CN104687239B - An electronic cigarette liquid rich in ultrafine green tea powder and tea persin - Google Patents

Abstract

The invention discloses a kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea, it is by propylene glycol 50��60 parts by weight, glycerol 10��15 parts, deionized water 7��10 parts, 6��12 parts of the mixture of ultrafine green tea powder and tea training element, tobacco extract 3��10 parts, flavouring essence for tobacco 1��5 part, thickening agent 1��3 part composition. The present invention is absent from high temperature pyrolysis reaction rich in the tobacco juice for electronic smoke of ultrafine green tea powder, is meeting while consumer obtains smoking experience, reduce on self, the impact of other people and environment. Ultrafine green tea powder can be directly appended in electronic cigarette liquid without microencapsulation, effective ingredient dissolution rate is high, add to and the every Sensory quality index of electronic cigarette liquid after in electronic cigarette liquid, can be optimized, improve the pool of adding lustre to of tobacco juice for electronic smoke, again can fresh breath, tea training element plays good antioxidation jointly with ultrafine green tea powder, it is not necessary in ree-oil, auxiliary adds other antioxidants.

Description

An electronic cigarette liquid rich in ultrafine green tea powder and tea persin

technical field

Embodiments of the present invention relate to the field of tobacco, and more specifically, embodiments of the present invention relate to an electronic cigarette liquid rich in ultrafine green tea powder and tea permein.

Background technique

The issue of smoking and health has always been the focus of global medical and health circles. At present, under the macro situation of continuous strengthening of global tobacco control and sluggish economic growth, the world tobacco industry is facing severe challenges. In order to reduce the impact of traditional cigarettes on consumers, smokeless tobacco products represented by snus, heat-not-burn cigarettes and electronic cigarettes have become the mainstream of new tobacco products.

E-cigarettes, or electronic nicotine delivery devices, were invented by the Chinese. At present, foreign tobacco giants are investing heavily in the research and development of related products in the field of electronic cigarettes. E-cigarettes atomize the e-cigarette liquid into aerosol through the atomization device, so that consumers can experience the feeling similar to smoking. Because there is no high-temperature pyrolysis process of tobacco in electronic cigarettes, the tar content is almost zero, there is no visible sidestream smoke, and the impact on the surrounding environment is small, which is gradually recognized by consumers. At present, electronic cigarettes mainly release nicotine and flavor components through atomization of propylene glycol and glycerin, and some electronic cigarettes release nicotine and flavor components through ultrasonically atomized water.

After smoking a cigarette, consumers often leave a lot of tobacco flavor in their mouth, feeling dry and uncomfortable. Therefore, refreshing the mouth is a necessary homework for most smokers after smoking. However, brushing teeth after smoking is limited by the time and place, and the use of chewing gum will also pollute the environment. Therefore, when smoking a cigarette, it is the goal pursued by most smokers to achieve the effect of refreshing the oral cavity.

Tea polyphenols are high-efficiency antioxidants. The solubility of general tea powder is not good, and its active ingredients are difficult to dissolve in large quantities. The application of tea polyphenols in the field of tobacco is limited, while green tea has a fresh taste and is rich in various catechus Tea polyphenols are recognized as safe and efficient antioxidants in the world. In addition, the inventor discovered a substance with particularly significant anti-oxidation effect from the big-leaf tea produced in Xishuangbanna, Yunnan, and successfully extracted the substance, which coordinates with tea polyphenols to achieve a good anti-oxidation effect. Its structure is as follows:

Because tea is rich in tea polyphenols, alkaloids, aromatic substances, etc., the inventor uses the form of ultra-fine green tea powder to mix with tea culture and add it to the e-cigarette liquid, which can not only comprehensively utilize all active substances of green tea, but also It can achieve a high extraction rate, and under the synergistic effect of the high antioxidant tea pecine, it allows e-cigarette consumers to obtain a higher sense of physiological satisfaction while refreshing the mouth.

Contents of the invention

The present invention overcomes the deficiencies of the prior art, and provides an embodiment of an electronic cigarette liquid rich in ultrafine green tea powder and tea persin, in order to improve the taste and quality of the electronic cigarette liquid, and at the same time when smoking a cigarette Freshens the mouth.

In order to solve the above-mentioned technical problems, one embodiment of the present invention adopts the following technical solutions:

An electronic cigarette liquid rich in ultrafine green tea powder and tea peroxide, which consists of the following components in parts by weight:

50-60 parts of propylene glycol, 10-15 parts of glycerin, 7-10 parts of deionized water, 6-12 parts of a mixture of ultra-fine green tea powder and tea pecine, 3-10 parts of tobacco extract, 1-10 parts of tobacco flavor 5 parts, thickener 1 to 3 parts.

