CN105166085A - Antioxidant health rice bran oil and preparation method thereof - Google Patents
Antioxidant health rice bran oil and preparation method thereof Download PDFInfo
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- CN105166085A CN105166085A CN201510400297.5A CN201510400297A CN105166085A CN 105166085 A CN105166085 A CN 105166085A CN 201510400297 A CN201510400297 A CN 201510400297A CN 105166085 A CN105166085 A CN 105166085A
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- rice bran
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Abstract
The invention discloses an antioxidant health rice bran oil, which comprises the following raw materials by weight: 50-70 parts of rice bran oil, 10-20 parts of camellia oil, 10-20 parts of canola oil, 3-6 parts of Chinese wolfberry, 5-10 parts of garlic, 6-9 parts of licorice, 3-5 parts of a ginkgo leaf extract, 2-4 parts of a rhodiola extract, 3-6 parts of a herba epimedii extract, 5-9 parts of grape seed, 3-9 parts of walnut kernel, 3-5 parts of Schisandra chinensis, 5-9 parts of peanut, and 6-10 parts of pinenut kernel. The invention also discloses a preparation method of the antioxidant health rice bran oil. The method includes the steps of: S1. Chinese wolfberry pretreatment; S2. garlic pretreatment; S3. licorice pretreatment; S4. squeezing oil making; and S5. mixing. The antioxidant health rice bran oil provided by the invention has strong antioxidant capacity, can delay aging, reduce blood fat, balance nutrition and enhance body immunity, and has the characteristics of health care, simple operation, good antioxidant effect, and an average DPPH free radical scavenging rate up to 99.69%.
Description
Technical field
The present invention relates to grease technical field, particularly relate to a kind of anti-oxidation health rice bran oil and preparation method thereof.
Background technology
Rice bran oil is rich in unrighted acid, and based on oleic acid and linoleic acid, both ratios are referred to as abroad close to 1:1 " health-nutrition oil ".Also containing some sp act compositions in rice bran oil, as oryzanol, tocopherol, squalene, sterol etc.Can not there is allergic reaction in edible rice bran oil, rice bran oil can increase HDL-C protein content, and reduce low density cholesterol lipoprotein content, be improved immunologic function, reduce blood fat, prevent and treat artery sclerosis, anticancer etc. maintains the effect of body health.
At present, the technique of China's refining rice bran oil is not perfect, and when storing rice bran, a large amount of unrighted acid can be decomposed; During refining rice bran oil, oryzanol, tocopherol, squalene, sterol isoreactivity become branch to run off in a large number.Cause single, the functional difference of rice bran oil composition commercially available at present.So, provide a kind of multi-functional rice bran oil to become the task of top priority.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes a kind of anti-oxidation health rice bran oil and preparation method thereof, oxidation resistance of the present invention is strong, can delay senility, reduce cholesterol, reduce blood fat, balanced nutritious, strengthen immunity of organisms, cancer-resisting, health care, simple to operate, antioxidant effect of the present invention is good, and average DPPH free radical scavenging activity reaches 99.69%.
A kind of anti-oxidation health rice bran oil that the present invention proposes, its raw material comprises by weight: rice bran oil 50-70 part, tea oil 10-20 part, Canola oil 10-20 part, fruit of Chinese wolfberry 3-6 part, garlic 5-10 part, Radix Glycyrrhizae 6-9 part, ginkgo biloba p.e 3-5 part, gadol extract 2-4 part, Shorthorned Epimedium P.E 3-6 part, grape pip 5-9 part, walnut kernel 3-9 part, fruit of Chinese magnoliavine 3-5 part, peanut 5-9 part, SEMEN PINI KORAIENSIS 6-10 part.
Tea oil, containing higher natural anti-oxidation ingredients Vitamin E, vitamin D, effectively can supplement the nutrition of needed by human body, removes harmful components, delays cell senescence, keeps cell viability.In addition low linolenic, makes tea oil good stability, easily stores, and not easily becomes sour rotten.The unsaturated fatty acid content of tea oil, up to 90%, is easily absorbed by the body after edible, can also promote that human body is to the absorption of the trace element such as fat-soluble fiber and calcium, iron, zinc simultaneously.Unrighted acid can make the concentration of Blood Cholesterol reduce, and can prevent artery sclerosis like this, suppresses and cardiovascular and cerebrovascular disease such as prevention coronary heart disease, hypertension etc.Tea oil is not containing the aflatoxins that can cause human carcinogen, and long-term eating has certain prevention effect to the disease such as hypertension, heart disease, is particularly suitable for the elderly edible.
Contain the unsaturated fat of 93% in Canola oil, do not contain cholesterol and trans fats, and have minimum saturated fat levels.Its LDL-C, to reduce coronary heart disease play good effect.Canola oil is rich in vitamin E, delays cell senescence, keeps cell viability.Canola oil contains a kind of special unrighted acid, is called ω-3 leukotrienes, can to congeal into bulk by anti-Hemostatic Oral Liquid, lowers the crisis of heart disease and stroke.
