CN105062683A - Lavender essence for water-based ink and preparation method thereof - Google Patents
Lavender essence for water-based ink and preparation method thereof Download PDFInfo
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- 244000178870 Lavandula angustifolia Species 0.000 title claims abstract description 100
- 235000010663 Lavandula angustifolia Nutrition 0.000 title claims abstract description 100
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 84
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000001102 lavandula vera Substances 0.000 title abstract description 92
- 235000018219 lavender Nutrition 0.000 title abstract description 92
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 claims abstract description 41
- 239000003921 oil Substances 0.000 claims abstract description 40
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 39
- GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 claims abstract description 38
- KGEKLUUHTZCSIP-HOSYDEDBSA-N [(1s,4s,6r)-1,7,7-trimethyl-6-bicyclo[2.2.1]heptanyl] acetate Chemical compound C1C[C@]2(C)[C@H](OC(=O)C)C[C@H]1C2(C)C KGEKLUUHTZCSIP-HOSYDEDBSA-N 0.000 claims abstract description 38
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 34
- IFYYFLINQYPWGJ-UHFFFAOYSA-N gamma-decalactone Chemical compound CCCCCCC1CCC(=O)O1 IFYYFLINQYPWGJ-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000000171 lavandula angustifolia l. flower oil Substances 0.000 claims abstract description 27
- KYQCOXFCLRTKLS-UHFFFAOYSA-N Pyrazine Chemical compound C1=CN=CC=N1 KYQCOXFCLRTKLS-UHFFFAOYSA-N 0.000 claims abstract description 22
- DTGKSKDOIYIVQL-WEDXCCLWSA-N (+)-borneol Chemical compound C1C[C@@]2(C)[C@@H](O)C[C@@H]1C2(C)C DTGKSKDOIYIVQL-WEDXCCLWSA-N 0.000 claims abstract description 19
- REPVLJRCJUVQFA-UHFFFAOYSA-N (-)-isopinocampheol Natural products C1C(O)C(C)C2C(C)(C)C1C2 REPVLJRCJUVQFA-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000005792 Geraniol Substances 0.000 claims abstract description 19
- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 claims abstract description 19
- 229940116229 borneol Drugs 0.000 claims abstract description 19
- CKDOCTFBFTVPSN-UHFFFAOYSA-N borneol Natural products C1CC2(C)C(C)CC1C2(C)C CKDOCTFBFTVPSN-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229940115397 bornyl acetate Drugs 0.000 claims abstract description 19
- DTGKSKDOIYIVQL-UHFFFAOYSA-N dl-isoborneol Natural products C1CC2(C)C(O)CC1C2(C)C DTGKSKDOIYIVQL-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229940113087 geraniol Drugs 0.000 claims abstract description 19
- HIGQPQRQIQDZMP-DHZHZOJOSA-N geranyl acetate Chemical compound CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 claims abstract description 19
- -1 lauryl nitrile Chemical class 0.000 claims abstract description 19
- UWKAYLJWKGQEPM-UHFFFAOYSA-N linalool acetate Natural products CC(C)=CCCC(C)(C=C)OC(C)=O UWKAYLJWKGQEPM-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000010678 thyme oil Substances 0.000 claims abstract description 19
- 239000008367 deionised water Chemical class 0.000 claims abstract description 17
- 229910021641 deionized water Chemical class 0.000 claims abstract description 17
- 239000002131 composite material Substances 0.000 claims abstract description 15
- FACFHHMQICTXFZ-UHFFFAOYSA-N 2-(2-phenylimidazo[1,2-a]pyridin-3-yl)ethanamine Chemical compound N1=C2C=CC=CN2C(CCN)=C1C1=CC=CC=C1 FACFHHMQICTXFZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- PCNDJXKNXGMECE-UHFFFAOYSA-N Phenazine Natural products C1=CC=CC2=NC3=CC=CC=C3N=C21 PCNDJXKNXGMECE-UHFFFAOYSA-N 0.000 claims abstract description 11
- IFYYFLINQYPWGJ-VIFPVBQESA-N gamma-Decalactone Natural products CCCCCC[C@H]1CCC(=O)O1 IFYYFLINQYPWGJ-VIFPVBQESA-N 0.000 claims abstract description 11
- 229940067137 musk ketone Drugs 0.000 claims abstract description 11
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Natural products CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 20
- 238000003756 stirring Methods 0.000 claims description 19
- PMGCQNGBLMMXEW-UHFFFAOYSA-N Isoamyl salicylate Chemical compound CC(C)CCOC(=O)C1=CC=CC=C1O PMGCQNGBLMMXEW-UHFFFAOYSA-N 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 17
- 239000006185 dispersion Substances 0.000 claims description 14
- 239000010659 mugwort oil Substances 0.000 claims description 11
- HQKQRXZEXPXXIG-VJOHVRBBSA-N chembl2333940 Chemical compound C1[C@]23[C@H](C)CC[C@H]3C(C)(C)[C@H]1[C@@](OC(C)=O)(C)CC2 HQKQRXZEXPXXIG-VJOHVRBBSA-N 0.000 claims description 10
- HMKKIXGYKWDQSV-KAMYIIQDSA-N alpha-Amylcinnamaldehyde Chemical compound CCCCC\C(C=O)=C\C1=CC=CC=C1 HMKKIXGYKWDQSV-KAMYIIQDSA-N 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 8
- 244000111489 Gardenia augusta Species 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 2
- 238000002156 mixing Methods 0.000 claims description 2
- IGODOXYLBBXFDW-UHFFFAOYSA-N alpha-Terpinyl acetate Chemical compound CC(=O)OC(C)(C)C1CCC(C)=CC1 IGODOXYLBBXFDW-UHFFFAOYSA-N 0.000 claims 8
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 claims 8
- WEFHSZAZNMEWKJ-KEDVMYETSA-N (6Z,8E)-undeca-6,8,10-trien-2-one (6E,8E)-undeca-6,8,10-trien-2-one (6Z,8E)-undeca-6,8,10-trien-3-one (6E,8E)-undeca-6,8,10-trien-3-one (6Z,8E)-undeca-6,8,10-trien-4-one (6E,8E)-undeca-6,8,10-trien-4-one Chemical compound CCCC(=O)C\C=C\C=C\C=C.CCCC(=O)C\C=C/C=C/C=C.CCC(=O)CC\C=C\C=C\C=C.CCC(=O)CC\C=C/C=C/C=C.CC(=O)CCC\C=C\C=C\C=C.CC(=O)CCC\C=C/C=C/C=C WEFHSZAZNMEWKJ-KEDVMYETSA-N 0.000 claims 4
- YGFGZTXGYTUXBA-UHFFFAOYSA-N (±)-2,6-dimethyl-5-heptenal Chemical compound O=CC(C)CCC=C(C)C YGFGZTXGYTUXBA-UHFFFAOYSA-N 0.000 claims 4
- 241000116713 Ferula gummosa Species 0.000 claims 4
- 235000018958 Gardenia augusta Nutrition 0.000 claims 4
- 241001072909 Salvia Species 0.000 claims 4
- 235000017276 Salvia Nutrition 0.000 claims 4
- 230000015572 biosynthetic process Effects 0.000 claims 4
- 239000001111 citrus aurantium l. leaf oil Substances 0.000 claims 4
- 239000004864 galbanum Substances 0.000 claims 4
- 150000002576 ketones Chemical class 0.000 claims 4
- BFBPISPWJZMWJN-UHFFFAOYSA-N methyl 2-[(7-hydroxy-3,7-dimethyloctylidene)amino]benzoate Chemical compound COC(=O)C1=CC=CC=C1N=CCC(C)CCCC(C)(C)O BFBPISPWJZMWJN-UHFFFAOYSA-N 0.000 claims 4
- 125000004998 naphthylethyl group Chemical group C1(=CC=CC2=CC=CC=C12)CC* 0.000 claims 4
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- 239000008346 aqueous phase Substances 0.000 claims 1
