CN105326660B - 一种带有结冷胶片状微胶囊的沐浴露 - Google Patents
一种带有结冷胶片状微胶囊的沐浴露 Download PDFInfo
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- 239000003094 microcapsule Substances 0.000 title claims abstract description 45
- 229920002148 Gellan gum Polymers 0.000 title claims abstract description 32
- 239000000216 gellan gum Substances 0.000 title claims abstract description 30
- 235000010492 gellan gum Nutrition 0.000 title claims abstract description 30
- 239000006071 cream Substances 0.000 title claims abstract description 19
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 18
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 16
- GHBFNMLVSPCDGN-UHFFFAOYSA-N caprylic acid monoglyceride Natural products CCCCCCCC(=O)OCC(O)CO GHBFNMLVSPCDGN-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000011780 sodium chloride Substances 0.000 claims abstract description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 6
- FENRSEGZMITUEF-ATTCVCFYSA-E [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].OP(=O)([O-])O[C@@H]1[C@@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H](OP(=O)([O-])[O-])[C@H](OP(=O)(O)[O-])[C@H]1OP(=O)([O-])[O-] FENRSEGZMITUEF-ATTCVCFYSA-E 0.000 claims abstract description 6
- 229940083982 sodium phytate Drugs 0.000 claims abstract description 6
- RMTFNDVZYPHUEF-XZBKPIIZSA-N 3-O-methyl-D-glucose Chemical compound O=C[C@H](O)[C@@H](OC)[C@H](O)[C@H](O)CO RMTFNDVZYPHUEF-XZBKPIIZSA-N 0.000 claims abstract description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 4
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 4
- 239000011734 sodium Substances 0.000 claims abstract description 4
- 239000003643 water by type Substances 0.000 claims abstract description 4
- -1 H-10 laurates Chemical class 0.000 claims abstract 2
- 239000000243 solution Substances 0.000 claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 8
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 4
- 239000011259 mixed solution Substances 0.000 claims description 4
- 239000012074 organic phase Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 239000006210 lotion Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- RWLALWYNXFYRGW-UHFFFAOYSA-N 2-Ethyl-1,3-hexanediol Chemical compound CCCC(O)C(CC)CO RWLALWYNXFYRGW-UHFFFAOYSA-N 0.000 claims description 2
- 239000008367 deionised water Substances 0.000 claims description 2
- 229910021641 deionized water Inorganic materials 0.000 claims description 2
- 229960005082 etohexadiol Drugs 0.000 claims description 2
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- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 2
- RRLOOYQHUHGIRJ-UHFFFAOYSA-M sodium;ethyl sulfate Chemical compound [Na+].CCOS([O-])(=O)=O RRLOOYQHUHGIRJ-UHFFFAOYSA-M 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims 1
- OVVINEZSSVQLTB-NRQGAZJASA-N (Z)-octadec-9-enoic acid (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal Chemical class OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O.CCCCCCCC\C=C/CCCCCCCC(O)=O.CCCCCCCC\C=C/CCCCCCCC(O)=O OVVINEZSSVQLTB-NRQGAZJASA-N 0.000 claims 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims 1