The fruit of Chinese wolfberry, calls as red fruit etc., is matrimony vine dry mature fruit.Taste is sweet, and property is put down.Return liver, kidney, lung channel.Can nourishing liver and kidney, benefiting shrewd head.Cure mainly that consumptive disease essence is lost, soreness of waist and knee joint, dizzy tinnitus, interior heat is quenched one's thirst, the deficiency of blood is sallow, blurred vision is not clear.Containing carrotene, betaine, vitamin A, vitamin B1, vitamin B2, vitamin C and calcium, phosphorus, iron etc. in matrimony vine, have the pharmacological action increasing leukocyte activity, promote liver cell new life, matrimony vine can also strengthen immunity of organisms, hypotensive, hypoglycemic, blood fat.Multiple components in the fruit of Chinese wolfberry; comprise polysaccharide, flavonoids, carotenoid etc. and all there is good anti-oxidation function; they effectively can improve the activity of anti-oxidant albumen in multiple positions of health, different cell types; scavenging capacity oxygen radical; reduce the generation of lipid, protein and DNA peroxide; and then Cell protection device, intracellular redox environment and body function, reach the effect delayed senility.
Garlic, calling as garlic, the head of garlic, giant garlic, calabash, solely garlic, single clove garlic etc., is the bulb of liliaceous plant garlic.Taste is pungent, flat, warm in nature.Return spleen, stomach, lung channel.Can Wen Zhonghang stagnant, removing toxic substances, desinsection.Cure mainly coldness and pain in the epigastrium, dysentery, for cancer, have loose bowels, pruritus vulvae, malaria, larynx numbness, oedema under tuberculosis, pertussis, flu, carbuncle furuncle poison, acute appendicitis, tinea sore, snake bite and insect sting, hookworm disease, enterobiasis, band.Containing allicin, diallyl disulphide, allyl sulfide, allicin and alliin in garlic, except above-mentioned sulfur-containing compound, the trace elements such as the selenium in garlic, germanium, and the natural component such as vitamin A, B1, C.Wherein, selenium, germanium, garlic alkene, at anti-oxidant, anticoagulation, removing toxic substances, anticancer, anti-aging and in organic cell-mediated immunity, all play very important effect in humoral immunity adjustment process.
Radix Glycyrrhizae, calls as sweet grass roots, Radix Glycyrrhizae, unpeeled RADIX GLYCYRRHIZAE, powder grass, lantern etc., is the root and rhizome of dicotyledon pulse family Radix Glycyrrhizae, glycyrrhiza inflate bat or glycyrrhiza glabra.Taste is sweet, and property is put down.Return stomach, lung, the spleen channel.Can clearing heat and detoxicating, moisten the lung and relieve the cough, coordinating the drug actions of a prescription, honey-fried licorice root can invigorate the spleen and benefit qi.Cure mainly abscess of throat, cough, weakness of the spleen and the stomach, taste-blindness rate, hepatitis, hysteria, carbuncle furuncle poison, medicine and food poisoning.Radix Glycyrrhizae has anti-arrhythmia, reducing blood lipid, anti arteriosclerosis, Antiaggregating activity on platelet, antineoplastic action.Containing multiple triterpenes and flavone compound in Radix Glycyrrhizae, these compounds have and all have antioxidation.
Containing a large amount of ginkgo flavonoid glycosides and ginkgolide in ginkgo biloba p.e, ginkgo is covered lactone with mat and optionally resists platelet activating factor, prevention of stroke, myocardial infarction; Ginkgo flavonoid glycoside can effectively resist and eliminate free radical, and plays the good action delayed senility; Ginkgolide and ginkgo flavonoid glycoside act synergistically; expansible blood vessel, increase CBF; improve cardiovascular and cerebrovascular circulation; under anaerobic conditions protect brain and cardiac muscle cell; triglycerides in blood can be reduced in addition; and improve hdl concentration, improve the activity of erythrocyte superoxide dismutase.
Containing rhodiola essence in gadol extract, can improve the activity of brain tissue SOD and glutathione peroxidase, suppressing the formation of lipid peroxide, is a kind of stronger polyphenoils; In addition gadol extract also has anti-diabetic, anti-pneumonia, asthma, anticancer effect.
Containing multiple flavones monomer component in Shorthorned Epimedium P.E, these flavones monomers all have antioxidation in various degree, never can ring Aging mechanism by Tongfang face.Barren wort total chromocor has the immunity of enhancing T cell and B cell is immune and adrenocortical function, illustrates that barrenwort has delaying senility function.