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- 150000002482 oligosaccharides Chemical class 0.000 abstract description 40
- 239000003205 fragrance Substances 0.000 abstract description 34
- 229920001542 oligosaccharide Polymers 0.000 abstract description 34
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 abstract description 30
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- 229940022663 acetate Drugs 0.000 abstract description 29
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- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 abstract description 15
- WTEVQBCEXWBHNA-UHFFFAOYSA-N Citral Natural products CC(C)=CCCC(C)=CC=O WTEVQBCEXWBHNA-UHFFFAOYSA-N 0.000 abstract description 15
- 244000179970 Monarda didyma Species 0.000 abstract description 15
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- 229940007550 benzyl acetate Drugs 0.000 abstract description 15
- 229940043350 citral Drugs 0.000 abstract description 15
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 abstract description 15
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- HMKKIXGYKWDQSV-SDNWHVSQSA-N 2-Pentyl-3-phenyl-2-propenal Chemical compound CCCCC\C(C=O)=C/C1=CC=CC=C1 HMKKIXGYKWDQSV-SDNWHVSQSA-N 0.000 abstract description 14
- 241000402754 Erythranthe moschata Species 0.000 abstract description 14
- ZMXIYERNXPIYFR-UHFFFAOYSA-N 1-ethylnaphthalene Chemical compound C1=CC=C2C(CC)=CC=CC2=C1 ZMXIYERNXPIYFR-UHFFFAOYSA-N 0.000 abstract description 13
- RJTJVVYSTUQWNI-UHFFFAOYSA-N beta-ethyl naphthalene Natural products C1=CC=CC2=CC(CC)=CC=C21 RJTJVVYSTUQWNI-UHFFFAOYSA-N 0.000 abstract description 13
- 239000001926 citrus aurantium l. subsp. bergamia wright et arn. oil Substances 0.000 abstract description 7
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- OPFTUNCRGUEPRZ-UHFFFAOYSA-N (+)-beta-Elemen Natural products CC(=C)C1CCC(C)(C=C)C(C(C)=C)C1 OPFTUNCRGUEPRZ-UHFFFAOYSA-N 0.000 abstract description 2
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- 238000000034 method Methods 0.000 abstract description 2
- NOKOOVDPFRWHJN-UHFFFAOYSA-N 2-(3-methylbutoxy)benzoic acid Chemical compound CC(C)CCOC1=CC=CC=C1C(O)=O NOKOOVDPFRWHJN-UHFFFAOYSA-N 0.000 abstract 1
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- WXCMHFPAUCOJIG-UHFFFAOYSA-N 4'-tert-Butyl-2',6'-dimethyl-3',5'-dinitroacetophenone Chemical compound CC(=O)C1=C(C)C([N+]([O-])=O)=C(C(C)(C)C)C([N+]([O-])=O)=C1C WXCMHFPAUCOJIG-UHFFFAOYSA-N 0.000 description 8
- VCOCESNMLNDPLX-BTXGZQJSSA-N (3s,6s)-2,2,8,8-tetramethyl-octahydro-1h-2,4a-methanonapthalene-10-one Chemical compound O=C1CCC(C)(C)[C@@]2(C3)C1C(C)(C)[C@H]3CC2 VCOCESNMLNDPLX-BTXGZQJSSA-N 0.000 description 6
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- 239000010619 basil oil Substances 0.000 description 2
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- Cosmetics (AREA)
- Medicinal Preparation (AREA)
Abstract
本发明一种水性油墨用薰衣草香精，按重量百分比计算，由1%-30%的薰衣草香精,5%-55%的复合改性低聚糖和去离子水组成；薰衣草香精由乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为冰片、百里香油、香柠檬薄荷油、格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、丙位癸内酯、乙醇组成，本发明还提供了上述水性油墨用薰衣草香精的制备方法。本发明提高了香精的留香和水溶性，使其适用于水性油墨的加香。A kind of lavender essence for water-based ink of the present invention, calculated by weight percentage, is made up of 1%-30% lavender essence, 5%-55% composite modified oligosaccharide and deionized water; Lavender essence is composed of linalyl acetate , linalool, bornyl acetate, terpineyl acetate, mass percent concentration of borneol, thyme oil, bergamot oil, gerpon pyrazine, methyl lavenderone, lavender oil, geraniol, geranyl acetate , Benzyl Acetate, Amyl Cinnamaldehyde, Neroli, Orange Leaf Oil, Ethyl Naphthalene, Artemisia Oil, Isopentyl Salicylic Acid, Gardeneraldehyde, Elemene, Clary Perilla Oil, Musk Ketone , Jiale musk, bergamot citral, lauryl nitrile, cedaryl acetate, isolonganone, synthetic moss, jasmonal, gamma-decalactone, ethanol, and the present invention also provides the lavender essence for the above-mentioned water-based ink method of preparation. The invention improves the fragrance retention and water solubility of the essence, making it suitable for the fragrance of water-based ink.
Description
技术领域 technical field
本发明属于化工领域，涉及一种香精，具体来说是一种水性油墨用薰衣草香精及其制备方法。 The invention belongs to the field of chemical industry and relates to an essence, in particular to a lavender essence for water-based ink and a preparation method thereof.
背景技术 Background technique
随着现代经济社会的发展，印刷业的发展逐渐被认为是衡量一个国家工业化、现代化的标志之一。油墨是用于印刷的重要材料，相对于传统的溶剂型油墨，水性油墨由于环保、低毒、健康、节约资源等特点深受使用者的青睐，受到越来越多的关注，目前的市场占有量越来越大，成为现今油墨行业的发展方向。水性油墨也叫水基油墨，是以水为主要溶剂，由水性高分子化合物形成的水基连接料与颜料及相关助剂经复配研磨加工而成的一种印刷油墨。 With the development of modern economy and society, the development of printing industry is gradually considered as one of the symbols to measure a country's industrialization and modernization. Ink is an important material for printing. Compared with traditional solvent-based ink, water-based ink is favored by users due to its environmental protection, low toxicity, health, and resource saving. It has received more and more attention. The current market share The volume is getting bigger and bigger, which has become the development direction of the ink industry today. Water-based ink is also called water-based ink. It is a printing ink made of water-based polymer compound, water-based binder, pigment and related additives, which are compounded and ground.
水性油墨一般不具有香气，若使水性油墨带有一定特征的芳香，将大大提高水性油墨的附加值和使用效果。这就需要在油墨中加入具有某种香型的香精。一般来说，香精是一种由人工调配出来的含有多种香料的混合物，而香料都是具有挥发性的有机化合物，在直接使用过程中易挥发，留香时间短，并且一般难溶于水。因此，具有长效留香的、可应用于水性油墨香精的研制具有非常重要的意义。可应用于水性油墨纳米胶囊薰衣草香精的制备未见报道。 Water-based inks generally do not have fragrance. If the water-based ink has a certain characteristic fragrance, the added value and use effect of the water-based ink will be greatly improved. This requires adding a fragrance with a certain fragrance to the ink. Generally speaking, essence is a mixture containing a variety of fragrances prepared artificially, and fragrances are volatile organic compounds, which are easy to volatilize during direct use, have a short fragrance retention time, and are generally difficult to dissolve in water. . Therefore, it is of great significance to develop a fragrance with a long-lasting fragrance that can be applied to water-based inks. There is no report on the preparation of nanocapsule lavender essence that can be applied to water-based ink.
