,
Presently used pesticide about 60% has carcinogenic danger.Thus the fruit antistaling agent of exploitation safety non-toxic and efficient stable is increasingly
By universal the paying close attention to of people, and it is increasingly becoming one of current scientific research focus.
Fruit antistaling agent can be divided into two big class, i.e. chemosynthesis and crude antistaling agent.For a long time, people utilize variousization
Learn synthetic, fruit is carried out with the research of fresh-retaining preserving and applies achieved with significant preservation and antisepsis effect.Universal at present
Use chemical preservative, such as TBZ, carbendazim, benzene Lai Te, chlorine, sulfur dioxide etc., although these chemical substance energy
Enough kill pathogen, reach the purpose of anti-corrosive fresh-keeping, the fresh-retaining preserving effect is significant to fruit, but life-time service chemical preservation
Agent, can damage health, pollution environment, so that pathogen is developed immunity to drugs.But, with scientific and technical development, the people
Growth in the living standard, and the enhancing of global environmental consciousness, replace chemosynthesis antistaling agent with the antistaling agent of natural origin
Exploitation is increasingly subject to people's attention with research.
Plants essential oil be extraction the distinctive aromatic substance of plant, be taken from herbal flower, leaf, root, bark, fruit,
Seed, resin etc. are to distill, squeezing mode extract.Each plants essential oil has a chemical constitution to determine its
Fragrance, color, mobility and its mode with System Operation, also make each plants essential oil respectively have a set of special function special
Matter.In recent years, research shows both at home and abroad, and plants essential oil removes has physiological action to human body, also has the speciality of natural anticorrosion.One
Aspect can suppress or kill pathogen, on the other hand can to animals and plants produce chemical effect, thus animal is played tag,
Repellent and stifling effect, play suppression or the action effect of poisoning to pathogenic microorganism.Plants essential oil can with antifungal and
Antibacterial, improves the immunity of Human Physiology system, promotes human metabolism.Research finds that plants essential oil also has and insect is smoked
The double activity steaming and tagging, insect smells the aromatic odor of plants essential oil, will escape.
Research finds, the bacteriostatic activity of plants essential oil has broad spectrum activity, and same plants essential oil can be simultaneously to multiple diseases
Pathogenic microorganism works, but plants essential oil has selectivity to the inhibitory action of plant pathogenic microorganisms again, different types of
The rejection ability of the pathogenic microorganism to different cultivars for the plants essential oil is different.Have mutually collaborative, no between different plants essential oils
Can react between the composition of quintessence oil, be used in combination and can improve its function.
Content of the invention
The purpose of the present invention is the defect existing for prior art, provides a kind of fruit antistaling agent containing plants essential oil
And application, the preferred plants essential oil of this fruit antistaling agent, as antistaling agent main component, has excellent antibacterial and antioxygen and is turned into
With being applied to the anti-corrosive fresh-keeping of fruit, the fresh-retaining preserving phase of fruit can be greatly prolonged it is ensured that fruit keeps original in freshness date
Quality, thus be effectively guaranteed the quality of fruit；The fruit freshness preserving agent compounding method of the present invention is simple, and application is convenient, completely
Prepared using natural constituents, without harmful chemical, safety and environmental protection, there is important industrial value.
The purpose of the present invention solves by the following technical programs:
A kind of fruit antistaling agent containing plants essential oil it is characterised in that: this fruit antistaling agent is as follows by parts by weight
Group is grouped into: lysozyme 0.2-0.3 part, tea polyphenols 1.0-1.5 part, nisin 0.3-0.4 part, plants essential oil a 13-
15 parts, plants essential oil b 6-8 part, vc 3-4 part, 1000 parts of distilled water.
The raw material of described plants essential oil a preparation and its proportioning are: Australia tea tree leaf 7-8 part, Cortex Cinnamomi 5-6 part, Herba Rosmarini Officinalis
4-5 part, Herba Cymbopogonis Citrari 2-3 part, Herba thymi vulgariss 3-4 part.
The raw material of described plants essential oil b preparation and its proportioning are: Pericarpium Zanthoxyli 5-6 part, Flos Caryophylli 4-5 part, Herba Menthae 3-4 part, brocade
Pericarpium Citri junoriss 1-2 part.
