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CL2019000991A1 - Process to obtain lithium carbonate from the spodumene mineral by sulphation with ferrous sulfate at high temperature - Google Patents

Process to obtain lithium carbonate from the spodumene mineral by sulphation with ferrous sulfate at high temperature

Info

Publication number
CL2019000991A1
CL2019000991A1 CL2019000991A CL2019000991A CL2019000991A1 CL 2019000991 A1 CL2019000991 A1 CL 2019000991A1 CL 2019000991 A CL2019000991 A CL 2019000991A CL 2019000991 A CL2019000991 A CL 2019000991A CL 2019000991 A1 CL2019000991 A1 CL 2019000991A1
Authority
CL
Chile
Prior art keywords
sulphation
high temperature
ferrous sulfate
lithium carbonate
obtain lithium
Prior art date
Application number
CL2019000991A
Other languages
Spanish (es)
Inventor
Fuica Igor Wilkomirsky
Luna Fernando Parada
Original Assignee
Univ Concepcion
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Concepcion filed Critical Univ Concepcion
Priority to CL2019000991A priority Critical patent/CL2019000991A1/en
Publication of CL2019000991A1 publication Critical patent/CL2019000991A1/en
Priority to PCT/CL2020/050038 priority patent/WO2020206567A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D15/00Lithium compounds
    • C01D15/08Carbonates; Bicarbonates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D7/00Carbonates of sodium, potassium or alkali metals in general
    • C01D7/06Preparation via sodium or potassium magnesium carbonate
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B1/00Preliminary treatment of ores or scrap
    • C22B1/02Roasting processes
    • C22B1/06Sulfating roasting
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/10Obtaining alkali metals
    • C22B26/12Obtaining lithium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • C22B3/06Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
    • C22B3/08Sulfuric acid, other sulfurated acids or salts thereof
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
CL2019000991A 2019-04-12 2019-04-12 Process to obtain lithium carbonate from the spodumene mineral by sulphation with ferrous sulfate at high temperature CL2019000991A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CL2019000991A CL2019000991A1 (en) 2019-04-12 2019-04-12 Process to obtain lithium carbonate from the spodumene mineral by sulphation with ferrous sulfate at high temperature
PCT/CL2020/050038 WO2020206567A1 (en) 2019-04-12 2020-04-09 Process for obtaining lithium carbonate from spodumene ore by sulphation with ferrous sulphate at high temperature

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CL2019000991A CL2019000991A1 (en) 2019-04-12 2019-04-12 Process to obtain lithium carbonate from the spodumene mineral by sulphation with ferrous sulfate at high temperature

Publications (1)

Publication Number Publication Date
CL2019000991A1 true CL2019000991A1 (en) 2019-08-30

Family

ID=67769705

Family Applications (1)

Application Number Title Priority Date Filing Date
CL2019000991A CL2019000991A1 (en) 2019-04-12 2019-04-12 Process to obtain lithium carbonate from the spodumene mineral by sulphation with ferrous sulfate at high temperature

Country Status (2)

Country Link
CL (1) CL2019000991A1 (en)
WO (1) WO2020206567A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115180639B (en) * 2022-08-08 2023-12-15 湖南五创循环科技有限公司 Method for purifying and removing impurities from lithium sulfate solution and producing lithium carbonate
CN116078344B (en) * 2023-03-16 2023-08-01 南京工程学院 A kind of whisker-shaped spinel-type magnesium-aluminum oxide lithium ion sieve salt lake adsorbent for lithium extraction and preparation method thereof
KR20250089788A (en) * 2023-12-12 2025-06-19 포스코홀딩스 주식회사 Separating method of lithium carbonate

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3017243A (en) * 1958-08-11 1962-01-16 Dept Of Mines Method of producing lithium carbonate from spodumene
AU2010341402B2 (en) * 2010-01-07 2014-01-30 Tianqi Lithium Corporation Process for the production of lithium carbonate
FI122831B (en) * 2010-05-25 2012-07-31 Outotec Oyj Procedure for treatment of spodum
CN107758705B (en) * 2017-12-18 2019-06-28 江西九岭新能源有限公司 Process for extracting lithium carbonate from lepidolite mica

Also Published As

Publication number Publication date
WO2020206567A1 (en) 2020-10-15

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