发明内容 Contents of the invention
针对现有技术中的上述技术问题，本发明提供了一种水性油墨用薰衣草香精及其制备方法，所述的这种水性油墨用薰衣草香精及其制备方法解决了现有技术中的芳香型油墨留香时间短的技术问题。 Aiming at the above-mentioned technical problems in the prior art, the invention provides a kind of lavender essence for water-based ink and preparation method thereof, described this water-based ink lavender essence and preparation method thereof have solved the aromatic type ink in the prior art The technical problem of short lasting fragrance.
本发明提供了一种水性油墨用薰衣草香精，按重量百分比计算，其原料的组成及含量如下： The invention provides a kind of lavender essence for water-based ink, calculated by weight percentage, the composition and content of its raw materials are as follows:
薰衣草香精1%-30%, Lavender essence 1%-30%,
复合改性低聚糖5%-55%, Composite modified oligosaccharides 5%-55%,
余量为去离子水； The balance is deionized water;
所述的薰衣草香精按重量百分比计算，其组成及含量如下： Described lavender essence is calculated by weight percentage, and its composition and content are as follows:
乙酸芳樟酯15%-20%， Linalyl acetate 15%-20%,
芳樟醇3%-6%， Linalool 3%-6%,
乙酸龙脑酯3%-8%， Bornyl acetate 3%-8%,
乙酸松油酯1%-5%， Terpine acetate 1%-5%,
质量百分比浓度为10%的冰片0.5%-1%， Mass percentage concentration is 0.5%-1% of borneol of 10%,
百里香油10%-20%， Thyme oil 10%-20%,
香柠檬薄荷油2%-6%， Bergamot mint oil 2%-6%,
质量百分比浓度为1%的格蓬吡嗪0.5%-1% Mass percentage concentration is 0.5%-1% of glycopyrizine of 1%
甲基薰衣草酮1%-3%， Methyllavandone 1%-3%,
薰衣草油4%-8%， Lavender oil 4%-8%,
香叶醇5%-8%， Geraniol 5%-8%,
乙酸香叶酯3%-6%， Geranyl acetate 3%-6%,
乙酸苄酯3%-5%， Benzyl acetate 3%-5%,
甲位戊基桂醛1%-4%， Amyl cinnamaldehyde 1%-4%,
橙花素1%-3%， Neroli 1%-3%,
橙叶油2%-8%， Orange leaf oil 2%-8%,
乙位萘乙醚1%-3%， Ethylene naphthalene ethyl ether 1%-3%,
艾蒿油0.5%-2%， Mugwort oil 0.5%-2%,
柳酸异戊酯1%-5%， Isoamyl salicylate 1%-5%,
栀子醛1%-3%， Gardenia 1%-3%,
质量百分比浓度为10%的榄青酮0.5%-1% The mass percent concentration is 0.5%-1% of elvene greenone of 10%
香紫苏油1%-3%， Clare basil oil 1%-3%,
酮麝香1%-3%， Ketone musk 1%-3%,
佳乐麝香0.5%-3%， Jiale musk 0.5%-3%,
香柠檬醛0.5%-1%， Bergamot citral 0.5%-1%,
质量百分比浓度为10%的十二腈0.5%-1.5%， Mass percent concentration is 0.5%-1.5% of 10% dodecyl nitrile,
乙酸柏木酯0.5%-2%， Cedaryl acetate 0.5%-2%,
异长叶烷酮1%-3%， Isophyllinone 1%-3%,
合成青苔1%-2%， Synthetic moss 1%-2%,
洋茉莉醛1%-3%， Jasmonal 1%-3%,
质量百分比浓度为10%的丙位癸内酯0.1%-1.5%， The mass percent concentration is 0.1%-1.5% of gamma-decalactone of 10%,
余量为乙醇。 The balance is ethanol.
本发明还提供了上述的一种水性油墨用薰衣草香精的制备方法，包括如下步骤： The present invention also provides the preparation method of above-mentioned a kind of water-based ink lavender essence, comprises the steps:
1)一个制备薰衣草香精的步骤，按照质量百分比称取乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为10%的冰片、百里香油、香柠檬薄荷油、1%格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、10%榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、10%十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、10%丙位癸内酯、乙醇，将乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为10%的冰片、百里香油、香柠檬薄荷油、1%格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、10%榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、10%十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、10%丙位癸内酯、乙醇均匀混合即得到薰衣草香精； 1) A step for preparing lavender essence, weighing linalyl acetate, linalool, bornyl acetate, terpineyl acetate, borneol with a mass percentage concentration of 10%, thyme oil, bergamot oil, 1% Gelponpyrazine, Methyllavenderone, Lavender Oil, Geraniol, Geranyl Acetate, Benzyl Acetate, Amyl Cinnamaldehyde, Nerolidin, Orange Leaf Oil, Ethyl Naphthalene Ethyl Ether, Artemisia Artemisiae Oil, Isoamyl Salicylate, Gardenide, 10% Elemone, Sclare Oil, Ketone Musk, Kara Musk, Bergamot Citral, 10% Dodecyl Nitrile, Cedaryl Acetate, Isophallanone, Synthetic moss, jasmonal, 10% gamma-decalactone, ethanol, linalyl acetate, linalool, bornyl acetate, terpineyl acetate, borneol with a concentration of 10% by mass percentage, thyme oil, incense Lemon peppermint oil, 1% gerpon pyrazine, methyllavandone, lavender oil, geraniol, geranyl acetate, benzyl acetate, amyl cinnamaldehyde, nerolidin, orange leaf oil, ethyl naphthalene Ether, Artemisia Oil, Isoamyl Salicylate, Gardeninal, 10% Elemene, Clare Perilla Oil, Musk Ketone, Musk Musk, Bergamot Citral, 10% Dodecyl Nitrile, Cedaryl Acetate, Isolong Lavender essence can be obtained by uniformly mixing phyllothane, synthetic moss, jasmonal, 10% gamma-decalactone, and ethanol;
2)按照质量百分比称取薰衣草香精、复合改性低聚糖和去离子水，在一个反应容器中加入复合改性低聚糖，再加入去离子水，开启搅拌，使复合改性低聚糖均匀的分散在水相中，得到复合改性低聚糖分散液； 2) Take lavender essence, compound modified oligosaccharide and deionized water according to mass percentage, add compound modified oligosaccharide in a reaction vessel, then add deionized water, start stirring, make compound modified oligosaccharide Uniformly dispersed in the water phase to obtain a composite modified oligosaccharide dispersion;
3)将薰衣草香精，滴加到所得的复合改性低聚糖分散液中，继续搅拌，使香精分散均匀，并使复合改性低聚糖形成对香精分子的包覆，得到水性油墨用薰衣草香精。 3) Add the lavender essence dropwise to the obtained composite modified oligosaccharide dispersion, and continue stirring to disperse the essence evenly, and make the composite modified oligosaccharide form a coating on the essence molecules to obtain lavender for water-based ink. essence.
本发明提供了一种水性油墨，由上述的水性油墨用薰衣草香精和染料墨水组成，所述的水性油墨用薰衣草香精和染料墨水的质量比为1~10:90~99。 The invention provides a water-based ink, which is composed of the above-mentioned lavender essence for water-based ink and dye ink, and the mass ratio of the lavender essence for water-based ink and the dye ink is 1-10:90-99.