A further technical solution is: the electronic cigarette liquid rich in ultrafine green tea powder and tea persimmon consists of the following components in parts by weight:

55-60 parts of propylene glycol, 10-12 parts of glycerin, 7-9 parts of deionized water, 6-10 parts of a mixture of ultra-fine green tea powder and tea pecine, 4-8 parts of tobacco extract, 2-2 parts of tobacco flavor 5 parts, thickener 1 to 3 parts.

According to a preferred embodiment of the present invention, the electronic cigarette liquid rich in ultrafine green tea powder and tea persimmon consists of the following components in parts by weight:

59 parts of propylene glycol, 12 parts of glycerin, 9 parts of deionized water, 6 parts of a mixture of ultrafine green tea powder and tea persimmon, 6 parts of tobacco extract, 5 parts of tobacco essence, and 3 parts of thickener.

According to a preferred embodiment of the present invention, the electronic cigarette liquid rich in ultrafine green tea powder and tea persimmon consists of the following components in parts by weight:

59 parts of propylene glycol, 10 parts of glycerin, 8 parts of deionized water, 10 parts of a mixture of ultrafine green tea powder and tea persimmon, 8 parts of tobacco extract, 2 parts of tobacco essence, and 3 parts of thickener.

A further technical solution is: the mass ratio of the superfine green tea powder and the tea pecine in the mixture of the superfine green tea powder and the tea pecine is 5-8:1.

A further technical solution is: the tobacco extract is an extract of at least one of flue-cured tobacco, air-cured tobacco, burley tobacco, and cigar tobacco.

A further technical solution is: the flavoring essence for tobacco is prepared by stirring and mixing the following components in parts by weight at room temperature: 2-3 parts of Yunyan Absolute, 0.5-1 part of Peruvian extract, ethyl vanillin 0.1 to 3 parts, 3 to 5 parts of 2-hydroxy-2,6,6-trimethylcyclohexanone with a mass concentration of 10%, 0.05 to 0.1 parts of maltol, 0.5 to 1.0 parts of 2-acetylpyrazine, 2 , 0.5-1 part of 3,5-trimethylpyrazine, 1.0-1.5 parts of isoamyl isovalerate, 0.1-0.5 part of menthyl acetate, 0.5-1 part of oxidized isophorone with a mass concentration of 1%, mass 1.0 to 2.0 parts of damascenone with a concentration of 1%, 0.5 to 1 part of damascenone with a mass concentration of 1%, 0.5 to 1 part of macrostigmatrienone with a mass concentration of 1%, 1.0 parts of lavender oil with a mass concentration of 1%. ~2.0 parts, 1.5-2.0 parts of coriander seed oil with a mass concentration of 1%, 7.0-8.0 parts of vanilla bean tincture, 9-11 parts of jujube tincture, 2.0-4.0 parts of lovage tincture, 18.0-22.0 parts of propylene glycol, 40.0-40 parts of ethanol 45.0 servings.

A further technical solution is: the flavoring essence for tobacco is prepared by stirring and mixing the following components in parts by weight at room temperature: 2.2 parts of Yunyan absolute, 0.6 part of Peruvian extract, 0.2 part of ethyl vanillin, mass 4.0 parts of 2-hydroxy-2,6,6-trimethylcyclohexanone with a concentration of 10%, 0.05 parts of maltol, 1.0 parts of 2-acetylpyrazine, and 0.5 parts of 2,3,5-trimethylpyrazine , 1.0 part of isoamyl isovalerate, 0.2 part of menthyl acetate, 0.9 part of oxidized isophorone with a mass concentration of 1%, 1.5 parts of damascenone with a mass concentration of 1%, and dihydrodamascone with a mass concentration of 1%. 0.5 parts, 0.5 parts of macrostigmatrienone with a mass concentration of 1%, 1.0 parts of lavender oil with a mass concentration of 1%, 1.5 parts of coriander seed oil with a mass concentration of 1%, 8.0 parts of vanilla bean tincture, 10 parts of jujube tincture, Lovage tincture 3.0 parts, propylene glycol 20 parts, ethanol 43.35 parts.