Described plants essential oil a adopts steam distillation to prepare, and concrete technology flow process is: plants essential oil a raw material is shone
Dry, pulverize, then with 30 mesh sub-sieve filtering and impurity removings, weigh the raw material of certain mass, according to solid-liquid ratio 1:10(w:v) add
Distilled water, 180 DEG C of heated at constant temperature boilings, quintessence oil starts to ooze timing, after 2 hours, terminates distillation, stands 15 minutes, treat profit
After separating, liquid is crude oil at the middle and upper levels to take oil water separator, obtains anhydrous plant quintessence oil a with anhydrous sodium sulfate dehydration.
Described plants essential oil b adopts carbon dioxide supercritical extraction method to prepare, and concrete technology flow process is: by plants essential oil b
Raw material dries in the shade to constant weight, pulverizes, then with 30 mesh sub-sieve filtering and impurity removings, with supercritical extraction instrument supercritical co2Extraction, extraction
Pressure power is controlled to 15-16mpa, and extraction temperature is controlled to 31-33 DEG C, and extraction time is controlled to 2.5-3h, and knockout tower discharging obtains
To plants essential oil b.
The described fruit antistaling agent containing plants essential oil first takes the distilled water of proportional quantity when using, and then sequentially adds and joins
The tea polyphenols of proportion, lysozyme, vc, nisin, plants essential oil a, plants essential oil b, stir and dissolve.
Application in fruit antisepsis are fresh-keeping for the described fruit antistaling agent containing plants essential oil.
Described application is to put fruits in the fruit antistaling agent containing plants essential oil, takes out after soaking 3-5min.
The present invention has the following advantages compared to existing technology:
The fruit antistaling agent containing plants essential oil of the present invention, preferably lysozyme, tea polyphenols, nisin and vc conduct
Active component.Wherein lysozyme is a kind of hydrolytic enzyme being acting exclusively on microorganism wall, and it exclusively acts on peptide polysaccharide
In molecule, the β between n- acetylmuramic acid and n- acetylglucosamine-Isosorbide-5-Nitrae key, thus destroying the cell wall of antibacterial, finally makes
Bacterolysises death is it is also possible to directly destroy the cell wall of gram positive bacteria, and reaches the effect of sterilization；Tea polyphenols have relatively
Staphylococcuses, escherichia coli, bacillus subtilis etc. are had strong inhibitory action by strong antioxidation and bacteriostasis, also
There is deodorization, protection pigment, the effect of the formation of suppression nitrite；Nisin can suppress most of Gram-positives
Bacterium, and have strong inhibitory action to the spore of bacillus cereuss, nisin eat after human body physiology ph condition and
It is hydrolyzed into aminoacid quickly under alpha -chymotrypsin effect, normal flora and generation such as other in human body intestinal canal will not be changed
, more will not cross tolerance with other antibiotics in the resistance problem that antibiotics occur, have efficient, nontoxic, safe, no secondary
The advantage of effect；Vc is a kind of efficient antioxidant, can prevent fruit oxidation, suppression free radical from producing, can also work in coordination with it
The activity of its antistaling agent composition.
The present invention adopts plants essential oil as antistaling agent main component, preferably Australia tea tree leaf, Cortex Cinnamomi, Herba Rosmarini Officinalis, perfume (or spice)
Thatch, Herba thymi vulgariss, Pericarpium Zanthoxyli, Flos Caryophylli, Herba Menthae, brocade orange skin are as extraction of essential oil raw material.Australia tea tree essential oil be rich in ethylene, dipentene,
Limonene, cineol, Oleum sesami brain and anisoxide isoreactivity material, are potent antibacterial, kill mycete and have better effect, and
There are the armaticity of uniqueness；Cinnamon essential oil is the supernatant liquid of yellow or yellowish-brown, and its main component is cinnamic aldehyde, and content is about
75%-90%, separately contains a small amount of methyleugenol, cinnamic alcohol, cinnamyl acetate, vanillin, coumarin, cinnamic acid, eugenol, 2- methoxyl group
Cinnamic acid, 2- 2-Methoxyacetic acid osmanthus ester and dioxy cinnamic acid etc., cinnamon essential oil compares the suppression of antibacterial to the inhibition of pathogenic fungi
Effect is good, and bacteriostasis are even more preferable than conventional chemical bactericide；Rosemary ethereal oil be rich in australene, Camphora, pinanone,