本发明提供了一种薰衣草香精，按重量百分比计算，其组成及含量如下： The invention provides a kind of lavender essence, calculated by weight percentage, its composition and content are as follows:
乙酸芳樟酯15%-20%， Linalyl acetate 15%-20%,
芳樟醇3%-6%， Linalool 3%-6%,
乙酸龙脑酯3%-8%， Bornyl acetate 3%-8%,
乙酸松油酯1%-5%， Terpine acetate 1%-5%,
质量百分比浓度为10%的冰片0.5%-1%， Mass percentage concentration is 0.5%-1% of borneol of 10%,
百里香油10%-20%， Thyme oil 10%-20%,
香柠檬薄荷油2%-6%， Bergamot mint oil 2%-6%,
质量百分比浓度为1%的格蓬吡嗪0.5%-1% Mass percentage concentration is 0.5%-1% of glycopyrizine of 1%
甲基薰衣草酮1%-3%， Methyllavandone 1%-3%,
薰衣草油4%-8%， Lavender oil 4%-8%,
香叶醇5%-8%， Geraniol 5%-8%,
乙酸香叶酯3%-6%， Geranyl acetate 3%-6%,
乙酸苄酯3%-5%， Benzyl acetate 3%-5%,
甲位戊基桂醛1%-4%， Amyl cinnamaldehyde 1%-4%,
橙花素1%-3%， Neroli 1%-3%,
橙叶油2%-8%， Orange leaf oil 2%-8%,
乙位萘乙醚1%-3%， Ethylene naphthalene ethyl ether 1%-3%,
艾蒿油0.5%-2%， Mugwort oil 0.5%-2%,
柳酸异戊酯1%-5%， Isoamyl salicylate 1%-5%,
栀子醛1%-3%， Gardenia 1%-3%,
质量百分比浓度为10%的榄青酮0.5%-1% The mass percent concentration is 0.5%-1% of elvene greenone of 10%
香紫苏油1%-3%， Clare basil oil 1%-3%,
酮麝香1%-3%， Ketone musk 1%-3%,
佳乐麝香0.5%-3%， Jiale musk 0.5%-3%,
香柠檬醛0.5%-1%， Bergamot citral 0.5%-1%,
质量百分比浓度为10%的十二腈0.5%-1.5%， Mass percent concentration is 0.5%-1.5% of 10% dodecyl nitrile,
乙酸柏木酯0.5%-2%， Cedaryl acetate 0.5%-2%,
异长叶烷酮1%-3%， Isophyllinone 1%-3%,
合成青苔1%-2%， Synthetic moss 1%-2%,
洋茉莉醛1%-3%， Jasmonal 1%-3%,
质量百分比浓度为10%的丙位癸内酯0.1%-1.5%， The mass percent concentration is 0.1%-1.5% of gamma-decalactone of 10%,
余量为乙醇。 The balance is ethanol.
复合改性低聚糖为市售产品，是由多个葡萄糖单元形成的具有多羟基的特殊结构的化合物，它能够溶于水并具有亲水和亲油的两亲结构，从而能够包覆油溶性香精，使油溶性香精溶于水，并增强了香精的留香。 Composite modified oligosaccharides are commercially available products, which are compounds with a special structure of multiple hydroxyl groups formed by multiple glucose units. Essence, which makes oil-soluble essence dissolve in water and enhances the fragrance of essence.
本发明根据天然薰衣草的香气特征和香韵，选取合适的原料，调配出香气新鲜、逼真的薰衣草香精。然后采用复合改性低聚糖为壁材，将薰衣草香精进行包覆，形成纳米胶囊香精，从而提高香精的留香和水溶性，使其适用于水性油墨的加香。 According to the aroma characteristics and flavor of natural lavender, the invention selects suitable raw materials to prepare the lavender essence with fresh and lifelike aroma. Then, the composite modified oligosaccharide is used as the wall material, and the lavender essence is coated to form a nanocapsule essence, thereby improving the fragrance retention and water solubility of the essence, making it suitable for the fragrance of water-based ink.
本发明和已有技术相比，其技术进步是显著的。本发明的一种纳米胶囊薰衣草香精，可更好地应用于水性油墨的加香，从而提高水性油墨的附加值和使用效果。该纳米胶囊薰衣草香精不发生分层，体系稳定，留香持久。 Compared with the prior art, the technical progress of the present invention is remarkable. The nanocapsule lavender essence of the present invention can be better applied to the perfuming of water-based ink, thereby improving the added value and use effect of the water-based ink. The nanocapsule lavender essence does not delaminate, has a stable system and lasts for a long time.
具体实施方式 Detailed ways
下面通过实施例对本发明作进一步地说明，但不影响本发明的保护范围。 The present invention will be further described below by way of examples, but does not affect protection scope of the present invention.
实施例1Example 1
一种水性油墨用薰衣草香精，按重量百分比计算，其原料的组成及含量如下： A kind of lavender essence for water-based ink, calculated by weight percentage, the composition and content of its raw materials are as follows:
薰衣草香精1g(1%)， Lavender essence 1g (1%),
复合改性低聚糖55g(55%)， Compound modified oligosaccharide 55g (55%),
去离子水44g(44%)； 44g (44%) deionized water;
上述的薰衣草香精，按重量百分比计算，其组成及含量如下： Above-mentioned lavender essence, by weight percentage, its composition and content are as follows:
乙酸芳樟酯15g(15%)， Linalyl acetate 15g (15%),
芳樟醇6g(6%)， Linalool 6g (6%),
乙酸龙脑酯3g(3%)， Bornyl acetate 3g (3%),
乙酸松油酯1g(1%)， Terpine acetate 1g (1%),
质量百分比浓度为10%的冰片1g(1%)， Mass percent concentration is 10% borneol 1g (1%),
百里香油10g(10%)， Thyme oil 10g (10%),
香柠檬薄荷油6g(6%)， bergamot mint oil 6g (6%),
质量百分比浓度为1%的格蓬吡嗪0.5g(0.5%)， Mass percentage concentration is 0.5g (0.5%) of 1% glycopyrizine,
甲基薰衣草酮3g(3%)， Methyllavandone 3g (3%),
薰衣草油4g(4%)， Lavender oil 4g (4%),
香叶醇5g(5%)， Geraniol 5g (5%),
乙酸香叶酯5g(5%)， Geranyl acetate 5g (5%),
乙酸苄酯3g(3%)， Benzyl acetate 3g (3%),
甲位戊基桂醛4g(4%)， Amyl cinnamic aldehyde 4g (4%),
橙花素1g(1%)， Nerolitin 1g (1%),
橙叶油8g(8%)， Orange leaf oil 8g (8%),
乙位萘乙醚1g(1%)， Ethyl naphthalene ethyl ether 1g (1%),
艾蒿油2g(2%)， Mugwort oil 2g (2%),
柳酸异戊酯1g(1%)， Isoamyl salicylate 1g (1%),
栀子醛3g(3%)， Gardenin aldehyde 3g (3%),
质量百分比浓度为10%的榄青酮0.5g(0.5%)， Mass percent concentration is 0.5g (0.5%) of elequinone 0.5g (0.5%) of 10%,
香紫苏油3g(3%)， Clare Perilla Oil 3g (3%),
酮麝香1g(1%)， Ketone musk 1g (1%),
佳乐麝香3g(3%)， Jiale musk 3g (3%),
香柠檬醛0.5g(0.5%)， Bergamot Citral 0.5g (0.5%),
质量百分比浓度为10%的十二腈1.5g(1.5%)， Mass percent concentration is 1.5g (1.5%) of 10% dodecyl nitrile,
乙酸柏木酯0.5g(0.5%)， Cedryl acetate 0.5g (0.5%),
异长叶烷酮3g(3%)， Isolongifolanone 3g (3%),
合成青苔1g(1%)， Synthetic moss 1g (1%),
洋茉莉醛3g(3%)， Jasmonal 3g (3%),
质量百分比浓度为10%的丙位癸内酯0.1g(0.1%)， Mass percent concentration is 0.1g (0.1%) of 10% gamma-decalactone,
乙醇0.4g(0.4%)； Ethanol 0.4g (0.4%);
上述的薰衣草香精的制备方法如下： The preparation method of above-mentioned lavender essence is as follows:
将乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为10%的冰片、百里香油、香柠檬薄荷油、1%格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、10%榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、10%十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、10%丙位癸内酯、乙醇均匀混合即得到薰衣草香精。得到的香精香气新鲜，略有香柠檬薄荷的香韵，具有薰衣草的特征香气。 Linalyl acetate, linalool, bornyl acetate, terpineyl acetate, borneol with a concentration of 10% by mass, thyme oil, bergamot oil, 1% gerpon pyrazine, methyllavenderone, lavender Oil, Geraniol, Geranyl Acetate, Benzyl Acetate, Amyl Cinnamaldehyde, Neroli, Orange Leaf Oil, Ethyl Naphthalene, Artemisia Oil, Isoamyl Salicylate, Gardeninal, 10 % elequinone, claret oil, musk ketone, musk jale, bergamot citral, 10% dodecyl cyanide, cedaryl acetate, isolongifolanone, synthetic moss, jasmonal, 10% gamma-decane Ester and ethanol are evenly mixed to obtain lavender essence. The resulting essence has a fresh aroma, slightly bergamot-mint, with a characteristic aroma of lavender.