Grape seed extract has the effect of scavenging free radicals, anti-oxidant, anti-prostate cancer, anti-liver neoplasm, can also resist neural damage.The antioxidant effect of grape seed extract is 30-50 times of vitamin C and vitamin E.Superpower anti-oxidant efficiency has scavenging free radicals, improves the powerful effect of body immunity.Grape pip can reducing blood lipid, hypotensive, suppresses the formation of thrombus, reduces the generation of fatty liver, edema, the trace of blood that prevention vascular wall fragility causes, alleviate oedema and leg swelling, alleviate bruise, sports injuries, improve varication, venous insufficiency, phlebitis, control capillary hemorrhage.
Walnut kernel, calls as juglandis,semen, Semen Juglandis, walnut, is the dry mature seed of juglandaceae plant English walnut.Taste is sweet, warm in nature.Return lung, kidney, large intestine channel.Energy temperature compensation lung kidney, Dingchuan ease constipation.Cure mainly lumbago due to the kidney deficiency, pin be soft, the cold of insufficiency type is breathed with cough, dry feces.The fatty oil of walnut kernel, principal component is linoleic acid, oleic acid, linolenic glyceride; Another containing protein, carbohydrate, calcium, phosphorus, iron, carrotene, carbohydrate, nicotinic acid, α and γ-vitamin E, vitamin B1, B2.A large amount of vitamin Es that walnut kernel contains, often the edible effect having profit skin, black beard and hair, can make skin moisturizing smooth, springiness, have good antioxidation.
The fruit of Chinese magnoliavine, calling as mountain flower green pepper, sliding weight of steelyard, the medicine fruit of Chinese magnoliavine, face rattan, five plums etc., is the fruit of the Magnoliaceae liana fruit of Chinese magnoliavine, schisandra chinensis.Taste acid, warm in nature.Return lung, kidney channel.Can astringe the lung, nourshing kidney, promote the production of body fluid, receive sweat, puckery essence.Cure mainly that the deficiency syndrome of the lung is breathed with cough, dry makes thin thin, the emission of thirsty, spontaneous perspiration, night sweat, internal lesion caused by overexertion, rushes down protracted dysentery for a long time.The fruit of Chinese magnoliavine contains abundant organic acid, vitamin, flavonoids, phytosterol and has the lignan of potent antioxidation, as schizandrin, deoxyschizandrin or fruit of Chinese magnoliavine fat element etc., can beneficial gas strong liver, promote cells exclude refuse efficiency, improve memory, delay senility.
Peanut, calling as peanut, fallen flowers ginseng, kind beans, soil dew, peanut, the pine etc. that lands, is the seed of legume peanut.Taste is sweet, and property is put down.Return lung, the spleen channel.Energy moistening lung, and stomach.Cure mainly cough caused by dryness, gastric disorder causing nausea, beriberi, newborn woman's milk is few.Peanut is containing abundant fat, and protein, mineral matter, the multivitamins such as thiamine, riboflavin, niacin, also containing the amino acid that human body is necessary, have promotion brain cell development, strengthen the function of memory.Containing a large amount of α-and Gamma-Tocopherol etc., there is antioxidation.
SEMEN PINI KORAIENSIS, calling as son, korean pine seed, is the seed benevolence of pinaceae plant Korean pine.Taste is sweet, warm in nature.Have nourishing Yin and moistening lung, beautifying and antisenility, the function such as to promote longevity.Containing a large amount of unrighted acids and vitamin E in SEMEN PINI KORAIENSIS, vitamin E has effect that is anti-oxidant, that delay senility.
Preferably, its raw material comprises by weight: rice bran oil 55-65 part, tea oil 13-17 part, Canola oil 13-17 part, fruit of Chinese wolfberry 4-5 part, garlic 6-8 part, Radix Glycyrrhizae 7-8 part, ginkgo biloba p.e 3.5-4.5 part, gadol extract 2.5-3.5 part, Shorthorned Epimedium P.E 4-5 part, grape pip 6-8 part, walnut kernel 5-7 part, fruit of Chinese magnoliavine 3.5-4.5 part, peanut 6-8 part, SEMEN PINI KORAIENSIS 7-9 part.
The invention allows for the preparation method of above-mentioned anti-oxidation health rice bran oil, comprise the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 60-80wt% ethanol water, is to heat 0.6-1min in the microwave of 380-420W in power, warming-in-water is to 75-85 DEG C, and be incubated 30-50min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 20-40wt% ethanol water, be heat 0.5-1.5min in the microwave of 480-520W in power, warming-in-water is to 85-95 DEG C, insulation 30-50min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing;
S2, garlic pretreatment: pulverized by garlic, add water, be warming up to 40-60 DEG C, after insulation 50-70min, be warming up to 90-100 DEG C, steam distillation 100-140min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing;
S3, Radix Glycyrrhizae pretreatment: pulverized by Radix Glycyrrhizae, adding mass fraction is 70-90wt% ethanol water, is warming up to 90-110 DEG C, backflow 30-50min, fetch flow liquid, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing;
S4, squeezing liquefaction: grape pip, walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 30-50 DEG C, being dried to moisture is 0.5-1.5wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 0-5 DEG C, pressure is adjusted to 40-60MPa, squeezing 30-50min, and essence filter obtains expressed oil;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
Preferably, in S1, the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 60-80wt% ethanol water is 1:15-20, and the fruit of Chinese wolfberry and mass fraction are that the bulking value (g/ml) of 20-40wt% ethanol water is than being 1:15-20.