Borneol acetate, lauro lene, nopinene, linalool isoreactivity material, have good suppression effect to antibacterial, original place microorganism；
The main component of oil of Cymbopogon winterianus is Chinese catalpa lemon aldehyde, and Chinese catalpa lemon aldehyde has the biocidal property of wide spectrum, to candidiasises, trichophyton, aspergillosiss, golden yellow
The funguses such as color staphylococcuses, gonococcuss and escherichia coli and antibacterial all have suppression and the dual function killed；Thyme oil
Main component is thymol, linalool, fragrant chaste tree nationality phenol, Borneolum Syntheticum, linalool, nopinene and Flos Caryophylli hydrocarbon, has powerful antibacterial
And antioxidant activity, it is one of antibacterial the strongest, husky to staphylococcus aureuses, bacillus subtilises, escherichia coli, enteritis
Door Salmonella, Listeria monocytogenes, the suppression such as aspergillus parasiticus bacterium and kill effect it is further preferred that；Japan pepper essential oil is by polytype compound
The mixture of composition, its chemical composition is mainly by terpene compound, aromatic compound, aliphatic compound and nitrogenous sulfur-bearing
Compound 4 big class forms, and can not only suppress gram negative bacteria, also can suppress gram positive bacteria, simultaneously to mycete, funguses
There is inhibitory action, also there is preferable antioxidation and pesticide and miticide actility；Clove oil is rich in eugenol, acetyl Oleum Caryophylli
Phenol, β-Dianthus chinensis dilute isoreactivity material, have excellent antibacterium and antifungic action, especially oidium schoenleinii, white are read
The suppression effect of the bacillus such as the pathogenic funguses such as pearl bacterium, staphylococcus aureuses and pneumonia, dysentery will Hayes, large intestine, deformation, tuberculosis
Fruit it is further preferred that, also very excellent to the inhibition of the funguses such as star-shaped nocardia, trichophyton schoenleini, microsporon gypseum, also have
Anthelmintic action；Main component in Peppermint essential oil is isophorone, β-caryophyllene, spathulenol, nopinene and eucalyptole etc., to withered
The gram positive bacteria such as careless bacillus cereuss and staphylococcus aureuses has excellent suppression effect, but the suppression to gram negative bacteria
Effect on driving birds is not good processed；The main component of brocade orange quintessence oil is limonene, has very strong biocidal property, the antibacterial work to gram positive bacteria
Bacteriostasis with gram negative bacteria to be compared are strong.Generally a kind of plants essential oil can act as to multiple pathogenic microorganisms simultaneously
With, but plants essential oil has selectivity to the inhibitory action of plant pathogenic microorganisms again, and different types of plants essential oil is not to
Rejection ability with the pathogenic microorganism of kind is different.And have mutually collaborative between different plants essential oils, different quintessence oils
Can react between composition, be used in combination and can improve its function, and the fruit freshness preserving containing plants essential oil of the present invention
Agent can also give fresh-keeping fruit with pleasant fragrance.
To Australia tea tree leaf, Cortex Cinnamomi, Herba Rosmarini Officinalis, Herba Cymbopogonis Citrari, Herba thymi vulgariss, Pericarpium Zanthoxyli, Flos Caryophylli, Herba Menthae, brocade orange skin be raw material system
Standby plants essential oil, has been respectively adopted steam distillation and carbon dioxide supercritical extraction method, steam distillation has equipment
Simply, easily operation, low cost, environmentally friendly the advantages of, but preparation process raw material is placed in high temperature, if quintessence oil active matter
Matter non-refractory, can affect essential oil product quality.Carbon dioxide supercritical extraction method extracting power is strong, high income, the production cycle
The advantage that short effective ingredient is not destroyed, operating parameter is easily controlled, but equipment and cost are high compared with steam distillation.Our roots
Factually border Production requirement, to Australia tea tree, Cortex Cinnamomi, Herba Rosmarini Officinalis, Herba Cymbopogonis Citrari, thyme oil extraction adopt steam distillation,
Pericarpium Zanthoxyli, Flos Caryophylli, Herba Menthae, the extraction of brocade orange quintessence oil adopt carbon dioxide supercritical extraction method, and classification extraction have been directed to different quintessence oils
The difference that active component is constituted, separates the plants essential oil obtaining high-quality activity.