A further technical solution is: the preparation method of the tea culture is:

(1) after pulverizing the tea leaves, use 5 to 10 times by weight of an ethanol solution with a concentration of 40% to extract 3 times in a water bath at a temperature of 60° C., each extraction for 2 hours, and the obtained extract is filtered and concentrated to obtain an extract;

(2) Dissolve and filter the extract with hot water, absorb it through the macroporous resin D101, and then use pure water, 10% ethanol water solution, 20% ethanol water solution, and 40% ethanol water solution gradient elution, and collect the elution Liquid, using thin layer chromatography or high performance liquid phase analysis, the part containing the target component is concentrated to obtain a concentrate;

(3) The concentrate is further chromatographed with a molecular sieve filler of dextran gel LH20, then eluted with a 40% aqueous methanol solution, and the eluate is collected, analyzed by thin layer chromatography or high performance liquid phase, and combined Get Cha Peisu. Ethanol concentration refers to the volume fraction of ethanol.

Green tea has a refreshing taste and is rich in various catechins, vitamins, amino acids, caffeine, etc. Among them, tea polyphenols are recognized as safe and efficient antioxidants in the world. The ultrafine green tea powder is emerald green in color, fine in texture and rich in nutrition, which can be effectively mixed with e-cigarette liquid and fully dissolve the active ingredients. Tea Peisu is a natural product with high antioxidant activity contained in some tea leaves. Its structure is composed of gallic acid and quinolinic acid. Tea Peisu has good compatibility with e-liquid, which can adjust the taste of e-liquid and improve the aftertaste, coordination and concentration of e-liquid.

Compared with the prior art, one of the beneficial effects of the present invention is that the e-cigarette liquid rich in ultrafine green tea powder of the present invention does not have high-temperature pyrolysis reaction, so the amount of tar released is almost zero, and it satisfies the needs of consumers to obtain smoking. While feeling, reduce the impact on yourself, others and the environment. At the same time, the ultra-fine green tea powder can be directly added to the e-liquid without microencapsulation. The active ingredients in the ultra-fine green tea powder have a high dissolution rate, which can optimize the smoking of the e-liquid after being added to the e-liquid indicators, improve the color of e-cigarette liquid, and can freshen the breath. Tea Peisu and ultra-fine green tea powder have a good antioxidant effect, and there is no need to add other antioxidants to the e-liquid, which simplifies the composition of the e-liquid.

detailed description

In order to make the object, technical solution and advantages of the present invention more clear, the present invention will be further described in detail below in conjunction with the examples. It should be understood that the specific embodiments described here are only used to explain the present invention, not to limit the present invention.

The essence for tobacco is prepared by stirring and mixing the following components in parts by weight at room temperature: 2.2 parts of Yunyan absolute, 0.6 parts of Peruvian extract, 0.2 parts of ethyl vanillin, and 10% 2-hydroxyl-2 , 4.0 parts of 6,6-trimethylcyclohexanone, 0.05 parts of maltol, 1.0 parts of 2-acetylpyrazine, 0.5 parts of 2,3,5-trimethylpyrazine, 1.0 parts of isoamyl isovalerate , 0.2 part of menthyl acetate, 0.9 part of oxidized isophorone with a mass concentration of 1%, 1.5 parts of damascenone with a mass concentration of 1%, 0.5 part of dihydrodamascone with a mass concentration of 1%, 0.5 part of a mass concentration of damascenone with a mass concentration of 1%. 0.5 parts of stigmatrienone, 1.0 parts of lavender oil with a mass concentration of 1%, 1.5 parts of coriander seed oil with a mass concentration of 1%, 8.0 parts of vanilla bean tincture, 10 parts of jujube tincture, 3.0 parts of lovage tincture, 20 parts of propylene glycol, 43.35 parts of ethanol. This flavoring essence for tobacco is used in following each embodiment.

The preparation of tea Peisu:

(1) After crushing 100g of tea leaves, use 700g of 40% ethanol solution to extract 3 times in a water bath at a temperature of 60° C., each extraction for 2 hours, and the obtained extract is filtered and concentrated to obtain 30 g of extract;

(2) Dissolve and filter the extract with hot water, absorb it through the macroporous resin D101, and then use pure water, 10% ethanol water solution, 20% ethanol water solution, and 40% ethanol water solution gradient elution, and collect the elution liquid, using thin layer chromatography or high performance liquid phase analysis, the part containing the target component was concentrated to obtain 5.5 g of the concentrate;

(3) The concentrate is further chromatographed with a molecular sieve filler of dextran gel LH20, then eluted with a 40% aqueous methanol solution, and the eluate is collected, analyzed by thin layer chromatography or high performance liquid phase, and combined Obtain 0.3 g of tea peisu.