Preferably, in S1, the fruit of Chinese wolfberry after pulverizing is 30-60 order.
Preferably, in S2, the bulking value (g/ml) of garlic and water is than being 1:4-6, and the garlic after pulverizing is 60-120 order.
Preferably, in S3, Radix Glycyrrhizae and mass fraction are bulking value (g/ml) ratio of 70-90wt% ethanol water is 1:15-25, and the Radix Glycyrrhizae after pulverizing is 30-50 order.
Preferably, in S4, walnut kernel is cooked peeling process before pulverizing, and peeling concrete steps are: walnut kernel being added temperature is in the mass fraction 0.3-0.5wt% sodium hydroxide solution of 65-75 DEG C, soak 15-20min, wash and obtain barking walnut kernel 5-7 time.
Preferably, in S4, the concrete steps of essence filter are: through 800 keevil frame Filter Press under 1-2MPa pressure, then filter through ultra-filtration membrane device under 1-3MPa pressure.
In above-mentioned S1, the concrete steps of " being heat 0.6-1min in the microwave of 380-420W in power " are: be heat 3 times in the microwave of 380-420W in power, heat 0.6-1min at every turn.
In above-mentioned S1, the concrete steps of " being heat 0.5-1.5min in the microwave of 480-520W in power " are: be heat 3 times in the microwave of 480-520W in power, heat 0.5-1.5min at every turn.
In above-mentioned S3, the concrete operations of " backflow 30-50min " are: backflow 30-50min, reflux 3 times, when refluxing, Radix Glycyrrhizae and mass fraction are that the bulking value (g/ml) of 70-90wt% ethanol water is than being 1:15-25 at every turn.
The tea oil that the present invention selects, Canola oil contain a large amount of vitamin E, have higher oxidation resistance, can be anti-ageing, and tea oil, Canola oil can reduce blood fat, prevent artery sclerosis, the polysaccharide contained in the fruit of Chinese wolfberry, flavonoids, carotenoid, selenium in garlic, germanium, garlic alkene, containing multiple triterpenes and flavone compound in Radix Glycyrrhizae, containing a large amount of ginkgo flavonoid glycosides in ginkgo biloba p.e, containing rhodiola essence in gadol extract, containing multiple flavones monomer component in Shorthorned Epimedium P.E, grape seed extract, a large amount of vitamin Es that walnut kernel contains, the fruit of Chinese magnoliavine contains lignan, peanut contains α-and Gamma-Tocopherol, SEMEN PINI KORAIENSIS contains vitamin E, these materials all have good anti-oxidation function, above-mentioned each material and rice bran oil interact and reach anti-oxidant, the effect delayed senility, tea oil, Canola oil, matrimony vine, ginkgo biloba p.e cooperatively interact and can reach the function of reduction cholesterol, reduction blood fat, the present invention take rice bran oil as solvent, absorb trace element and the active material of above-mentioned plurality of raw materials, make it contain multivitamin, trace element and other active materials useful to human body, reach anti-oxidant, delay senility, reduce blood fat, balanced nutritious, strengthen immunity of organisms, cancer-resisting, health care effect, simple to operate, antioxidant effect of the present invention is good, and average DPPH free radical scavenging activity reaches 99.69%.
Accompanying drawing explanation
Fig. 1 is preparation method's schematic flow sheet of a kind of anti-oxidation health rice bran oil that the present invention proposes.
Detailed description of the invention
As shown in Figure 1, Fig. 1 is preparation method's schematic flow sheet of a kind of anti-oxidation health rice bran oil that the present invention proposes.