Generally certain fruit antistaling agent is typically only used for the anti-corrosive fresh-keeping of one or more fruit, has certain use
Limitation, but the fruit antistaling agent of the present invention by extract Australia tea tree, Cortex Cinnamomi, Herba Rosmarini Officinalis, Herba Cymbopogonis Citrari, Herba thymi vulgariss, Pericarpium Zanthoxyli, fourth
Perfume, Herba Menthae, brocade orange peel essential oil and lysozyme, tea polyphenols, nisin, vc and potassium sorbate are compounded, and greatly improve
Antimicrobial spectrum, can be widely applied to greatly prolong the fresh-retaining preserving of fruit in the anti-corrosive fresh-keeping of almost all kinds fruit
Phase is it is ensured that fruit keeps original quality in freshness date, thus being effectively guaranteed the quality of fruit.
Specific embodiment
With reference to embodiment, the present invention is further illustrated.
A kind of fruit antistaling agent containing plants essential oil it is characterised in that: this fruit antistaling agent is by parts by weight
Following group is grouped into: lysozyme 0.2-0.3 part, tea polyphenols 1.0-1.5 part, nisin 0.3-0.4 part, plants essential oil a
13-15 part, plants essential oil b 6-8 part, vc 3-4 part, 1000 parts of distilled water；
Plants essential oil a preparation method is: will form and proportioning is respectively Australia tea tree leaf 7-8 part, Cortex Cinnamomi 5-6 part, Herba Rosmarini Officinalis 4-5
Part, Herba Cymbopogonis Citrari 2-3 part, the plants essential oil of Herba thymi vulgariss 3-4 part are prepared raw material and are dried, and pulverize, are then crossed with 30 mesh sub-sieves and filter
Miscellaneous, weigh the raw material of certain mass, according to solid-liquid ratio 1:10(w:v) add distilled water, 180 DEG C of heated at constant temperature boilings, quintessence oil
Start to ooze timing, after 2 hours, terminate distillation, stand 15 minutes, after oil-water separation, take oil water separator liquid at the middle and upper levels
I.e. crude oil, obtains anhydrous plant quintessence oil a with anhydrous sodium sulfate dehydration；
Plants essential oil b preparation method is: will form and proportioning is respectively Pericarpium Zanthoxyli 5-6 part, Flos Caryophylli 4-5 part, Herba Menthae 3-4 part, brocade orange
The plants essential oil of skin 1-2 part is prepared raw material and is dried in the shade to constant weight, pulverizes, then with 30 mesh sub-sieve filtering and impurity removings, uses supercritical
Abstraction instrument supercritical co2Extraction, extracting pressure is controlled to 15-16mpa, and extraction temperature is controlled to 31-33 DEG C, and extraction time controls
For 2.5-3h, knockout tower discharging obtains plants essential oil b；
The compound method of the fruit antistaling agent of the present invention is: first takes the distilled water of proportional quantity during use, then sequentially adds proportioning
The tea polyphenols of amount, lysozyme, vc, nisin, plants essential oil a, plants essential oil b, stir and dissolve；
The using method of the fruit antistaling agent of the present invention: put fruits in the fruit antistaling agent containing plants essential oil, soak 3-
Take out after 5min in the anti-corrosive fresh-keeping that can be applicable to fruit.
The preferred plants essential oil of the fruit antistaling agent of the present invention as antistaling agent main component, has excellent antibacterial and anti-
Oxidation, is applied to the anti-corrosive fresh-keeping of fruit, can greatly prolong the fresh-retaining preserving phase of fruit it is ensured that fruit is protected in freshness date
Hold original quality, thus being effectively guaranteed the quality of fruit；The fruit freshness preserving agent compounding method of the present invention is simple, application side
Just, adopt natural constituents to prepare completely, without harmful chemical, safety and environmental protection, there is important industrial value.
Embodiment
In July, 2015, our fresh from market purchasing, no disease and pests harm, kyoto grapes of uniform size and pears are as guarantor
Fresh test material, carries out fresh-keeping test using the fruit antistaling agent containing plants essential oil for the present invention, simultaneously from technical literature
Find other two kinds of fruit antistaling agents and carry out contrast test, and one group of distilled water group is set as blank.Other two kinds
Fruit antistaling agent component is as follows:
Suppression miaow cream antistaling agent: (documents derive from Liu Haoqiang etc., and " different antistaling agents mix 333.3 g/l suppression miaow cream
Pairing brocade orange adopts toxicity and its storage effect of rear pathogenic bacteria ")；
Sorbic acid and calcium propionate antistaling agent: sorbic acid 0.039%+ calcium propionate 0.131%(documents derive from the " Pyrusussuriensiss such as Tan Zhen
Acid and calcium propionate composite preservative are to the research extending the apple fresh-keeping phase ").