上述的一种水性油墨用薰衣草香精的制备方法包括如下步骤： The preparation method of above-mentioned a kind of water-based ink lavender essence comprises the steps:
（1）、在150ml烧杯中加入55g的复合改性低聚糖，再加入44g的去离子水，开启搅拌，使复合改性低聚糖均匀的分散在水相中，形成复合改性低聚糖分散液； (1) Add 55g of compound modified oligosaccharides into a 150ml beaker, then add 44g of deionized water, start stirring, so that the compound modified oligosaccharides are evenly dispersed in the water phase to form a compound modified oligosaccharide sugar dispersion;
（2）、称取1g薰衣草香精，滴加到步骤（1）所得的复合改性低聚糖分散液中，继续搅拌，使香精分散均匀，并使复合改性低聚糖形成对香精分子的包覆，得到可应用于水性油墨的薰衣草纳米胶囊缓释香精。 (2) Weigh 1g of lavender essence, add it dropwise to the compound modified oligosaccharide dispersion obtained in step (1), and continue to stir to make the essence disperse evenly, and make the compound modified oligosaccharide form a bond to the essence molecules. Coating, obtain the lavender nanocapsule slow-release essence that can be applied to water-based ink.
称取薰衣草纳米胶囊缓释香精10g,加到90g水性油墨中，搅拌均匀，得到质量稳定的具有薰衣草特征香气的水性油墨。 Weigh 10 g of lavender nanocapsule slow-release essence, add it to 90 g of water-based ink, and stir evenly to obtain water-based ink with lavender characteristic fragrance with stable quality.
上述所得的薰衣草纳米胶囊缓释香精质量稳定，留香持久，具有薰衣草的特征香气，但香气强度稍弱。 The lavender nanocapsule slow-release essence obtained above has stable quality, long-lasting fragrance, and has the characteristic fragrance of lavender, but the fragrance intensity is slightly weak.
实施例2Example 2
一种水性油墨用薰衣草香精，按重量百分比计算，其原料的组成及含量如下： A kind of lavender essence for water-based ink, calculated by weight percentage, the composition and content of its raw materials are as follows:
薰衣草香精10g(10%)， Lavender essence 10g (10%),
复合改性低聚糖50g(50%)， Composite modified oligosaccharide 50g (50%),
去离子水40g(40%)； 40g (40%) deionized water;
上述的薰衣草香精，按重量百分比计算，其组成及含量如下： Above-mentioned lavender essence, by weight percentage, its composition and content are as follows:
乙酸芳樟酯20g(20%)， Linalyl acetate 20g (20%),
芳樟醇3g(3%)， Linalool 3g (3%),
乙酸龙脑酯8g(8%)， Bornyl acetate 8g (8%),
乙酸松油酯5g(5%)， Terpine acetate 5g (5%),
质量百分比浓度为10%的冰片0.5g(0.5%)， Mass percentage concentration is borneol 0.5g (0.5%) of 10%,
百里香油10g(10%)， Thyme oil 10g (10%),
香柠檬薄荷油2g(2%)， bergamot mint oil 2g (2%),
质量百分比浓度为1%的格蓬吡嗪1g(1%)， Mass percent concentration is 1% glycopyrizine 1g (1%),
甲基薰衣草酮1g(1%)， Methyllavandone 1g (1%),
薰衣草油4g(4%)， Lavender oil 4g (4%),
香叶醇8g(8%)， Geraniol 8g (8%),
乙酸香叶酯3g(3%)， Geranyl acetate 3g (3%),
乙酸苄酯5g(5%)， Benzyl acetate 5g (5%),
甲位戊基桂醛1g(1%)， Amyl cinnamaldehyde 1g (1%),
橙花素3g(3%)， Nerolitin 3g (3%),
橙叶油2g(2%)， Orange Leaf Oil 2g (2%),
乙位萘乙醚3g(3%)， Ethyl naphthalene ethyl ether 3g (3%),
艾蒿油0.5g(0.5%)， Mugwort oil 0.5g (0.5%),
柳酸异戊酯5g(5%)， Isopentyl salicylate 5g (5%),
栀子醛1g(1%)， Gardenin aldehyde 1g (1%),
质量百分比浓度为10%的榄青酮1g(1%)， Mass percent concentration is 10% evelynone 1g (1%),
香紫苏油1g(1%)， Clare Perilla Oil 1g (1%),
酮麝香3g(3%)， Ketone musk 3g (3%),
佳乐麝香0.5g(0.5%)， Jiale musk 0.5g (0.5%),
香柠檬醛1g(1%)， Bergamot citral 1g (1%),
质量百分比浓度为10%的十二腈0.5g(0.5%)， Mass percent concentration is 10% dodecyl nitrile 0.5g (0.5%),
乙酸柏木酯2g(2%)， Cedaryl acetate 2g (2%),
异长叶烷酮1g(1%)， Isophallanone 1g (1%),
合成青苔2g(2%)， synthetic moss 2g (2%),
洋茉莉醛1g(1%)， Jasmonal 1g (1%),
质量百分比浓度为10%的丙位癸内酯0.5g(0.5%)， Mass percent concentration is 0.5g (0.5%) of 10% gamma-decalactone,
乙醇0.5g(0.5%)； Ethanol 0.5g (0.5%);
上述的薰衣草香精的制备方法如下： The preparation method of above-mentioned lavender essence is as follows:
将乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为10%的冰片、百里香油、香柠檬薄荷油、1%格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、10%榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、10%十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、10%丙位癸内酯、乙醇均匀混合即得到薰衣草香精。得到的香精香气新鲜，凉香韵稍重，具有薰衣草的特征香气。 Linalyl acetate, linalool, bornyl acetate, terpineyl acetate, borneol with a concentration of 10% by mass, thyme oil, bergamot oil, 1% gerpon pyrazine, methyllavenderone, lavender Oil, Geraniol, Geranyl Acetate, Benzyl Acetate, Amyl Cinnamaldehyde, Neroli, Orange Leaf Oil, Ethyl Naphthalene, Artemisia Oil, Isoamyl Salicylate, Gardeninal, 10 % elequinone, claret oil, musk ketone, musk jale, bergamot citral, 10% dodecyl cyanide, cedaryl acetate, isolongifolanone, synthetic moss, jasmonal, 10% gamma-decane Ester and ethanol are evenly mixed to obtain lavender essence. The obtained essence has a fresh aroma, slightly heavier cool aroma, and has the characteristic aroma of lavender.