With reference to Fig. 1, the preparation method of a kind of anti-oxidation health rice bran oil that the present invention proposes, comprises the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 60-80wt% ethanol water, is to heat 0.6-1min in the microwave of 380-420W in power, warming-in-water is to 75-85 DEG C, and be incubated 30-50min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 20-40wt% ethanol water, be heat 0.5-1.5min in the microwave of 480-520W in power, warming-in-water is to 85-95 DEG C, insulation 30-50min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing;
S2, garlic pretreatment: pulverized by garlic, add water, be warming up to 40-60 DEG C, after insulation 50-70min, be warming up to 90-100 DEG C, steam distillation 100-140min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing;
S3, Radix Glycyrrhizae pretreatment: pulverized by Radix Glycyrrhizae, adding mass fraction is 70-90wt% ethanol water, is warming up to 90-110 DEG C, backflow 30-50min, fetch flow liquid, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing;
S4, squeezing liquefaction: grape pip, walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 30-50 DEG C, being dried to moisture is 0.5-1.5wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 0-5 DEG C, pressure is adjusted to 40-60MPa, squeezing 30-50min, and essence filter obtains expressed oil;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
A kind of anti-oxidation health rice bran oil, its raw material comprises by weight: rice bran oil 70 parts, tea oil 10 parts, Canola oil 20 parts, the fruit of Chinese wolfberry 3 parts, 10 parts, garlic, 6 parts, Radix Glycyrrhizae, ginkgo biloba p.e 5 parts, gadol extract 2 parts, Shorthorned Epimedium P.E 6 parts, grape pip 5 parts, walnut kernel 9 parts, 3 parts, the fruit of Chinese magnoliavine, peanut 9 parts, SEMEN PINI KORAIENSIS 6 parts.
The preparation method of above-mentioned anti-oxidation health rice bran oil, comprises the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 80wt% ethanol water, be heat 3 times in the microwave of 380W in power, heat 1min, warming-in-water to 75 DEG C at every turn, insulation 50min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 20wt% ethanol water, be heat 3 times in the microwave of 520W in power, each heating 0.5min, warming-in-water to 95 DEG C, insulation 30min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing, wherein, the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 80wt% ethanol water is 1:15, and the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 20wt% ethanol water is 1:20, and the fruit of Chinese wolfberry after pulverizing is 30 orders;
S2, garlic pretreatment: garlic is pulverized, add water, be warming up to 60 DEG C, after insulation 50min, be warming up to 100 DEG C, steam distillation 100min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing, wherein, the bulking value (g/ml) of garlic and water is than being 1:6, and the garlic after pulverizing is 60 orders;
S3, Radix Glycyrrhizae pretreatment: Radix Glycyrrhizae is pulverized, adding mass fraction is 90wt% ethanol water, be warming up to 90 DEG C, backflow 50min, refluxes 3 times, merge phegma, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing, wherein, when refluxing at every turn, Radix Glycyrrhizae and mass fraction be the bulking value (g/ml) of 90wt% ethanol water than being 1:15, the Radix Glycyrrhizae after pulverizing is 50 orders;
S4, squeezing liquefaction: walnut kernel being added temperature is in the mass fraction 0.5wt% sodium hydroxide solution of 65 DEG C, soaks 15min, washes and obtain barking walnut kernel 7 times; Grape pip, barking walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 30 DEG C, being dried to moisture is 1.5wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 0 DEG C, pressure is adjusted to 60MPa, squeezing 30min, through 800 keevil frame Filter Press under 2MPa pressure, then obtain expressed oil through ultra-filtration membrane device filtration under 1MPa pressure;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
Embodiment 2
A kind of anti-oxidation health rice bran oil, its raw material comprises by weight: rice bran oil 50 parts, tea oil 20 parts, Canola oil 10 parts, the fruit of Chinese wolfberry 6 parts, 5 parts, garlic, 9 parts, Radix Glycyrrhizae, ginkgo biloba p.e 3 parts, gadol extract 4 parts, Shorthorned Epimedium P.E 3 parts, grape pip 9 parts, walnut kernel 3 parts, 5 parts, the fruit of Chinese magnoliavine, peanut 5 parts, SEMEN PINI KORAIENSIS 10 parts.
The preparation method of above-mentioned anti-oxidation health rice bran oil, comprises the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 60wt% ethanol water, be heat 3 times in the microwave of 420W in power, heat 0.6min, warming-in-water to 85 DEG C at every turn, insulation 30min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 40wt% ethanol water, be heat 3 times in the microwave of 480W in power, each heating 1.5min, warming-in-water to 85 DEG C, insulation 50min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing, wherein, the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 60wt% ethanol water is 1:20, and the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 40wt% ethanol water is 1:15, and the fruit of Chinese wolfberry after pulverizing is 60 orders;
S2, garlic pretreatment: garlic is pulverized, add water, be warming up to 40 DEG C, after insulation 70min, be warming up to 90 DEG C, steam distillation 140min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing, wherein, the bulking value (g/ml) of garlic and water is than being 1:4, and the garlic after pulverizing is 120 orders;
S3, Radix Glycyrrhizae pretreatment: Radix Glycyrrhizae is pulverized, adding mass fraction is 70wt% ethanol water, be warming up to 110 DEG C, backflow 30min, refluxes 3 times, merge phegma, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing, wherein, when refluxing at every turn, Radix Glycyrrhizae and mass fraction be the bulking value (g/ml) of 70wt% ethanol water than being 1:25, the Radix Glycyrrhizae after pulverizing is 30 orders;
S4, squeezing liquefaction: walnut kernel being added temperature is in the mass fraction 0.3wt% sodium hydroxide solution of 75 DEG C, soaks 20min, washes and obtain barking walnut kernel 5 times; Grape pip, barking walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 50 DEG C, being dried to moisture is 0.5wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 5 DEG C, pressure is adjusted to 40MPa, squeezing 50min, through 800 keevil frame Filter Press under 1MPa pressure, then obtain expressed oil through ultra-filtration membrane device filtration under 3MPa pressure;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
Embodiment 3
A kind of anti-oxidation health rice bran oil, its raw material comprises by weight: rice bran oil 55 parts, tea oil 17 parts, Canola oil 13 parts, the fruit of Chinese wolfberry 5 parts, 6 parts, garlic, 8 parts, Radix Glycyrrhizae, ginkgo biloba p.e 3.5 parts, gadol extract 3.5 parts, Shorthorned Epimedium P.E 4 parts, grape pip 8 parts, walnut kernel 5 parts, 4.5 parts, the fruit of Chinese magnoliavine, peanut 6 parts, SEMEN PINI KORAIENSIS 9 parts.