Soak kyoto grape and pears 3-5min respectively with three kinds of antistaling agent solution and distilled water, dry, be then charged into poly- second
Alkene plastics bag is wrapped, is respectively put in carton, is placed in 25 ± 2 DEG C of room temperatures, air humidity is storage under conditions of 85%-90%, often
Every vc content, the rotting rate of the vc content, healthy fruit and pears of 1 month sampling and measuring kyoto grape, successive survey 3 months, result
Following Tables 1 and 2.
From Tables 1 and 2 it is found that the vc content of the kyoto grape of fruit antistaling agent Preservation Treatment of the present invention and healthy fruit exist
In 3 months not only all be significantly larger than same period distilled water matched group, also significantly greater than the same period suppression miaow cream antistaling agent treatment group and
Sorbic acid and calcium propionate antistaling agent treatment group；The vc content of the pears of fruit antistaling agent Preservation Treatment of the present invention is also above the same period
Suppression miaow cream antistaling agent treatment group and sorbic acid and calcium propionate antistaling agent treatment group, Decayed rate is below same period suppression miaow cream
Antistaling agent treatment group and sorbic acid and calcium propionate antistaling agent treatment group.It can therefore be seen that the present invention containing plants essential oil
Fresh-keeping, the antiseptic effect of fruit antistaling agent will be considerably better than suppression miaow cream antistaling agent, sorbic acid and calcium propionate antistaling agent.
Substantial amounts of pilot production finds that the fruit antistaling agent of the present invention has excellent antibacterial and antioxidation, is applied to
The anti-corrosive fresh-keeping of fruit, can greatly prolong the fresh-retaining preserving phase of fruit it is ensured that fruit keeps original quality in freshness date, thus
It is effectively guaranteed the quality of fruit；The fruit freshness preserving agent compounding method of the present invention is simple, and application is convenient, adopts natural group completely
Assignment system, without harmful chemical, safety and environmental protection, has important industrial value.
Above example technological thought only to illustrate the invention is it is impossible to limit protection scope of the present invention with this, every
According to technological thought proposed by the present invention, any change done on the basis of technical scheme, each fall within the scope of the present invention
Within；The technology that the present invention is not directed to all can be realized by prior art.
Claims (8)
1. a kind of fruit antistaling agent containing plants essential oil it is characterised in that: this fruit antistaling agent be by parts by weight as
The following group is grouped into: lysozyme 0.2-0.3 part, tea polyphenols 1.0-1.5 part, nisin 0.3-0.4 part, plants essential oil a
13-15 part, plants essential oil b 6-8 part, vc 3-4 part, 1000 parts of distilled water.
2. the fruit antistaling agent containing plants essential oil according to claim 1 it is characterised in that: described plants essential oil a system
Standby raw material and its proportioning are: Australia tea tree leaf 7-8 part, Cortex Cinnamomi 5-6 part, Herba Rosmarini Officinalis 4-5 part, Herba Cymbopogonis Citrari 2-3 part, Herba thymi vulgariss 3-
4 parts.
3. the fruit antistaling agent containing plants essential oil according to claim 1 it is characterised in that: described plants essential oil b system
Standby raw material and its proportioning are: Pericarpium Zanthoxyli 5-6 part, Flos Caryophylli 4-5 part, Herba Menthae 3-4 part, brocade orange skin 1-2 part.
4. the fruit antistaling agent containing plants essential oil according to claim 1 and 2 it is characterised in that: described plants essential oil a
Using steam distillation preparation, concrete technology flow process is: plants essential oil a raw material is dried, pulverizes, then divide sample with 30 mesh
Sieve filtering and impurity removing, weighs the raw material of certain mass, according to solid-liquid ratio 1:10(w:v) add distilled water, 180 DEG C of heated at constant temperature boilings
Rise, quintessence oil starts to ooze timing, after 2 hours, terminate distillation, stand 15 minutes, after oil-water separation, take in oil water separator
Layer liquid is crude oil, obtains anhydrous plant quintessence oil a with anhydrous sodium sulfate dehydration.
