CA2816195C - Procede de pyrolyse aqueuse et appareil permettant d'obtenir un liquide de pyrolyse dans la plage du carburant diesel - Google Patents
Procede de pyrolyse aqueuse et appareil permettant d'obtenir un liquide de pyrolyse dans la plage du carburant diesel Download PDFInfo
- Publication number
- CA2816195C CA2816195C CA2816195A CA2816195A CA2816195C CA 2816195 C CA2816195 C CA 2816195C CA 2816195 A CA2816195 A CA 2816195A CA 2816195 A CA2816195 A CA 2816195A CA 2816195 C CA2816195 C CA 2816195C
- Authority
- CA
- Canada
- Prior art keywords
- char
- organic matter
- reactor
- slurry
- solid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 238000000354 decomposition reaction Methods 0.000 title claims abstract description 41
- 239000007788 liquid Substances 0.000 title claims abstract description 30
- 238000000034 method Methods 0.000 title claims description 43
- 238000000197 pyrolysis Methods 0.000 title description 7
- 239000002283 diesel fuel Substances 0.000 title description 6
- 239000005416 organic matter Substances 0.000 claims abstract description 30
- 239000004215 Carbon black (E152) Substances 0.000 claims abstract description 19
- 229930195733 hydrocarbon Natural products 0.000 claims abstract description 19
- 150000002430 hydrocarbons Chemical class 0.000 claims abstract description 19
- 239000002002 slurry Substances 0.000 claims abstract description 18
- 239000003054 catalyst Substances 0.000 claims abstract description 17
- 238000006243 chemical reaction Methods 0.000 claims abstract description 6
- 230000000694 effects Effects 0.000 claims abstract description 6
- 238000012546 transfer Methods 0.000 claims abstract description 6
- 230000003197 catalytic effect Effects 0.000 claims abstract description 5
- 239000012223 aqueous fraction Substances 0.000 claims abstract description 3
- 238000001027 hydrothermal synthesis Methods 0.000 claims abstract description 3
- 239000007787 solid Substances 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 239000003921 oil Substances 0.000 claims description 14
- 239000002028 Biomass Substances 0.000 claims description 8
- 239000000295 fuel oil Substances 0.000 claims description 8
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical class O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 7
- 238000009835 boiling Methods 0.000 claims description 6
- 229910021536 Zeolite Inorganic materials 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 238000002360 preparation method Methods 0.000 claims description 5
- 239000010457 zeolite Substances 0.000 claims description 5
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- 239000002699 waste material Substances 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 239000002480 mineral oil Substances 0.000 claims description 3
- 235000010446 mineral oil Nutrition 0.000 claims description 3
- 239000010801 sewage sludge Substances 0.000 claims description 3
- 241001465754 Metazoa Species 0.000 claims description 2
- 230000005494 condensation Effects 0.000 claims description 2
- 239000003925 fat Substances 0.000 claims description 2
- 239000004033 plastic Substances 0.000 claims description 2
- 229920003023 plastic Polymers 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims description 2
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 3
- 239000002245 particle Substances 0.000 claims 3
- 150000004679 hydroxides Chemical class 0.000 claims 2
- 238000002604 ultrasonography Methods 0.000 claims 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims 1
- 239000000920 calcium hydroxide Substances 0.000 claims 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims 1
- 235000011116 calcium hydroxide Nutrition 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 241000196324 Embryophyta Species 0.000 description 10
- 239000007789 gas Substances 0.000 description 9
- 238000005516 engineering process Methods 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 238000011160 research Methods 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 4
- 235000011613 Pinus brutia Nutrition 0.000 description 4
- 241000018646 Pinus brutia Species 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 4
- 239000012263 liquid product Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 3
- 239000000292 calcium oxide Substances 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 229910000000 metal hydroxide Inorganic materials 0.000 description 3
- 239000012071 phase Substances 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 229910001038 basic metal oxide Inorganic materials 0.000 description 2
- 239000010779 crude oil Substances 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 239000011368 organic material Substances 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000011282 treatment Methods 0.000 description 2
- 229910000323 aluminium silicate Inorganic materials 0.000 description 1
- -1 aluminosilicate compound Chemical class 0.000 description 1
- 239000010828 animal waste Substances 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 239000012075 bio-oil Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 239000010791 domestic waste Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000010800 human waste Substances 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000010335 hydrothermal treatment Methods 0.000 description 1
- 239000002440 industrial waste Substances 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 239000010815 organic waste Substances 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000012429 reaction media Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000011949 solid catalyst Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 230000001052 transient effect Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/10—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal from rubber or rubber waste
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
- C10G1/08—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts
- C10G1/083—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal with moving catalysts in the presence of a solvent
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/10—Feedstock materials
- C10G2300/1011—Biomass
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P30/00—Technologies relating to oil refining and petrochemical industry
- Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
La conversion de matière organique en produits dhydrocarbures valorisés comprend létape de décomposition de la matière organique en du liquide, du produit de carbonisation et du gaz à laide dune méthode hydrothermique catalytique rapide ayant une efficacité améliorée grâce à un transfert élevé dénergie locale par un effet de cavitation. La matière organique et des catalyseurs sont alimentés dans un réacteur de décomposition hydrothermique pour décomposer la matière organique en gaz, en vapeurs et en produit de carbonisation, le réacteur utilisant le transfert élevé dénergie locale par effet de cavitation. Le réacteur fonctionne à des températures denviron 200 °C à 380 °C et présente un temps de séjour denviron 1 à 60 minutes. Le produit est séparé en une boue lourde de produit de carbonisation et dhuile, en vapeurs et en gaz, les vapeurs étant ensuite condensées et séparées en partie aqueuse et une partie dhydrocarbures. Une partie de la boue de produit de carbonisation est recyclée en chambre de cavitation et le produit de carbonisation excédentaire est sorti de la chambre de décomposition.
