CN106074200A - A kind of biodiesel extracts natural astaxanthin and the formula of facial film thereof and preparation method - Google Patents

Abstract

A formula and preparation method for extracting natural astaxanthin from functional oils and its facial mask. The present invention relates to the technical field of making beauty care products. The present invention provides a facial mask containing natural astaxanthin, a natural astaxanthin facial mask The formula is: glycerin 2‑3%, sodium lactate 0.8‑2%, butanediol 1‑3%, acrylic acid (or ester)/C10‑30 alcohol acrylate crosslinked polymer potassium salt 0.2‑0.7%, trehalose 0.2‑1%, sodium hyaluronate 0.01‑0.2%, phenoxyethanol 0.1‑0.3%, EDTA disodium salt 0.01‑0.03%g, natural oil astaxanthin extract 5‑10%, deionized water 81‑90 %. Compared with the prior art, the present invention has stronger anti-oxidation, whitening and anti-aging effects, and can avoid stains, wrinkles and the like caused by cells being oxidized.

Description

A kind of formula and preparation method of extracting natural astaxanthin from functional oil and its mask

technical field

The invention relates to the technical field of making beauty care products, in particular to the extraction of natural astaxanthin and a facial mask of functional oil and a preparation method thereof.

Background technique

Reactive oxygen species are the by-products of the human body's aerobic metabolism, including oxygen ions, peroxides and oxygen free radicals. Reactive oxygen species are active in nature, have strong chemical reactivity, and participate in various physiological and biochemical processes in vivo. However, too much active oxygen will have serious side effects, leading to the destruction of normal cells and tissues of the human body, and causing various diseases. Reactive oxygen species will increase under the influence of environment and time. For example, smoking, air pollution, water pollution, radiation (x-rays, ultraviolet rays), pesticides, high life pressure, excessive exercise, etc., will increase the concentration of free radicals, which is called oxidative stress. The greater the oxidative stress, the higher the concentration of free radicals in the body. Studies have shown that anti-oxidation is an important step in preventing aging. If excessive oxidative free radicals can be eliminated, many free radical-induced and aging-related diseases can be prevented.

Antioxidants can capture and neutralize active oxygen, thereby eliminating the damage of active oxygen to the human body, preventing aging of cells, and delaying the rate of body degradation. Natural astaxanthin has a strong antioxidant effect, can effectively remove active oxygen in cells, enhance cell regeneration, maintain body balance and reduce the accumulation of aging cells, thereby protecting skin health, promoting hair growth, anti-aging, and alleviating exercise Fatigue, enhanced vitality. Studies have shown that the antioxidant activity of natural astaxanthin is 6,000 times that of vitamin C, 1,000 times that of vitamin E, 800 times that of coenzyme Q10, 700 times that of anthocyanins, and 100 times that of β-carotene. More importantly, natural astaxanthin is the only carotenoid that can pass through the blood-brain barrier, and has important applications in many fields.

Animals cannot synthesize astaxanthin themselves, and can only ingest it from the outside world through the food chain. Microalgae and yeast can synthesize astaxanthin in nature, and only astaxanthin synthesized by microalgae is 100% L-handed and has stronger biological activity. The absorption peak of astaxanthin is about 470nm, which is similar to the wavelength of ultraviolet rays. Therefore, a small amount of astaxanthin can absorb a large amount of UVA, which can effectively prevent ultraviolet radiation, quench free radicals caused by ultraviolet rays, and reduce the damage of ultraviolet rays to the skin. damage prevention. In addition, it can also quickly restore skin damaged by UV burns. Due to its strong antioxidant properties, many cosmetic brands around the world have added natural astaxanthin as their super antioxidant ingredients, including Estee Lauder, DermaE, Kose, Fang Kai and Mentholatum, etc. have launched special astaxanthin muscle research series moisturizing cream , anti-wrinkle eye cream, lipstick, etc.

So far, many astaxanthin components have been used in cosmetics, but the research and application of natural astaxanthin in China has just started, and the application of natural astaxanthin in the cosmetics industry is still very small.

Contents of the invention

The purpose of the present invention is to develop a facial mask containing natural astaxanthin, which has stronger anti-oxidation, whitening and anti-aging effects, and avoids stains and wrinkles caused by oxidized cells.