5. the fruit antistaling agent containing plants essential oil according to claim 1 and 2 it is characterised in that: described plants essential oil b
Using carbon dioxide supercritical extraction method preparation, concrete technology flow process is: plants essential oil b raw material is dried in the shade to constant weight, pulverizes,
Then with 30 mesh sub-sieve filtering and impurity removings, with supercritical extraction instrument supercritical co2Extraction, extracting pressure is controlled to 15-16mpa,
Extraction temperature is controlled to 31-33 DEG C, and extraction time is controlled to 2.5-3h, and knockout tower discharging obtains plants essential oil b.
6. the fruit antistaling agent containing plants essential oil according to claim 1 it is characterised in that: described contain plants essential oil
Fruit antistaling agent first take the distilled water of proportional quantity when using, then sequentially add the tea polyphenols of proportional quantity, lysozyme, vc,
Nisin, plants essential oil a, plants essential oil b, stir and dissolve.
7. application in fruit antisepsis are fresh-keeping for the fruit antistaling agent containing plants essential oil according to claim 1.
8. the fruit antistaling agent containing plants essential oil according to claim 7 it is characterised in that: described application is by fruit
Put in the fruit antistaling agent containing plants essential oil, take out after soaking 3-5min.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610738641.6A CN106359567A (en) | 2016-08-29 | 2016-08-29 | Fresh keeping agent containing essential oil, for fruits, and application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610738641.6A CN106359567A (en) | 2016-08-29 | 2016-08-29 | Fresh keeping agent containing essential oil, for fruits, and application |
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| Publication Number | Publication Date |
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| CN106359567A true CN106359567A (en) | 2017-02-01 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106819094A (en) * | 2017-04-09 | 2017-06-13 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN106942355A (en) * | 2017-04-09 | 2017-07-14 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107027877A (en) * | 2017-04-09 | 2017-08-11 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107079724A (en) * | 2017-05-04 | 2017-08-22 | 宁波大学 | Sprinkling antistaling agent and its spray method before a kind of greenhouse strawberry is adopted |
| CN107079984A (en) * | 2017-04-09 | 2017-08-22 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107079983A (en) * | 2017-04-09 | 2017-08-22 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107410463A (en) * | 2017-04-09 | 2017-12-01 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107494712A (en) * | 2017-09-25 | 2017-12-22 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of longan seed essential oil fresh applied to banana and preparation method thereof |
| CN108991104A (en) * | 2018-07-10 | 2018-12-14 | 湖州燕子果业有限公司 | A kind of fruit freshness preserving expelling parasite spray and its production technology |
| CN109043290A (en) * | 2018-09-07 | 2018-12-21 | 中国海洋大学 | A kind of synergist and its application method of biological food antiseptic |
| CN109393014A (en) * | 2018-12-05 | 2019-03-01 | 海南省林业科学研究所 | A kind of plant source mango preservative |
| CN111449132A (en) * | 2020-03-18 | 2020-07-28 | 浙江冒个泡电子商务有限公司 | Fresh-keeping method in fruit transportation process |
| CN111607462A (en) * | 2020-06-04 | 2020-09-01 | 长沙学院 | A kind of compound essential oil and its preparation method and application |
| CN111972492A (en) * | 2020-07-31 | 2020-11-24 | 贵州石阡佛顶山野生油茶油业有限公司 | Preservative for prolonging storage period of oil tea fruits and preparation method thereof |
| CN113416608A (en) * | 2021-06-29 | 2021-09-21 | 中国热带农业科学院热带作物品种资源研究所 | Extraction method of intelligence-developing essential oil for inhibiting listeria monocytogenes and intelligence-developing essential oil |
| CN115281300A (en) * | 2022-08-09 | 2022-11-04 | 苏州市农业科学院 | Compound bacteriostatic method for fresh-keeping and storage of gastrodia elata |
| CN115886176A (en) * | 2022-12-07 | 2023-04-04 | 湖北艾艾贴健康科技有限公司 | A kind of compound wormwood essential oil natural preservative and preparation method thereof |