The preparation method of above-mentioned anti-oxidation health rice bran oil, comprises the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 65wt% ethanol water, be heat 3 times in the microwave of 410W in power, heat 0.7min, warming-in-water to 82 DEG C at every turn, insulation 35min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 35wt% ethanol water, be heat 3 times in the microwave of 490W in power, each heating 1.2min, warming-in-water to 87 DEG C, insulation 45min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing, wherein, the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 65wt% ethanol water is 1:19, and the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 35wt% ethanol water is 1:17, and the fruit of Chinese wolfberry after pulverizing is 50 orders;
S2, garlic pretreatment: garlic is pulverized, add water, be warming up to 45 DEG C, after insulation 65min, be warming up to 93 DEG C, steam distillation 130min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing, wherein, the bulking value (g/ml) of garlic and water is than being 1:4.5, and the garlic after pulverizing is 100 orders;
S3, Radix Glycyrrhizae pretreatment: Radix Glycyrrhizae is pulverized, adding mass fraction is 75wt% ethanol water, be warming up to 105 DEG C, backflow 35min, refluxes 3 times, merge phegma, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing, wherein, when refluxing at every turn, Radix Glycyrrhizae and mass fraction be the bulking value (g/ml) of 75wt% ethanol water than being 1:23, the Radix Glycyrrhizae after pulverizing is 35 orders;
S4, squeezing liquefaction: walnut kernel being added temperature is in the mass fraction 0.35wt% sodium hydroxide solution of 72 DEG C, soaks 19min, washes and obtain barking walnut kernel 5 times; Grape pip, barking walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 45 DEG C, being dried to moisture is 0.8wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 3 DEG C, pressure is adjusted to 45MPa, squeezing 45min, through 800 keevil frame Filter Press under 1.3MPa pressure, then obtain expressed oil through ultra-filtration membrane device filtration under 2.5MPa pressure;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
Embodiment 4
A kind of anti-oxidation health rice bran oil, its raw material comprises by weight: rice bran oil 65 parts, tea oil 13 parts, Canola oil 17 parts, the fruit of Chinese wolfberry 4 parts, 8 parts, garlic, 7 parts, Radix Glycyrrhizae, ginkgo biloba p.e 4.5 parts, gadol extract 2.5 parts, Shorthorned Epimedium P.E 5 parts, grape pip 6 parts, walnut kernel 7 parts, 3.5 parts, the fruit of Chinese magnoliavine, peanut 8 parts, SEMEN PINI KORAIENSIS 7 parts.
The preparation method of above-mentioned anti-oxidation health rice bran oil, comprises the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 75wt% ethanol water, be heat 3 times in the microwave of 390W in power, heat 0.9min, warming-in-water to 78 DEG C at every turn, insulation 45min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 25wt% ethanol water, be heat 3 times in the microwave of 510W in power, each heating 0.8min, warming-in-water to 93 DEG C, insulation 35min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing, wherein, the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 75wt% ethanol water is 1:17, and the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 25wt% ethanol water is 1:19, and the fruit of Chinese wolfberry after pulverizing is 40 orders;
S2, garlic pretreatment: garlic is pulverized, add water, be warming up to 55 DEG C, after insulation 55min, be warming up to 97 DEG C, steam distillation 110min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing, wherein, the bulking value (g/ml) of garlic and water is than being 1:5.5, and the garlic after pulverizing is 80 orders;
S3, Radix Glycyrrhizae pretreatment: Radix Glycyrrhizae is pulverized, adding mass fraction is 85wt% ethanol water, be warming up to 95 DEG C, backflow 45min, refluxes 3 times, merge phegma, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing, wherein, when refluxing at every turn, Radix Glycyrrhizae and mass fraction be the bulking value (g/ml) of 85wt% ethanol water than being 1:17, the Radix Glycyrrhizae after pulverizing is 45 orders;
S4, squeezing liquefaction: walnut kernel being added temperature is in the mass fraction 0.45wt% sodium hydroxide solution of 68 DEG C, soaks 17min, washes and obtain barking walnut kernel 7 times; Grape pip, barking walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 35 DEG C, being dried to moisture is 1.2wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 1 DEG C, pressure is adjusted to 55MPa, squeezing 35min, through 800 keevil frame Filter Press under 1.7MPa pressure, then obtain expressed oil through ultra-filtration membrane device filtration under 1.5MPa pressure;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
Embodiment 5
A kind of anti-oxidation health rice bran oil, its raw material comprises by weight: rice bran oil 60 parts, tea oil 15 parts, Canola oil 15 parts, the fruit of Chinese wolfberry 4.5 parts, 7 parts, garlic, 7.5 parts, Radix Glycyrrhizae, ginkgo biloba p.e 4 parts, gadol extract 3 parts, Shorthorned Epimedium P.E 4.5 parts, grape pip 7 parts, walnut kernel 6 parts, 4 parts, the fruit of Chinese magnoliavine, peanut 7 parts, SEMEN PINI KORAIENSIS 8 parts.