上述的一种水性油墨用薰衣草香精的制备方法包括如下步骤： The preparation method of above-mentioned a kind of water-based ink lavender essence comprises the steps:
（1）、在150ml烧杯中加入50g的复合改性低聚糖，再加入40g的去离子水，开启搅拌，使复合改性低聚糖均匀的分散在水相中，形成复合改性低聚糖分散液； (1) Add 50g of compound modified oligosaccharides into a 150ml beaker, then add 40g of deionized water, start stirring, so that the compound modified oligosaccharides are evenly dispersed in the water phase to form a compound modified oligosaccharides sugar dispersion;
（2）、称取10g薰衣草香精，滴加到步骤（1）所得的复合改性低聚糖分散液中，继续搅拌，使香精分散均匀，并使复合改性低聚糖形成对香精分子的包覆，得到可应用于水性油墨的薰衣草纳米胶囊缓释香精。 (2) Weigh 10g of lavender essence, add it dropwise to the compound modified oligosaccharide dispersion obtained in step (1), and continue to stir to make the essence disperse evenly, and make the compound modified oligosaccharide form a bond to the essence molecules. Coating, obtain the lavender nanocapsule slow-release essence that can be applied to water-based ink.
称取薰衣草纳米胶囊缓释香精5g,加到95g水性油墨中，搅拌均匀，得到质量稳定的具有薰衣草特征香气的水性油墨。 Weigh 5 g of lavender nanocapsule slow-release essence, add it to 95 g of water-based ink, stir evenly, and obtain water-based ink with lavender characteristic fragrance with stable quality.
上述所得的薰衣草纳米胶囊缓释香精质量稳定，留香持久，香气强度适中，具有薰衣草的特征香气。 The obtained lavender nanocapsule slow-release essence has stable quality, long-lasting fragrance, moderate fragrance intensity and characteristic fragrance of lavender.
实施例3Example 3
一种水性油墨用薰衣草香精，按重量百分比计算，其原料的组成及含量如下： A kind of lavender essence for water-based ink, calculated by weight percentage, the composition and content of its raw materials are as follows:
薰衣草香精30g(30%)， Lavender essence 30g (30%),
复合改性低聚糖30g(30%)， Compound modified oligosaccharide 30g (30%),
去离子水40g(40%)， 40g (40%) deionized water,
上述的薰衣草香精，按重量百分比计算，其组成及含量如下： Above-mentioned lavender essence, by weight percentage, its composition and content are as follows:
乙酸芳樟酯16g(16%)， Linalyl acetate 16g (16%),
芳樟醇4g(4%)， Linalool 4g (4%),
乙酸龙脑酯4g(4%)， Bornyl acetate 4g (4%),
乙酸松油酯2g(2%)， Terpine acetate 2g (2%),
质量百分比浓度为10%的冰片0.7g(0.7%)， Mass percentage concentration is borneol 0.7g (0.7%) of 10%,
百里香油15g(15%)， Thyme oil 15g (15%),
香柠檬薄荷油3g(3%)， bergamot mint oil 3g (3%),
质量百分比浓度为1%的格蓬吡嗪0.7g(0.7%)， Mass percentage concentration is 0.7g (0.7%) of 1% glycopyrizine,
甲基薰衣草酮2g(2%)， Methyllavandone 2g (2%),
薰衣草油8g(8%)， Lavender oil 8g (8%),
香叶醇6g(6%)， Geraniol 6g (6%),
乙酸香叶酯4g(4%)， Geranyl acetate 4g (4%),
乙酸苄酯4g(4%)， Benzyl acetate 4g (4%),
甲位戊基桂醛2g(2%)， Amyl cinnamaldehyde 2g (2%),
橙花素2g(2%)， Nerolitin 2g (2%),
橙叶油3g(3%)， Orange Leaf Oil 3g (3%),
乙位萘乙醚2g(2%)， Ethyl naphthalene ethyl ether 2g (2%),
艾蒿油1g(1%)， Mugwort Oil 1g (1%),
柳酸异戊酯2g(2%)， Isopentyl salicylate 2g (2%),
栀子醛2g(2%)， Gardenide 2g (2%),
质量百分比浓度为10%的榄青酮0.6g(0.6%)， Mass percentage concentration is 0.6g (0.6%) of 10% elequinone,
香紫苏油2g(2%)， Clare Perilla Oil 2g (2%),
酮麝香2g(2%)， Ketone musk 2g (2%),
佳乐麝香1.5g(1.5%)， Jiale musk 1.5g (1.5%),
香柠檬醛0.7g(0.7%)， Bergamot Citral 0.7g (0.7%),
质量百分比浓度为10%的十二腈0.8g(0.8%)， Mass percent concentration is 10% dodecyl nitrile 0.8g (0.8%),
乙酸柏木酯1.5g(1.5%)， Cedaryl acetate 1.5g (1.5%),
异长叶烷酮2g(2%)， Isophallanone 2g (2%),
合成青苔1.5g(1.5%)， Synthetic moss 1.5g (1.5%),
洋茉莉醛2g(2%)， Jasmonal 2g (2%),
质量百分比浓度为10%的丙位癸内酯1.5g(1.5%)， Mass percent concentration is 1.5g (1.5%) of 10% gamma decanolactone,
乙醇0.5g(0.5%)； Ethanol 0.5g (0.5%);
上述的薰衣草香精的制备方法如下： The preparation method of above-mentioned lavender essence is as follows:
将乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为10%的冰片、百里香油、香柠檬薄荷油、1%格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、10%榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、10%十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、10%丙位癸内酯、乙醇均匀混合即得到薰衣草香精。得到的香精香气新鲜，具有薰衣草的特征香气。 Linalyl acetate, linalool, bornyl acetate, terpineyl acetate, borneol with a concentration of 10% by mass, thyme oil, bergamot oil, 1% gerpon pyrazine, methyllavenderone, lavender Oil, Geraniol, Geranyl Acetate, Benzyl Acetate, Amyl Cinnamaldehyde, Neroli, Orange Leaf Oil, Ethyl Naphthalene, Artemisia Oil, Isoamyl Salicylate, Gardeninal, 10 % elequinone, claret oil, musk ketone, musk jale, bergamot citral, 10% dodecyl cyanide, cedaryl acetate, isolongifolanone, synthetic moss, jasmonal, 10% gamma-decane Ester and ethanol are evenly mixed to obtain lavender essence. The resulting essence has a fresh aroma with a characteristic aroma of lavender.