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA2816195A CA2816195C (fr) | 2013-05-22 | 2013-05-22 | Procede de pyrolyse aqueuse et appareil permettant d'obtenir un liquide de pyrolyse dans la plage du carburant diesel |
| PCT/EP2014/060562 WO2014187910A2 (fr) | 2013-05-22 | 2014-05-22 | Procédé et appareil de décomposition hydrothermique permettant de fabriquer un liquide de pyrolyse de type carburant diesel |
| CN201480013553.9A CN105121604B (zh) | 2013-05-22 | 2014-05-22 | 用于制造柴油燃料范围内的热解液体的水热分解方法和设备 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA2816195A CA2816195C (fr) | 2013-05-22 | 2013-05-22 | Procede de pyrolyse aqueuse et appareil permettant d'obtenir un liquide de pyrolyse dans la plage du carburant diesel |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CA2816195A1 CA2816195A1 (fr) | 2014-11-22 |
| CA2816195C true CA2816195C (fr) | 2021-11-02 |
Family
ID=50771299
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2816195A Active CA2816195C (fr) | 2013-05-22 | 2013-05-22 | Procede de pyrolyse aqueuse et appareil permettant d'obtenir un liquide de pyrolyse dans la plage du carburant diesel |
Country Status (3)
| Country | Link |
|---|---|
| CN (1) | CN105121604B (fr) |
| CA (1) | CA2816195C (fr) |
| WO (1) | WO2014187910A2 (fr) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106315578B (zh) * | 2016-08-19 | 2018-08-03 | 华中科技大学 | 一种联产超级活性炭和液体产品的系统及方法 |
| CN108218160A (zh) * | 2018-02-02 | 2018-06-29 | 中国科学院生态环境研究中心 | 一种高压水热及循环流化床热解辅助的污泥快速无害化处理工艺 |
| CN109569476B (zh) * | 2018-10-24 | 2023-07-04 | 浙江海洋大学 | 淡水鱼废弃物制备生物质油的方法 |
| EE05860B1 (et) * | 2021-01-17 | 2023-11-15 | Jüri LIIV | Biomassi hüdrotermilise veeldamise ja gaasistamise meetod ning süsteem |
| NL2027380B1 (nl) | 2021-01-25 | 2022-08-12 | Bintell B V | Werkwijze voor het onder hoge druk en temperatuur in een waterige omgeving behandelen van een organisch uitgangsmateriaal. |
| CN114149167B (zh) * | 2021-12-20 | 2024-02-06 | 黑龙江省科学院高技术研究院 | 一种空化技术处理剩余污泥释放内碳源处理装置及方法 |
| KR20240164904A (ko) * | 2022-03-22 | 2024-11-21 | 레이턴트 에너지 리미티드 | 플라스틱 폐기물 전환을 위한 통합 프로세스 |
| CN118774706B (zh) * | 2024-07-19 | 2025-03-04 | 西南石油大学 | 一种稠油热采注汽装置及稠油热采方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5914027A (en) * | 1994-09-12 | 1999-06-22 | Thermtech A/S | Thermo-mechanical cracking and hydrogenation |
| DE102006052995B4 (de) * | 2006-11-10 | 2008-12-18 | Tschirner, Erhard, Dr. | Verfahren zur Herstellung von Gasöl aus kohlenwasserstoffhaltigen organischen Reststoffen und nachwachsenden Rohstoffen durch Reaktionsführung und Energieeintrag mittels prozeßintegrierter Kavitation/Friktion |
| FR2929287A1 (fr) * | 2008-03-28 | 2009-10-02 | Europ Ltd | Procede d'obtention d'hydrocarbures liquides. |
| EP2350244A1 (fr) * | 2008-10-14 | 2011-08-03 | Kai Bioenergy Corporation | Extraction hydrodynamique d huiles à partir de cultures photosynthétiques |
| EP2432854A4 (fr) * | 2009-05-15 | 2014-01-29 | Ausbiodiesel Pty Ltd | Procédé et appareil permettant de fabriquer un carburant |
| CN103080274A (zh) * | 2010-07-26 | 2013-05-01 | 埃米尔·A·J·维泽尔-林哈特 | 由生物质/塑料混合物制备燃料的系统和方法 |
-
2013
- 2013-05-22 CA CA2816195A patent/CA2816195C/fr active Active
-
2014
- 2014-05-22 WO PCT/EP2014/060562 patent/WO2014187910A2/fr not_active Ceased
- 2014-05-22 CN CN201480013553.9A patent/CN105121604B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN105121604B (zh) | 2018-05-18 |
| CN105121604A (zh) | 2015-12-02 |
| WO2014187910A3 (fr) | 2015-07-23 |
| CA2816195A1 (fr) | 2014-11-22 |
| WO2014187910A2 (fr) | 2014-11-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EEER | Examination request |
Effective date: 20180425 |