- 241000372132 Hydrometridae Species 0.000 claims 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims 1
- 239000005642 Oleic acid Substances 0.000 claims 1
- 229930182478 glucoside Natural products 0.000 claims 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims 1
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- 150000002148 esters Chemical class 0.000 abstract 1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/11—Encapsulated compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
本发明公开一种带有结冷胶片状微胶囊的沐浴露，所述沐浴露以重量份计，包括如下成分：76~80份去离子水、5~8份聚甘油－10‑月桂酸酯、0.15~0.3份香精、0.5~1份氢氧化钠、0.1~0.5份植酸钠、8~10份月桂醇硫酸酯钠、1~3份聚甘油－2‑葵酸酯、1~2份甘油辛酸酯、3~5份PEG－120 甲基葡萄糖二油酸酯、0.9~1.4份氯化钠和3~7份结冷胶片状微胶囊。采用本发明所述成分时，可使该结冷胶片状微胶囊在本发明沐浴露基质中得到软化，很容易推抹开。
Description
技术领域
本发明属于微胶囊技术领域，具体涉及一种带有结冷胶片状微胶囊的沐浴露。
背景技术
常采用微胶囊技术将对光、热等外界环境敏感的活性物质进行包埋，来延长活性物质的有效活性期间，这些包埋有活性成分的微胶囊被添加入化妆品基质以后，不容易被基质中的化学组分所影响，进而不会被破坏其所特有的活性，能够再化妆品基质中稳定存在。
但现有的微胶囊在化妆品基质中常常不能软化，仍保持原有的硬质质地，进而使消费者在使用带有该微胶囊的化妆品时，不能将微胶囊在皮肤上轻松推抹开，导致皮肤上出现很多硬质的微胶囊碎片，涂抹不均匀，因而存在一定的问题。
发明内容
针对现有技术存在的上述不足，本发明所要解决的技术问题是：如何提供一种带有结冷胶片状微胶囊的沐浴露，使该片状微胶囊在本发明沐浴露中能够得到软化，进而在皮肤上进行涂抹时容易推抹开，不会使皮肤上出现推抹不均匀的微胶囊碎片。
为了解决上述技术问题，本发明采用如下技术方案：一种带有结冷胶片状微胶囊的沐浴露，以重量份计，包括如下成分：76~80份去离子水、5~8份聚甘油－10-月桂酸酯、0.15~0.3份香精、0.5~1份氢氧化钠、0.1~0.5份植酸钠、8~10份月桂醇硫酸酯钠、1~3份聚甘油-2-癸酸酯、1~2份甘油辛酸酯、3~5份PEG－120 甲基葡萄糖二油酸酯、0.9~1.4份氯化钠和3~7份结冷胶片状微胶囊；
所述片状微胶囊以重量份计，包括如下成分：75份结冷胶、25份透明质酸钠、0.5份氧化铁黄、0.1份乙基己基甘油和0.8份1,2辛二醇。
相比现有技术，本发明具有如下有益效果：
1、本发明针对所使用的片状微胶囊的材料性质，通过创造性的研究发现，采用本发明所述成分时，通过各成分之间的交互配伍作用，可使该结冷胶片状微胶囊在本发明沐浴露基质中得到软化，进而通过实验发现将本发明带有结冷胶片状微胶囊的沐浴露涂抹在皮肤上时，片状微胶囊很容易推抹开，不会在皮肤上残留微胶囊的碎片，具有良好的涂抹性能。
2、本发明通过各成分之间的协同配伍作用，使本发明带有结冷胶片状微胶囊的沐浴露能稳定地发挥滋养、防止皮肤干燥的功效，不会使具有滋养、防止皮肤干燥功效的活性成分在产品保存期间内被破坏，稳定性良好。
3、本发明通过各成分之间的协同配伍作用，使片状微胶囊在沐浴露基质中既能被软化，又不会过分软化而导致微胶囊结构破坏、囊芯物质泄漏，对微胶囊具有良好的保护作用，有效延长了产品的货架期，具有良好的市场前景。
具体实施方式
下面结合实施例对本发明作进一步详细说明，本实施例中如无特别说明，所用原料均为市售。
本发明带有结冷胶片状微胶囊的沐浴露将去离子水和氢氧化钠、氯化钠、植酸钠混合均匀，作为水相；将聚甘油－10-月桂酸酯、香精、月桂醇硫酸酯钠、聚甘油-2-癸酸酯、甘油辛酸酯和PEG－120 甲基葡萄糖二油酸酯混合，搅拌均匀，作为有机相；将有机相和水相混合均匀，先进行高速搅拌搅拌均匀，再进行均质，得到均质物，向均质物中加入结冷胶片状微胶囊，得到带有结冷胶片状微胶囊的沐浴露。
所述结冷胶片状微胶囊采用如下方法制备而得：
1）将结冷胶用纯净水配制成质量浓度为0.5%的溶液，将透明质酸钠用纯净水配制成质量浓度为1%的溶液；
2）将步骤1）配制的溶液加热到60℃后，混合溶液并加入氧化铁黄混合均匀，保温，备用；
3）将乙基己基甘油和1,2辛二醇混合均匀，加热到75℃，加入步骤2）混合后的溶液中，进行均质，并保持混合物的温度为60~70℃，得均质物备用；
4）将步骤3）均质保温后的均质物用泵输出并滴加到斜面上，所述斜面上流淌有质量浓度为2%的氯化钠溶液，得到结冷胶片状微胶囊。
实施例1：
一种带有结冷胶片状微胶囊的沐浴露，成分如下表1所示：
表1 成分配方表
实施例2：
一种带有结冷胶片状微胶囊的沐浴露，所述成分如下表2所示：
表2 沐浴露的成分
最后说明的是，以上实施例仅用以说明本发明的技术方案而非限制，尽管申请人参照较佳实施例对本发明进行了详细说明，本领域的普通技术人员应当理解，对本发明的技术方案进行修改或者等同替换，而不脱离本发明技术方案的宗旨和范围的，均应涵盖在本发明的权利要求范围当中。
Claims (2)
1.一种带有结冷胶片状微胶囊的沐浴露，其特征在于，以重量份计，包括如下成分：76~80份去离子水、5~8份聚甘油－10-月桂酸酯、0.15~0.3份香精、0.5~1份氢氧化钠、0.1~0.5份植酸钠、8~10份月桂醇硫酸酯钠、1~3份聚甘油-2-癸酸酯、1~2份甘油辛酸酯、3~5份PEG－120 甲基葡萄糖二油酸酯、0.9~1.4份氯化钠和3~7份结冷胶片状微胶囊；
该带有结冷胶片状微胶囊的沐浴露的制备方法，包括如下步骤：
将去离子水和氢氧化钠、氯化钠、植酸钠混合均匀，作为水相；将聚甘油－10-月桂酸酯、香精、月桂醇硫酸酯钠、聚甘油-2-癸酸酯、甘油辛酸酯和PEG－120 甲基葡萄糖二油酸酯混合，搅拌均匀，作为有机相；将有机相和水相混合均匀，先进行高速搅拌搅拌均匀，再进行均质，得到均质物，向均质物中加入结冷胶片状微胶囊，得到带有结冷胶片状微胶囊的沐浴露；