The purpose of the present invention can be achieved through the following technical solutions, a method for extracting natural astaxanthin from functional oils, the method comprising: food-grade Haematococcus pluvialis dry powder or food-grade Phaffia rhodozyme powder or astaxanthin rich in astaxanthin Add functional oil to the dry bacterial cells of prime bacteria at a ratio of 1:10-1:2. Under the conditions of anaerobic temperature of 5-15 degrees Celsius and pressure of 35Mpa-45Mpa, high-pressure homogenization for 3-5 times, Every 10-30 minutes, you can get the natural oil astaxanthin extract.

The functional oil is one or more of olive oil, camellia oil, deep-sea fish oil, and safflower oil.

The formula of a kind of natural astaxanthin facial film is, when its facial film is liquid state, its contained component weight percent is: glycerin 2-3%, sodium lactate 0.8-2%, butylene glycol 1-3%, acrylic acid (or ester) Class/C10-30 Alcohol Acrylate Crosslinked Polymer Potassium Salt 0.2-0.7%, Trehalose 0.2-1%, Sodium Hyaluronate 0.01-0.2%, Phenoxyethanol 0.1-0.3%, EDTA Disodium Salt 0.01-0.03 %g, natural oil astaxanthin extract 5-10%, deionized water 81-90%.

A kind of preparation method of natural astaxanthin facial film, when its facial film is liquid state, concrete step is played as:

(1), mix acrylic acid (ester) type/C10-30 alcohol acrylate crosslinked polymer potassium salt, glycerin, EDTA disodium salt, butylene glycol and deionized water according to the ratio in the formula of natural astaxanthin facial mask, Stir until completely dispersed, fully swell for 12 hours, heat to 80 degrees Celsius, and keep warm for 20-30 minutes;

(2), when it is cooled to 50 degrees Celsius, add sodium lactate, trehalose, sodium hyaluronate and phenoxyethanol in the formula amount, stir and mix thoroughly, place in vacuum, and wait for it to cool to 5-10 degrees Celsius;

(3), when cooling to 5-10 degrees Celsius, add natural oil astaxanthin extract, and stir evenly under vacuum;

(4), take a small amount of samples, check according to the QB/T2872 standard, after passing the test, filter at 300 mesh under nitrogen protection, vacuum pack in opaque containers, and obtain liquid natural astaxanthin facial mask.

In the preparation method of the natural astaxanthin facial mask, the liquid natural astaxanthin facial mask can be evenly coated on the mask substrate.

In the preparation method of the natural astaxanthin facial mask, the substrate of the facial mask is one of non-woven fabric, silk or biological fiber.

Compared with the prior art, the present invention has stronger anti-oxidation, whitening and anti-aging effects, and can avoid stains, wrinkles and the like caused by cells being oxidized.

specific implementation plan

A facial mask containing natural astaxanthin and functional oil according to the present invention, the natural astaxanthin mainly comes from Haematococcus pluvialis, and also includes various bacteria, yeast, plants and animal materials containing astaxanthin.

Embodiment 1: the preparation of the olive oil extract of natural astaxanthin:

The selected functional oil is olive oil, which is rich in unsaturated fatty acids, multivitamins and antioxidants, etc., which can effectively avoid stains and wrinkles caused by cell aging caused by fat oxidation. Olive oil is used as a solvent to extract natural oil astaxanthin extract, which can fully dissolve astaxanthin and promote skin absorption, and can better exert the antioxidant properties of astaxanthin.

The extraction steps of natural oil astaxanthin extract are as follows: for every 40-200g of food-grade Haematococcus pluvialis dry powder or food-grade Phaffia rhodozyma powder or bacterial dry bacteria rich in astaxanthin, add 400g of olive oil, Anaerobic, 5-15 degrees Celsius, pressure 35Mpa-45Mpa, high-pressure homogenization 3-5 times to obtain natural oil astaxanthin extract, vacuum low-temperature preservation; the content of natural astaxanthin in the extract is 0.1 Between %-10%.