| CN118160776A (en) * | 2024-05-14 | 2024-06-11 | 西南林业大学 | A kind of fruit long-acting preservative and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1374003A (en) * | 2002-03-27 | 2002-10-16 | 上海宇盛科技有限公司 | Biological fruit and vegetable preservative |
| CN102188034A (en) * | 2010-03-03 | 2011-09-21 | 天津科技大学 | Compound biological antiseptic and preservation agent for food |
| CN103571613A (en) * | 2012-08-06 | 2014-02-12 | 湖北大自然农业实业有限公司 | Preparation method of vitex negundo linn volatile oil |
| CN103689060A (en) * | 2013-12-04 | 2014-04-02 | 佛山市新战略知识产权文化有限公司 | Chinese herbal medicine preservative |
| CN104082830A (en) * | 2014-06-11 | 2014-10-08 | 南通昊友食品添加剂有限公司 | Composite biological antiseptic antistaling agent |
-
2016
- 2016-08-29 CN CN201610738641.6A patent/CN106359567A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1374003A (en) * | 2002-03-27 | 2002-10-16 | 上海宇盛科技有限公司 | Biological fruit and vegetable preservative |
| CN102188034A (en) * | 2010-03-03 | 2011-09-21 | 天津科技大学 | Compound biological antiseptic and preservation agent for food |
| CN103571613A (en) * | 2012-08-06 | 2014-02-12 | 湖北大自然农业实业有限公司 | Preparation method of vitex negundo linn volatile oil |
| CN103689060A (en) * | 2013-12-04 | 2014-04-02 | 佛山市新战略知识产权文化有限公司 | Chinese herbal medicine preservative |
| CN104082830A (en) * | 2014-06-11 | 2014-10-08 | 南通昊友食品添加剂有限公司 | Composite biological antiseptic antistaling agent |
Non-Patent Citations (3)
| Title |
|---|
| 朱德明 等: "互叶白千层油保鲜剂研制与试验", 《农产品加工(学刊)》 * |
| 杜传来 等: "天然果蔬保鲜剂的研究与应用", 《食品工业科技》 * |
| 王后生 等: "天然药用果蔬保鲜剂的研究进展", 《科技视界》 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106819094A (en) * | 2017-04-09 | 2017-06-13 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN106942355A (en) * | 2017-04-09 | 2017-07-14 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107027877A (en) * | 2017-04-09 | 2017-08-11 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107079984A (en) * | 2017-04-09 | 2017-08-22 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107079983A (en) * | 2017-04-09 | 2017-08-22 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107410463A (en) * | 2017-04-09 | 2017-12-01 | 湖南易科生物工程有限公司 | A kind of compound method of fruit vegetables antistaling agent |
| CN107079724A (en) * | 2017-05-04 | 2017-08-22 | 宁波大学 | Sprinkling antistaling agent and its spray method before a kind of greenhouse strawberry is adopted |
| CN107494712A (en) * | 2017-09-25 | 2017-12-22 | 广西壮族自治区农业科学院农产品加工研究所 | A kind of longan seed essential oil fresh applied to banana and preparation method thereof |
| CN108991104A (en) * | 2018-07-10 | 2018-12-14 | 湖州燕子果业有限公司 | A kind of fruit freshness preserving expelling parasite spray and its production technology |
| CN109043290A (en) * | 2018-09-07 | 2018-12-21 | 中国海洋大学 | A kind of synergist and its application method of biological food antiseptic |
| CN109043290B (en) * | 2018-09-07 | 2021-12-28 | 中国海洋大学 | Synergist for food biological preservative and using method thereof |
| CN109393014A (en) * | 2018-12-05 | 2019-03-01 | 海南省林业科学研究所 | A kind of plant source mango preservative |
| CN111449132A (en) * | 2020-03-18 | 2020-07-28 | 浙江冒个泡电子商务有限公司 | Fresh-keeping method in fruit transportation process |
| CN111607462A (en) * | 2020-06-04 | 2020-09-01 | 长沙学院 | A kind of compound essential oil and its preparation method and application |
| CN111972492A (en) * | 2020-07-31 | 2020-11-24 | 贵州石阡佛顶山野生油茶油业有限公司 | Preservative for prolonging storage period of oil tea fruits and preparation method thereof |
| CN113416608A (en) * | 2021-06-29 | 2021-09-21 | 中国热带农业科学院热带作物品种资源研究所 | Extraction method of intelligence-developing essential oil for inhibiting listeria monocytogenes and intelligence-developing essential oil |
| CN115281300A (en) * | 2022-08-09 | 2022-11-04 | 苏州市农业科学院 | Compound bacteriostatic method for fresh-keeping and storage of gastrodia elata |
| CN115886176A (en) * | 2022-12-07 | 2023-04-04 | 湖北艾艾贴健康科技有限公司 | A kind of compound wormwood essential oil natural preservative and preparation method thereof |
| CN118160776A (en) * | 2024-05-14 | 2024-06-11 | 西南林业大学 | A kind of fruit long-acting preservative and preparation method thereof |
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