上述的一种水性油墨用薰衣草香精的制备方法包括如下步骤： The preparation method of above-mentioned a kind of water-based ink lavender essence comprises the steps:
（1）、在150ml烧杯中加入30g的复合改性低聚糖，再加入40g的去离子水，开启搅拌，使复合改性低聚糖均匀的分散在水相中，形成复合改性低聚糖分散液； (1) Add 30g of compound modified oligosaccharides into a 150ml beaker, then add 40g of deionized water, start stirring, so that the compound modified oligosaccharides are evenly dispersed in the water phase to form a compound modified oligosaccharide sugar dispersion;
（2）、称取30g薰衣草香精，滴加到步骤（1）所得的复合改性低聚糖分散液中，继续搅拌，使香精分散均匀，并使复合改性低聚糖形成对香精分子的包覆，得到可应用于水性油墨的薰衣草纳米胶囊缓释香精。 (2) Weigh 30g of lavender essence, add it dropwise to the compound modified oligosaccharide dispersion obtained in step (1), and continue to stir to make the essence disperse evenly, and make the compound modified oligosaccharide form a bond to the essence molecules. Coating, obtain the lavender nanocapsule slow-release essence that can be applied to water-based ink.
称取薰衣草纳米胶囊缓释香精1g,加到99g水性油墨中，搅拌均匀，得到质量稳定的具有薰衣草特征香气的水性油墨。 Weigh 1 g of lavender nanocapsule slow-release essence, add it to 99 g of water-based ink, stir evenly, and obtain water-based ink with lavender characteristic aroma with stable quality.
上述所得的薰衣草纳米胶囊缓释香精质量稳定，留香持久，香气强度大，具有薰衣草的特征香气。 The obtained lavender nanocapsule slow-release essence has stable quality, long-lasting fragrance, high fragrance intensity and characteristic fragrance of lavender.
实施例4Example 4
一种水性油墨用薰衣草香精，按重量百分比计算，其原料的组成及含量如下： A kind of lavender essence for water-based ink, calculated by weight percentage, the composition and content of its raw materials are as follows:
薰衣草香精1g(1%)， Lavender essence 1g (1%),
复合改性低聚糖5g(5%)， Compound modified oligosaccharide 5g (5%),
去离子水94g(94%)， Deionized water 94g (94%),
上述的薰衣草香精，按重量百分比计算，其组成及含量如下： Above-mentioned lavender essence, by weight percentage, its composition and content are as follows:
乙酸芳樟酯15g(15%)， Linalyl acetate 15g (15%),
芳樟醇3g(3%)， Linalool 3g (3%),
乙酸龙脑酯3g(3%)， Bornyl acetate 3g (3%),
乙酸松油酯1g(1%)， Terpine acetate 1g (1%),
质量百分比浓度为10%的冰片0.5g(0.5%)， Mass percentage concentration is borneol 0.5g (0.5%) of 10%,
百里香油20g(20%)， Thyme oil 20g (20%),
香柠檬薄荷油2g(2%)， bergamot mint oil 2g (2%),
质量百分比浓度为1%的格蓬吡嗪0.7g(0.7%)， Mass percentage concentration is 0.7g (0.7%) of 1% glycopyrizine,
甲基薰衣草酮1g(1%)， Methyllavandone 1g (1%),
薰衣草油8g(8%)， Lavender oil 8g (8%),
香叶醇6g(6%)， Geraniol 6g (6%),
乙酸香叶酯4g(4%)， Geranyl acetate 4g (4%),
乙酸苄酯4g(4%)， Benzyl acetate 4g (4%),
甲位戊基桂醛2g(2%)， Amyl cinnamaldehyde 2g (2%),
橙花素2g(2%)， Nerolitin 2g (2%),
橙叶油3g(3%)， Orange Leaf Oil 3g (3%),
乙位萘乙醚2g(2%)， Ethyl naphthalene ethyl ether 2g (2%),
艾蒿油1g(1%)， Mugwort Oil 1g (1%),
柳酸异戊酯2g(2%)， Isopentyl salicylate 2g (2%),
栀子醛2g(2%)， Gardenide 2g (2%),
质量百分比浓度为10%的榄青酮0.6g(0.6%)， Mass percentage concentration is 0.6g (0.6%) of 10% elequinone,
香紫苏油2g(2%)， Clare Perilla Oil 2g (2%),
酮麝香2g(2%)， Ketone musk 2g (2%),
佳乐麝香1.5g(1.5%)， Jiale musk 1.5g (1.5%),
香柠檬醛0.7g(0.7%)， Bergamot Citral 0.7g (0.7%),
质量百分比浓度为10%的十二腈0.8g(0.8%)， Mass percent concentration is 10% dodecyl nitrile 0.8g (0.8%),
乙酸柏木酯1.5g(1.5%)， Cedaryl acetate 1.5g (1.5%),
异长叶烷酮2g(2%)， Isophallanone 2g (2%),
合成青苔1.5g(1.5%)， Synthetic moss 1.5g (1.5%),
洋茉莉醛2g(2%)， Jasmonal 2g (2%),
质量百分比浓度为10%的丙位癸内酯1.5g(1.5%)， Mass percent concentration is 1.5g (1.5%) of 10% gamma decanolactone,
乙醇1.7g(1.7%)； Ethanol 1.7g (1.7%);
上述的薰衣草香精的制备方法如下： The preparation method of above-mentioned lavender essence is as follows:
将乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为10%的冰片、百里香油、香柠檬薄荷油、1%格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、10%榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、10%十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、10%丙位癸内酯、乙醇均匀混合即得到薰衣草香精。得到的香精香气新鲜，百里香药草气略突出，具有薰衣草的特征香气。 Linalyl acetate, linalool, bornyl acetate, terpineyl acetate, borneol with a concentration of 10% by mass, thyme oil, bergamot oil, 1% gerpon pyrazine, methyllavenderone, lavender Oil, Geraniol, Geranyl Acetate, Benzyl Acetate, Amyl Cinnamaldehyde, Neroli, Orange Leaf Oil, Ethyl Naphthalene, Artemisia Oil, Isoamyl Salicylate, Gardeninal, 10 % elequinone, claret oil, musk ketone, musk jale, bergamot citral, 10% dodecyl cyanide, cedaryl acetate, isolongifolanone, synthetic moss, jasmonal, 10% gamma-decane Ester and ethanol are evenly mixed to obtain lavender essence. The obtained essence has a fresh aroma, the herbal aroma of thyme is slightly prominent, and it has the characteristic aroma of lavender.
上述的一种水性油墨用薰衣草香精的制备方法包括如下步骤： The preparation method of above-mentioned a kind of water-based ink lavender essence comprises the steps:
（1）、在150ml烧杯中加入5g的复合改性低聚糖，再加入94g的去离子水，开启搅拌，使复合改性低聚糖均匀的分散在水相中，形成复合改性低聚糖分散液； (1) Add 5g of compound modified oligosaccharides into a 150ml beaker, then add 94g of deionized water, start stirring, so that the compound modified oligosaccharides are evenly dispersed in the water phase to form a compound modified oligosaccharides sugar dispersion;
（2）、称取1g薰衣草香精，滴加到步骤（1）所得的复合改性低聚糖分散液中，继续搅拌，使香精分散均匀，并使复合改性低聚糖形成对香精分子的包覆，得到可应用于水性油墨的薰衣草纳米胶囊缓释香精。 (2) Weigh 1g of lavender essence, add it dropwise to the compound modified oligosaccharide dispersion obtained in step (1), and continue to stir to make the essence disperse evenly, and make the compound modified oligosaccharide form a bond to the essence molecules. Coating, obtain the lavender nanocapsule slow-release essence that can be applied to water-based ink.
称取薰衣草纳米胶囊缓释香精10g,加到90g水性油墨中，搅拌均匀，得到质量稳定的具有薰衣草特征香气的水性油墨。 Weigh 10 g of lavender nanocapsule slow-release essence, add it to 90 g of water-based ink, and stir evenly to obtain water-based ink with lavender characteristic fragrance with stable quality.
