CH204118A - Process for the production of a valuable substance which is active in the boil capillary. - Google Patents
Process for the production of a valuable substance which is active in the boil capillary.Info
- Publication number
- CH204118A CH204118A CH204118DA CH204118A CH 204118 A CH204118 A CH 204118A CH 204118D A CH204118D A CH 204118DA CH 204118 A CH204118 A CH 204118A
- Authority
- CH
- Switzerland
- Prior art keywords
- production
- capillary
- propane
- active
- boil
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 5
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 239000000126 substance Substances 0.000 title description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 6
- 239000000194 fatty acid Substances 0.000 claims description 6
- 229930195729 fatty acid Natural products 0.000 claims description 6
- 150000004665 fatty acids Chemical class 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 6
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical class [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 4
- 150000001447 alkali salts Chemical class 0.000 claims description 4
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 235000008733 Citrus aurantifolia Nutrition 0.000 claims description 2
- 235000011941 Tilia x europaea Nutrition 0.000 claims description 2
- 239000002253 acid Substances 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 claims description 2
- 239000013543 active substance Substances 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 claims description 2
- 230000001804 emulsifying effect Effects 0.000 claims description 2
- 239000004571 lime Substances 0.000 claims description 2
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 238000009736 wetting Methods 0.000 claims description 2
- 235000019864 coconut oil Nutrition 0.000 claims 1
- 239000003240 coconut oil Substances 0.000 claims 1
- 239000001294 propane Substances 0.000 claims 1
- 235000013162 Cocos nucifera Nutrition 0.000 description 3
- 244000060011 Cocos nucifera Species 0.000 description 3
- 229940114930 potassium stearate Drugs 0.000 description 2
- ANBFRLKBEIFNQU-UHFFFAOYSA-M potassium;octadecanoate Chemical compound [K+].CCCCCCCCCCCCCCCCCC([O-])=O ANBFRLKBEIFNQU-UHFFFAOYSA-M 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 1
- DCXXMTOCNZCJGO-UHFFFAOYSA-N Glycerol trioctadecanoate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C309/00—Sulfonic acids; Halides, esters, or anhydrides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Description
Verfahren zur Herstellung eines wertvollen kochkapillaraktiven Stoffes. Zur Herstellung eines wertvollen hoch kapillaraktiven Stoffes kann nach dem Haupt patent durch Umsetzung von 3-chlor-2-oxy- propan-l-sulfonsaurem Natrium mit Kalium- stearat intermediär gebildetes 2,3-oxido-pro- pan-l-sulfonsaures Natrium mit dem bei dieser Umsetzung gleichzeitig freigewordenen Stearin zu einem bei der Verarbeitung von Textilien nützlichen Endstoff umgesetzt wer den.
Gemäss dem vorliegenden Verfahren wird an Stelle des Kaliumstearats ein Al kalisalz des dem gokosöl entsprechenden Fettsäuregemisches verwendet.
Der Endstoff zeichnet sich durch ein hervorragendes Netz-, Wasch-, Reinigungs-, Emulgier- und Dispergiervermögen und durch eine ebensolche Säure-, Bittersalz- und Kalk beständigkeit aus.
Gemäss einem Ausführungsbeispiel des Verfahrens werden 10 Teile feingepulvertes trockenes Kalisalz oder die entsprechende Menge eines andern Alkalisalzes der Kokos- fettsäuren mit 8 Teilen wasserfreiem 3-Chlor- 2-oxy-propan-l-sulfonsaurem Natrium gut vermischt und so lange auf 135-1450 C.
erhitzt; bis eine Probe in Wasser gelöst auf Zusatz von verdünnter Salzsäure klar bleibt Bei der Reaktion von 3-Chlor-2-oxy-propan- 1-sulfonsaurem Natrium mit dem Alkalisalz der Kokosfettsäuren bildet sich intermediär 2,3-oxido-propan-l-sulfonsaures Natrium, wel ches mit den im Reaktionsgemisch sich gleich zeitig bildenden Kokosfettsäuren umgesetzt wird. Die Verbindung stellt ein farbloses Pulver dar, das sich den eingangs erwähnten Eigenschaften durch ein vorzügliches Schaum vermögen auszeichnet.
Process for the production of a valuable substance which is active in the boil capillary. According to the main patent, to produce a valuable, highly capillary-active substance, 2,3-oxido-propane-l-sulfonic acid sodium formed as an intermediate by reacting sodium 3-chloro-2-oxypropane-1-sulfonic acid with potassium stearate can be added the stearin released at the same time during this implementation to a useful end product in the processing of textiles who implemented the.
According to the present process, instead of the potassium stearate, an alkali salt of the fatty acid mixture corresponding to the goos oil is used.
The end product is characterized by excellent wetting, washing, cleaning, emulsifying and dispersing properties and by being resistant to acids, Epsom salts and lime.
According to one embodiment of the method, 10 parts of finely powdered dry potassium salt or the corresponding amount of another alkali salt of coconut fatty acids are mixed well with 8 parts of anhydrous 3-chloro-2-oxy-propane-1-sulfonic acid and kept at 135-1450 ° C. .
heated; until a sample dissolved in water remains clear after the addition of dilute hydrochloric acid. During the reaction of sodium 3-chloro-2-oxy-propane-1-sulphonic acid with the alkali salt of coconut fatty acids, 2,3-oxido-propane-1-sulphonic acid is formed as an intermediate Sodium, which is reacted with the coconut fatty acids which are formed at the same time in the reaction mixture. The compound is a colorless powder, which is characterized by the properties mentioned at the beginning by an excellent foam capacity.
Claims (1)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE204118X | 1935-11-05 | ||
| CH195069T | 1936-10-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CH204118A true CH204118A (en) | 1939-04-15 |
Family
ID=25722719
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CH204118D CH204118A (en) | 1935-11-05 | 1936-10-02 | Process for the production of a valuable substance which is active in the boil capillary. |
Country Status (1)
| Country | Link |
|---|---|
| CH (1) | CH204118A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2427577A (en) * | 1945-03-01 | 1947-09-16 | Colgate Palmolive Peet Co | Production of ether sulphonates |
-
1936
- 1936-10-02 CH CH204118D patent/CH204118A/en unknown
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2427577A (en) * | 1945-03-01 | 1947-09-16 | Colgate Palmolive Peet Co | Production of ether sulphonates |
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