Superfine green tea powder is a commercially available conventional product.

The thickener is a commercially available conventional product in the field of tobacco.

Example 1

In parts by weight, take 59 parts of propylene glycol, 12 parts of glycerin, 9 parts of deionized water, 5 parts of superfine green tea powder, 1 part of tea pecine, 6 parts of flue-cured tobacco extract, 5 parts of tobacco essence, thickener 3 parts are formulated as e-cigarette liquid rich in ultrafine green tea powder and tea peroxide.

Comparative Example 1

In parts by weight, take 65 parts of propylene glycol, 12 parts of glycerin, 9 parts of deionized water, 6 parts of flue-cured tobacco extract, 5 parts of tobacco essence, and 3 parts of thickener to prepare electronic cigarette liquid. Does not contain micronized green tea powder and tea pecine.

Example 2

In parts by weight, get 59 parts of propylene glycol, 10 parts of glycerol, 8 parts of deionized water, 8.5 parts of superfine green tea powder, 1.5 parts of tea pecine, 8 parts of Burley tobacco extract, 2 parts of tobacco essence, and Three parts of the thickener are configured to form an electronic cigarette liquid rich in ultrafine green tea powder and tea peroxide.

Comparative Example 2

In parts by weight, take 66 parts of propylene glycol, 10 parts of glycerin, 8 parts of deionized water, 8 parts of burley tobacco extract, 5 parts of tobacco essence, and 3 parts of thickener to prepare electronic cigarette liquid. The e-liquid does not contain ultra-fine green tea powder and tea pecine.

Take Example 1 and Comparative Example 1 as a group, and Example 2 and Comparative Example 2 as a group to conduct sensory evaluation of electronic cigarettes. The evaluation method refers to Gong Xiaowei’s method (CN201310031800.5). The evaluation standards of various indicators are as follows: Table 1, embodiment 1, 2, the evaluation suction result of comparative example 1, 2 is as table 2:

Table 1 Quantitative description of the 9-point scoring method for individual sensory evaluation indicators

Note: The minimum scoring standard is 0.5.

Table 2 embodiment compares with comparative embodiment sensory evaluation result

As can be seen from Table 2, the sensory evaluation score of Example 1 is 51 points, which is better than that of Comparative Example 1, wherein the aroma, coordination, miscellaneous gas, irritation, and aftertaste of Example 1 are all better than those of Comparative Example 1, especially the aftertaste and coordination, due to the fresh breath of green tea, the aftertaste is significantly improved, and the coordination of the e-cigarette liquid is significantly improved due to the combination of tea permeate and ultra-fine green tea powder in the e-cigarette liquid; the sensory evaluation score of Example 2 Be 50.0, be better than comparative example 2, wherein, embodiment 2 coordination, miscellaneous gas, pungency, aftertaste are better than comparative example 2. In addition, in terms of appearance, the e-cigarette liquid added with ultra-fine green tea powder is green and transparent, with a pleasant color and luster, which stimulates consumers' desire to smoke.

Although the invention has been described herein with reference to a number of illustrative embodiments thereof, it is to be understood that numerous other modifications and implementations can be devised by those skilled in the art which will fall within the scope of the disclosure disclosed herein. within the scope and spirit of the principles. More specifically, within the scope of the disclosure and claims of the present application, various modifications and improvements can be made to the components and/or layout of the subject combination layout. In addition to modifications and improvements in component parts and/or layout, other uses will be apparent to those skilled in the art.

Claims (7)