The preparation method of above-mentioned anti-oxidation health rice bran oil, comprises the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 70wt% ethanol water, be heat 3 times in the microwave of 400W in power, heat 0.8min, warming-in-water to 80 DEG C at every turn, insulation 40min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 30wt% ethanol water, be heat 3 times in the microwave of 500W in power, each heating 1min, warming-in-water to 90 DEG C, insulation 40min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing, wherein, the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 70wt% ethanol water is 1:18, and the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 30wt% ethanol water is 1:18, and the fruit of Chinese wolfberry after pulverizing is 45 orders;
S2, garlic pretreatment: garlic is pulverized, add water, be warming up to 50 DEG C, after insulation 60min, be warming up to 95 DEG C, steam distillation 120min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing, wherein, the bulking value (g/ml) of garlic and water is than being 1:5, and the garlic after pulverizing is 90 orders;
S3, Radix Glycyrrhizae pretreatment: Radix Glycyrrhizae is pulverized, adding mass fraction is 80wt% ethanol water, be warming up to 100 DEG C, backflow 40min, refluxes 3 times, merge phegma, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing, wherein, when refluxing at every turn, Radix Glycyrrhizae and mass fraction be the bulking value (g/ml) of 80wt% ethanol water than being 1:20, the Radix Glycyrrhizae after pulverizing is 40 orders;
S4, squeezing liquefaction: walnut kernel being added temperature is in the mass fraction 0.4wt% sodium hydroxide solution of 70 DEG C, soaks 18min, washes and obtain barking walnut kernel 6 times; Grape pip, barking walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 40 DEG C, being dried to moisture is 1wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 2 DEG C, pressure is adjusted to 50MPa, squeezing 40min, through 800 keevil frame Filter Press under 1.5MPa pressure, then obtain expressed oil through ultra-filtration membrane device filtration under 2MPa pressure;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
DPPH free radical scavenging activity is utilized to evaluate the oxidation resistance of anti-oxidation health rice bran oil.
Solution preparation:
Solvent: absolute ethyl alcohol.
Need testing solution 1-5: the accurate anti-oxidation health rice bran oil taking embodiment 1-5 respectively, adds anhydrous alcohol solution, be mixed with the solution that concentration is 0.4mg/ml.
DPPH solution: DPPH concentration is the ethanol solution of 0.02mg/ml.
Precision measures 5ml need testing solution and 5mlDPPH solution respectively, is placed in same tool plug test tube, shakes up, and places 1h.Be that blank solvent measures its absorbance A in 517nm with absolute ethyl alcohol
i, and calculate clearance rate with following formula: clearance rate=[1-(A
i-A
j)/A
c] × 100%
In formula: A
c: the absorbance of 5ml absolute ethyl alcohol+5mlDPPH solution;
A
i: the absorbance of 5ml need testing solution+5mlDPPH solution;
A
j: the absorbance of 5ml need testing solution+5ml absolute ethyl alcohol.
The results are shown in following table:
As can be seen from the above table, antioxidant effect of the present invention is good, and average DPPH free radical scavenging activity reaches 99.69%.
The above; be only the present invention's preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (9)
1. an anti-oxidation health rice bran oil, is characterized in that, its raw material comprises by weight: rice bran oil 50-70 part, tea oil 10-20 part, Canola oil 10-20 part, fruit of Chinese wolfberry 3-6 part, garlic 5-10 part, Radix Glycyrrhizae 6-9 part, ginkgo biloba p.e 3-5 part, gadol extract 2-4 part, Shorthorned Epimedium P.E 3-6 part, grape pip 5-9 part, walnut kernel 3-9 part, fruit of Chinese magnoliavine 3-5 part, peanut 5-9 part, SEMEN PINI KORAIENSIS 6-10 part.