Implementation Example 2: The preparation method of natural astaxanthin facial mask (liquid):

The preparation method of natural astaxanthin facial mask: select the following components, glycerin 3%, sodium lactate 2%, butylene glycol 3%, acrylic acid (ester) type/C10-30 alcohol acrylate cross-linked polymer potassium salt 0.7%, seaweed Sugar 1%, sodium hyaluronate 0.2%, phenoxyethanol 0.3%, EDTA disodium salt 0.03%g, natural oil astaxanthin extract 6%, deionized water 83.77%. According to the selected components:

(1) Mix acrylic acid (ester)/C10-30 alcohol acrylate cross-linked polymer potassium salt, glycerin, EDTA disodium salt, butanediol and deionized water, stir until completely dispersed, fully swell for 12 hours and then heat To 80 degrees, keep warm for 230 minutes;

(2), add sodium lactate, trehalose, sodium hyaluronate and phenoxyethanol when it cools down to 50 degrees, stir and mix thoroughly, place in vacuum, and wait for it to cool;

(3), when cooling to 5 degrees, add the natural oil astaxanthin extract, and stir evenly under vacuum;

(4) Take a small amount of samples and inspect them according to the QB/T2872 standard. After passing the inspection, filter at 300 meshes under the protection of nitrogen, vacuum pack into opaque containers, and obtain natural astaxanthin mask (liquid). When in use, the natural astaxanthin mask (liquid) can be smeared or sprayed on the face.

Implementation example 3: the preparation method of natural astaxanthin facial mask:

Astaxanthin mask consists of mask material and mask solution. The mask substrate is one of non-woven fabric, silk or biological fiber, wherein non-woven fabric is preferred.

The raw material of mask solution is made into astaxanthin mask solution according to the following ratio: every 100g mask solution contains glycerin 2g, sodium lactate 2g, butylene glycol 1g, acrylic acid (ester) type/C10-30 alcohol acrylate cross-linked polymer potassium salt 0.5 g, trehalose 1g, sodium hyaluronate 0.2g, phenoxyethanol 0.3g, EDTA disodium salt 0.03g, olive oil astaxanthin extract 8g, deionized water 84.97g. The prepared liquid natural astaxanthin mask can be evenly coated on the mask substrate.

Claims (6)

1. A method for extracting natural astaxanthin from functional oils, characterized in that the method comprises: food-grade Haematococcus pluvialis dry powder or food-grade Phaffia rhodozyme powder or bacterial dry thallus containing astaxanthin , according to the ratio of 1:10-1:2 to add functional oil, under the conditions of anaerobic, temperature 5-15 degrees Celsius, pressure 35Mpa-45Mpa, high-pressure homogenization 3-5 times, 10-30 minutes each time , the natural oil astaxanthin extract can be obtained. 2. The method for extracting natural astaxanthin from functional oils as claimed in claim 1, wherein said functional oils are one or more of olive oil, camellia oil, deep-sea fish oil, and safflower oil. 3. A formula of natural astaxanthin facial mask, characterized in that, when the facial mask is in a liquid state, its contained composition weight percent is: glycerin 2-3%, sodium lactate 0.8-2%, butylene glycol 1-3% , acrylic acid or propylene ester or C10-30 alcohol acrylate crosslinked polymer potassium salt 0.2-0.7%, trehalose 0.2-1%, sodium hyaluronate 0.01-0.2%, phenoxyethanol 0.1-0.3%, EDTA Disodium salt 0.01-0.03%g, natural oil astaxanthin extract 5-10%, deionized water 81-90%. 4. a preparation method of natural astaxanthin facial film, is characterized in that, when described facial film is liquid state, concrete steps are: (1), mix acrylic acid (ester) type/C10-30 alcohol acrylate crosslinked polymer potassium salt, glycerin, EDTA disodium salt, butylene glycol and deionized water according to the ratio in the formula of natural astaxanthin facial mask, Stir until completely dispersed, fully swell for 12 hours, heat to 80 degrees Celsius, and keep warm for 20-30 minutes; (2), when it is cooled to 50 degrees Celsius, add sodium lactate, trehalose, sodium hyaluronate and phenoxyethanol in the formula amount, stir and mix thoroughly, place in vacuum, and wait for it to cool to 5-10 degrees Celsius; (3), when cooling to 5-10 degrees Celsius, add natural oil astaxanthin extract, and stir evenly under vacuum; (4), take a small amount of samples, check according to the QB/T2872 standard, after passing the test, filter at 300 mesh under nitrogen protection, vacuum pack in opaque containers, and obtain liquid natural astaxanthin facial mask. 5. the preparation method of natural astaxanthin facial film as claimed in claim 4 is characterized in that, described liquid natural astaxanthin facial film is evenly coated on the facial mask substrate. 6. the preparation method of natural astaxanthin facial mask as claimed in claim 5 is characterized in that, described facial mask substrate is a kind of in non-woven fabric, silk or biological fiber.