其中，所述片状微胶囊以重量份计，包括如下成分：75份结冷胶、25份透明质酸钠、0.5份氧化铁黄、0.1份乙基己基甘油和0.8份1,2辛二醇；
所述结冷胶片状微胶囊采用如下方法制备而得：
1）将结冷胶用纯净水配制成质量浓度为0.5%的溶液，将透明质酸钠用纯净水配制成质量浓度为1%的溶液；
2）将步骤1）配制的溶液加热到60℃后，混合溶液并加入氧化铁黄混合均匀，保温，备用；
3）将乙基己基甘油和1,2辛二醇混合均匀，加热到75℃，加入步骤2）混合后的溶液中，进行均质，并保持混合物的温度为60~70℃，得均质物备用；
4）将步骤3）均质保温后的均质物用泵输出并滴加到斜面上，所述斜面上流淌有质量浓度为2%的氯化钠溶液，得到结冷胶片状微胶囊。
2.根据权利要求1所述带有结冷胶片状微胶囊的沐浴露，其特征在于，以重量份计，包括如下成分：76.45份去离子水、5.5份聚甘油－10-月桂酸酯、0.15香精、0.5份氢氧化钠、0.1份植酸钠、8份月桂醇硫酸酯钠、1份聚甘油-2-癸酸酯、1份甘油辛酸酯、3份PEG－120 甲基葡萄糖二油酸酯、0.9份氯化钠和3份结冷胶片状微胶囊。
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| US11628126B2 (en) | 2018-06-05 | 2023-04-18 | The Procter & Gamble Company | Clear cleansing composition |
| US11633072B2 (en) | 2021-02-12 | 2023-04-25 | The Procter & Gamble Company | Multi-phase shampoo composition with an aesthetic design |
| US11896689B2 (en) | 2019-06-28 | 2024-02-13 | The Procter & Gamble Company | Method of making a clear personal care comprising microcapsules |
| US11932448B2 (en) | 2020-02-14 | 2024-03-19 | The Procter & Gamble Company | Bottle adapted for storing a liquid composition with an aesthetic design suspended therein |
| US12053130B2 (en) | 2021-02-12 | 2024-08-06 | The Procter & Gamble Company | Container containing a shampoo composition with an aesthetic design formed by bubbles |
| US12268765B2 (en) | 2016-10-10 | 2025-04-08 | The Procter & Gamble Company | Personal care compositions substantially free of sulfated surfactants and containing a gel network |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US10945935B2 (en) | 2016-06-27 | 2021-03-16 | The Procter And Gamble Company | Shampoo composition containing a gel network |
| CN113164787B (zh) | 2018-12-14 | 2023-11-03 | 宝洁公司 | 包含片状微胶囊的洗发剂组合物 |
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| JP2011519969A (ja) * | 2008-05-12 | 2011-07-14 | タグラ バイオテクノロジーズ リミテッド | マイクロカプセル封入着色剤を含む局所適用のための組成物 |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US12268765B2 (en) | 2016-10-10 | 2025-04-08 | The Procter & Gamble Company | Personal care compositions substantially free of sulfated surfactants and containing a gel network |
| US11628126B2 (en) | 2018-06-05 | 2023-04-18 | The Procter & Gamble Company | Clear cleansing composition |
| US12128116B2 (en) | 2018-06-05 | 2024-10-29 | The Procter & Gamble Company | Clear cleansing composition |
| US11896689B2 (en) | 2019-06-28 | 2024-02-13 | The Procter & Gamble Company | Method of making a clear personal care comprising microcapsules |
| US11932448B2 (en) | 2020-02-14 | 2024-03-19 | The Procter & Gamble Company | Bottle adapted for storing a liquid composition with an aesthetic design suspended therein |
| US11633072B2 (en) | 2021-02-12 | 2023-04-25 | The Procter & Gamble Company | Multi-phase shampoo composition with an aesthetic design |
| US12053130B2 (en) | 2021-02-12 | 2024-08-06 | The Procter & Gamble Company | Container containing a shampoo composition with an aesthetic design formed by bubbles |
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