上述所得的薰衣草纳米胶囊缓释香精质量稳定，留香持久，具有薰衣草的特征香气，但香气强度稍弱。 The lavender nanocapsule slow-release essence obtained above has stable quality, long-lasting fragrance, and has the characteristic fragrance of lavender, but the fragrance intensity is slightly weak.
实施例5Example 5
一种水性油墨用薰衣草香精，按重量百分比计算，其原料的组成及含量如下： A kind of lavender essence for water-based ink, calculated by weight percentage, the composition and content of its raw materials are as follows:
薰衣草香精10g(10%)， Lavender essence 10g (10%),
复合改性低聚糖55g(5%)， Compound modified oligosaccharide 55g (5%),
去离子水35g(35%)， 35g (35%) deionized water,
上述的薰衣草香精，按重量百分比计算，其组成及含量如下： Above-mentioned lavender essence, by weight percentage, its composition and content are as follows:
乙酸芳樟酯17g(17%)， Linalyl acetate 17g (17%),
芳樟醇5g(5%)， Linalool 5g (5%),
乙酸龙脑酯4g(4%)， Bornyl acetate 4g (4%),
乙酸松油酯3g(3%)， Terpine acetate 3g (3%),
质量百分比浓度为10%的冰片0.5g(0.5%)， Mass percentage concentration is borneol 0.5g (0.5%) of 10%,
百里香油10g(10%)， Thyme oil 10g (10%),
香柠檬薄荷油3g(3%)， bergamot mint oil 3g (3%),
质量百分比浓度为1%的格蓬吡嗪0.7g(0.7%)， Mass percentage concentration is 0.7g (0.7%) of 1% glycopyrizine,
甲基薰衣草酮2g(2%)， Methyllavandone 2g (2%),
薰衣草油8g(8%)， Lavender oil 8g (8%),
香叶醇6g(6%)， Geraniol 6g (6%),
乙酸香叶酯4g(4%)， Geranyl acetate 4g (4%),
乙酸苄酯4g(4%)， Benzyl acetate 4g (4%),
甲位戊基桂醛2g(2%)， Amyl cinnamaldehyde 2g (2%),
橙花素2g(2%)， Nerolitin 2g (2%),
橙叶油3g(3%)， Orange Leaf Oil 3g (3%),
乙位萘乙醚2g(2%)， Ethyl naphthalene ethyl ether 2g (2%),
艾蒿油1g(1%)， Mugwort Oil 1g (1%),
柳酸异戊酯2g(2%)， Isopentyl salicylate 2g (2%),
栀子醛2g(2%)， Gardenide 2g (2%),
质量百分比浓度为10%的榄青酮0.6g(0.6%)， Mass percentage concentration is 0.6g (0.6%) of 10% elequinone,
香紫苏油2g(2%)， Clare Perilla Oil 2g (2%),
酮麝香2g(2%)， Ketone musk 2g (2%),
佳乐麝香1.5g(1.5%)， Jiale musk 1.5g (1.5%),
香柠檬醛0.7g(0.7%)， Bergamot Citral 0.7g (0.7%),
质量百分比浓度为10%的十二腈0.8g(0.8%)， Mass percent concentration is 10% dodecyl nitrile 0.8g (0.8%),
乙酸柏木酯1.5g(1.5%)， Cedaryl acetate 1.5g (1.5%),
异长叶烷酮2g(2%)， Isophallanone 2g (2%),
合成青苔1.5g(1.5%)， Synthetic moss 1.5g (1.5%),
洋茉莉醛2g(2%)， Jasmonal 2g (2%),
质量百分比浓度为10%的丙位癸内酯1g(1%)， Mass percent concentration is 10% gamma decanolactone 1g (1%),
乙醇3.2g(3.2%)； Ethanol 3.2g (3.2%);
上述的薰衣草香精的制备方法如下： The preparation method of above-mentioned lavender essence is as follows:
将乙酸芳樟酯、芳樟醇、乙酸龙脑酯、乙酸松油酯、质量百分比浓度为10%的冰片、百里香油、香柠檬薄荷油、1%格蓬吡嗪、甲基薰衣草酮、薰衣草油、香叶醇、乙酸香叶酯、乙酸苄酯、甲位戊基桂醛、橙花素、橙叶油、乙位萘乙醚、艾蒿油、柳酸异戊酯、栀子醛、10%榄青酮、香紫苏油、酮麝香、佳乐麝香、香柠檬醛、10%十二腈、乙酸柏木酯、异长叶烷酮、合成青苔、洋茉莉醛、10%丙位癸内酯、乙醇均匀混合即得到薰衣草香精。得到的香精香气新鲜，协调、天然感强，具有薰衣草的特征香气。 Linalyl acetate, linalool, bornyl acetate, terpineyl acetate, borneol with a concentration of 10% by mass, thyme oil, bergamot oil, 1% gerpon pyrazine, methyllavenderone, lavender Oil, Geraniol, Geranyl Acetate, Benzyl Acetate, Amyl Cinnamaldehyde, Neroli, Orange Leaf Oil, Ethyl Naphthalene, Artemisia Oil, Isoamyl Salicylate, Gardeninal, 10 % elequinone, claret oil, musk ketone, musk jale, bergamot citral, 10% dodecyl cyanide, cedaryl acetate, isolongifolanone, synthetic moss, jasmonal, 10% gamma-decane Ester and ethanol are evenly mixed to obtain lavender essence. The obtained essence has fresh aroma, coordination and strong natural feeling, and has the characteristic aroma of lavender.
上述的一种水性油墨用薰衣草香精的制备方法包括如下步骤： The preparation method of above-mentioned a kind of water-based ink lavender essence comprises the steps:
（1）、在150ml烧杯中加入55g的复合改性低聚糖，再加入35g的去离子水，开启搅拌，使复合改性低聚糖均匀的分散在水相中，形成复合改性低聚糖分散液； (1) Add 55g of compound modified oligosaccharides into a 150ml beaker, then add 35g of deionized water, start stirring, so that the compound modified oligosaccharides are evenly dispersed in the water phase to form a compound modified oligosaccharide sugar dispersion;
（2）、称取10g薰衣草香精，滴加到步骤（1）所得的复合改性低聚糖分散液中，继续搅拌，使香精分散均匀，并使复合改性低聚糖形成对香精分子的包覆，得到可应用于水性油墨的薰衣草纳米胶囊缓释香精。 (2) Weigh 10g of lavender essence, add it dropwise to the compound modified oligosaccharide dispersion obtained in step (1), and continue to stir to make the essence disperse evenly, and make the compound modified oligosaccharide form a bond to the essence molecules. Coating, obtain the lavender nanocapsule slow-release essence that can be applied to water-based ink.
称取薰衣草纳米胶囊缓释香精5g,加到95g水性油墨中，搅拌均匀，得到质量稳定的具有薰衣草特征香气的水性油墨。 Weigh 5 g of lavender nanocapsule slow-release essence, add it to 95 g of water-based ink, stir evenly, and obtain water-based ink with lavender characteristic fragrance with stable quality.
上述所得的薰衣草纳米胶囊缓释香精质量稳定，留香持久，香气强度适中，具有薰衣草的特征香气，薰衣草天然感强。 The obtained lavender nanocapsule sustained-release essence has stable quality, long-lasting fragrance, moderate fragrance intensity, characteristic fragrance of lavender, and strong natural feeling of lavender.
以上所述内容仅为本发明构思下的基本说明，而根据本发明的技术方案所做的任何等效变换，均属于本发明保护的范围。 The above content is only a basic description of the concept of the present invention, and any equivalent transformation made according to the technical solution of the present invention belongs to the scope of protection of the present invention.
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