2. anti-oxidation health rice bran oil according to claim 1, it is characterized in that, its raw material comprises by weight: rice bran oil 55-65 part, tea oil 13-17 part, Canola oil 13-17 part, fruit of Chinese wolfberry 4-5 part, garlic 6-8 part, Radix Glycyrrhizae 7-8 part, ginkgo biloba p.e 3.5-4.5 part, gadol extract 2.5-3.5 part, Shorthorned Epimedium P.E 4-5 part, grape pip 6-8 part, walnut kernel 5-7 part, fruit of Chinese magnoliavine 3.5-4.5 part, peanut 6-8 part, SEMEN PINI KORAIENSIS 7-9 part.
3. the preparation method of anti-oxidation health rice bran oil according to claim 1 or 2, is characterized in that, comprise the steps:
S1, fruit of Chinese wolfberry pretreatment: pulverized by the fruit of Chinese wolfberry, adding mass fraction is 60-80wt% ethanol water, is to heat 0.6-1min in the microwave of 380-420W in power, warming-in-water is to 75-85 DEG C, and be incubated 30-50min, suction filtration obtains a leaching liquor; In filter residue, add mass fraction is 20-40wt% ethanol water, be heat 0.5-1.5min in the microwave of 480-520W in power, warming-in-water is to 85-95 DEG C, insulation 30-50min, suction filtration obtains secondary leaching liquor, merge a leaching liquor and secondary leaching liquor, rotary evaporation obtains fruit of Chinese wolfberry pretreatment thing;
S2, garlic pretreatment: pulverized by garlic, add water, be warming up to 40-60 DEG C, after insulation 50-70min, be warming up to 90-100 DEG C, steam distillation 100-140min, be separated, get oil phase Vacuum Concentration and obtain garlic pretreatment thing;
S3, Radix Glycyrrhizae pretreatment: pulverized by Radix Glycyrrhizae, adding mass fraction is 70-90wt% ethanol water, is warming up to 90-110 DEG C, backflow 30-50min, fetch flow liquid, rotary evaporation obtains Radix Glycyrrhizae pretreatment thing;
S4, squeezing liquefaction: grape pip, walnut kernel, the fruit of Chinese magnoliavine, peanut, SEMEN PINI KORAIENSIS are pulverized, be warming up to 30-50 DEG C, being dried to moisture is 0.5-1.5wt%, mix with fruit of Chinese wolfberry pretreatment thing, garlic pretreatment thing, Radix Glycyrrhizae pretreatment thing, ginkgo biloba p.e, gadol extract, Shorthorned Epimedium P.E, be cooled to 0-5 DEG C, pressure is adjusted to 40-60MPa, squeezing 30-50min, and essence filter obtains expressed oil;
S5, mixing: rice bran oil, tea oil, Canola oil and expressed oil are mixed and obtains anti-oxidation health rice bran oil.
4. the preparation method of anti-oxidation health rice bran oil according to claim 3, it is characterized in that, in S1, the fruit of Chinese wolfberry and mass fraction are bulking value (g/ml) ratio of 60-80wt% ethanol water is 1:15-20, and the fruit of Chinese wolfberry and mass fraction are that the bulking value (g/ml) of 20-40wt% ethanol water is than being 1:15-20.
5., according to the preparation method of claim 3 or 4 described anti-oxidation health rice bran oils, it is characterized in that, in S1, the fruit of Chinese wolfberry after pulverizing is 30-60 order.
6. the preparation method of anti-oxidation health rice bran oil according to any one of claim 3-5, is characterized in that, in S2, the bulking value (g/ml) of garlic and water is than being 1:4-6, and the garlic after pulverizing is 60-120 order.
7. the preparation method of anti-oxidation health rice bran oil according to any one of claim 3-6, it is characterized in that, in S3, Radix Glycyrrhizae and mass fraction are bulking value (g/ml) ratio of 70-90wt% ethanol water is 1:15-25, and the Radix Glycyrrhizae after pulverizing is 30-50 order.
8. the preparation method of anti-oxidation health rice bran oil according to any one of claim 3-7, it is characterized in that, in S4, walnut kernel is cooked peeling process before pulverizing, peeling concrete steps are: walnut kernel being added temperature is in the mass fraction 0.3-0.5wt% sodium hydroxide solution of 65-75 DEG C, soak 15-20min, wash and obtain barking walnut kernel 5-7 time.
9. the preparation method of anti-oxidation health rice bran oil according to any one of claim 3-8, is characterized in that, in S4, the concrete steps of essence filter are: through 800 keevil frame Filter Press under 1-2MPa pressure, then filter through ultra-filtration membrane device under 1-3MPa pressure.
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Application publication date: 20151223 |