1. An electronic cigarette liquid rich in ultrafine green tea powder and tea peroxide, characterized in that it consists of the following components by weight: 50-60 parts of propylene glycol, 10-15 parts of glycerin, 7-10 parts of deionized water, 6-12 parts of a mixture of ultra-fine green tea powder and tea pecine, 3-10 parts of tobacco extract, 1-10 parts of tobacco flavor 5 parts, 1-3 parts of thickener; the mass ratio of superfine green tea powder and tea-pearl in the mixture of superfine green tea powder and tea-pearl is 5-8:1; The following components in parts are stirred and mixed at room temperature: 2 to 3 parts of Yunyan absolute, 0.5 to 1 part of Peruvian extract, 0.1 to 3 parts of ethyl vanillin, and 2-hydroxyl-2 , 3-5 parts of 6,6-trimethylcyclohexanone, 0.05-0.1 parts of maltol, 0.5-1.0 parts of 2-acetylpyrazine, 0.5-1 part of 2,3,5-trimethylpyrazine, 1.0-1.5 parts of isoamyl isovalerate, 0.1-0.5 parts of menthyl acetate, 0.5-1 part of oxidized isophorone with a mass concentration of 1%, 1.0-2.0 parts of damascenone with a mass concentration of 1%, and a mass concentration of 1% 0.5 to 1 part of damascenone, 0.5 to 1 part of macrostigmatrienone with a mass concentration of 1%, 1.0 to 2.0 parts of lavender oil with a mass concentration of 1%, and 1.5 to 2.0 parts of coriander seed oil with a mass concentration of 1%. 7.0-8.0 parts of vanilla bean tincture, 9-11 parts of jujube tincture, 2.0-4.0 parts of lovage tincture, 18.0-22.0 parts of propylene glycol, and 40.0-45.0 parts of ethanol. 2. the e-cigarette liquid that is rich in superfine green tea powder and tea persimmon according to claim 1, is characterized in that it is made up of the following components by weight: 55-60 parts of propylene glycol, 10-12 parts of glycerin, 7-9 parts of deionized water, 6-10 parts of a mixture of ultra-fine green tea powder and tea pecine, 4-8 parts of tobacco extract, 2-2 parts of tobacco flavor 5 parts, thickener 1 to 3 parts. 3. the e-cigarette liquid that is rich in superfine green tea powder and tea persimmon according to claim 2, is characterized in that it is made up of the following components by weight: 59 parts of propylene glycol, 12 parts of glycerin, 9 parts of deionized water, 6 parts of a mixture of ultrafine green tea powder and tea persimmon, 6 parts of tobacco extract, 5 parts of tobacco essence, and 3 parts of thickener. 4. the e-cigarette liquid that is rich in superfine green tea powder and tea persimmon according to claim 2, is characterized in that it is made up of the following components by weight: 59 parts of propylene glycol, 10 parts of glycerin, 8 parts of deionized water, 10 parts of a mixture of ultrafine green tea powder and tea persimmon, 8 parts of tobacco extract, 2 parts of tobacco essence, and 3 parts of thickener. 5. The e-cigarette liquid rich in ultrafine green tea powder and tea permeate according to any one of claims 1 to 4, characterized in that the tobacco extract is flue-cured tobacco, air-cured tobacco, burley tobacco, and cigar tobacco at least one of the extracts. 6. The e-cigarette liquid rich in ultrafine green tea powder and tea persin according to any one of claim 1, characterized in that the flavoring essence for tobacco is stirred and mixed at room temperature by the following components in parts by weight Made: 2.2 parts of Yunyan absolute, 0.6 parts of Peruvian extract, 0.2 parts of ethyl vanillin, 4.0 parts of 2-hydroxy-2,6,6-trimethylcyclohexanone with a mass concentration of 10%, 0.05 parts of maltol Parts, 1.0 part of 2-acetylpyrazine, 0.5 part of 2,3,5-trimethylpyrazine, 1.0 part of isoamyl isovalerate, 0.2 part of menthyl acetate, oxidized isophorone with a mass concentration of 1% 0.9 parts, 1.5 parts of damascenone with a mass concentration of 1%, 0.5 parts of dihydrodamascenone with a mass concentration of 1%, 0.5 parts of mastigmatrienone with a mass concentration of 1%, 1.0 parts of lavender oil with a mass concentration of 1%, 1.5 parts of coriander seed oil with a mass concentration of 1%, 8.0 parts of vanilla bean tincture, 10 parts of jujube tincture, 3.0 parts of lovage tincture, 20 parts of propylene glycol, and 43.35 parts of ethanol. 7. The e-cigarette liquid rich in ultrafine green tea powder and tea pecine according to any one of claims 1 to 4, characterized in that the preparation method of the tea pecine is: (1) after pulverizing the tea leaves, use 5 to 10 times by weight of an ethanol solution with a concentration of 40% to extract 3 times in a water bath at a temperature of 60° C., each extraction for 2 hours, and the obtained extract is filtered and concentrated to obtain an extract; (2) Dissolve and filter the extract with hot water, absorb it through the macroporous resin D101, and then use pure water, 10% ethanol water solution, 20% ethanol water solution, and 40% ethanol water solution gradient elution, and collect the elution Liquid, using thin layer chromatography or high performance liquid phase analysis, the part containing the target component is concentrated to obtain a concentrate; (3) The concentrate is further chromatographed with a molecular sieve filler of dextran gel LH20, then eluted with a 40% aqueous methanol solution, and the eluate is collected, analyzed by thin layer chromatography or high performance liquid phase, and combined Get Cha Peisu.