CA2863773A1 - A process for producing a powder comprising an extruded carrier with an active compound - Google Patents
A process for producing a powder comprising an extruded carrier with an active compound Download PDFInfo
- Publication number
- CA2863773A1 CA2863773A1 CA2863773A CA2863773A CA2863773A1 CA 2863773 A1 CA2863773 A1 CA 2863773A1 CA 2863773 A CA2863773 A CA 2863773A CA 2863773 A CA2863773 A CA 2863773A CA 2863773 A1 CA2863773 A1 CA 2863773A1
- Authority
- CA
- Canada
- Prior art keywords
- active compound
- powder
- producing
- extruder
- carrier
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 150000001875 compounds Chemical class 0.000 title abstract 4
- 239000000843 powder Substances 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- 239000004615 ingredient Substances 0.000 abstract 3
- 238000001816 cooling Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C9/00—Fertilisers containing urea or urea compounds
- C05C9/02—Fertilisers containing urea or urea compounds containing urea-formaldehyde condensates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/49—Phosphorus-containing compounds
- C08K5/5399—Phosphorus bound to nitrogen
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/20—Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
- Y02P60/21—Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Pest Control & Pesticides (AREA)
- Health & Medical Sciences (AREA)
- Soil Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Glanulating (AREA)
- Medicinal Preparation (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Fertilizers (AREA)
Abstract
This invention provides processes for forming powders comprising at least one active compound and at least one carrier. The processes comprise (i) heating at least one active compound to at least its melting point or softening point; and (ii) in an extruder, combining at least the at least one active compound with at least one carrier, to form combined ingredients, and cooling the combined ingredients as they pass through the extruder, such that the combined ingredients exit the extruder at about ambient temperature in the form of a powder having particles sized so that about 95 wt% or more of the powder passes through a screen of about 8 standard U.S. mesh.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261598472P | 2012-02-14 | 2012-02-14 | |
| US61/598,472 | 2012-02-14 | ||
| PCT/US2013/026189 WO2013123229A1 (en) | 2012-02-14 | 2013-02-14 | A process for producing a powder comprising an extruded carrier with an active compound |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA2863773A1 true CA2863773A1 (en) | 2013-08-22 |
Family
ID=47843392
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA2863773A Abandoned CA2863773A1 (en) | 2012-02-14 | 2013-02-14 | A process for producing a powder comprising an extruded carrier with an active compound |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20150031786A1 (en) |
| EP (1) | EP2814318A1 (en) |
| JP (1) | JP2015513452A (en) |
| CN (1) | CN104254248A (en) |
| CA (1) | CA2863773A1 (en) |
| WO (1) | WO2013123229A1 (en) |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10173935B2 (en) | 2011-12-12 | 2019-01-08 | Rhodia Operations | Solvent systems of N-alkyl thiophosphoric triamides and methods of use in agricultural applications |
| US9682894B2 (en) | 2012-08-15 | 2017-06-20 | Koch Agronomic Services, Llc | Compositions of urea formaldehyde particles and methods of making thereof |
| MX2015001958A (en) * | 2012-08-15 | 2015-10-12 | Koch Agronomic Services Llc | Improved compositions of substantially spherical particles. |
| EP2935159B1 (en) | 2012-12-20 | 2019-02-27 | Rhodia Operations | Liquid dicyandiamide and/or alkyl thiophosphoric triamide compositions and their use in agricultural applications |
| AR097433A1 (en) * | 2013-08-23 | 2016-03-16 | Koch Agronomic Services Llc | COMPOSITION OF UREASA INHIBITOR AND A NON-UFP SOLID VEHICLE |
| US20160219829A1 (en) * | 2013-09-06 | 2016-08-04 | 7905122 Canada Inc. | Anti-odor material for animal litters using phosphorotriamides in powder form |
| EP3099651A1 (en) | 2014-01-31 | 2016-12-07 | Saudi Basic Industries Corporation | Fertilizer capsule comprising one or more cores and method of making same |
| US10974999B2 (en) * | 2014-05-02 | 2021-04-13 | Gary David McKnight | Increased longevity of the nitrogen content of soil through improved liquid delivery formulations of nitrification inhibitors designed for urea and manure based fertilizers |
| EP4474370A3 (en) | 2014-05-05 | 2025-02-19 | SABIC Global Technologies B.V. | Coated granular fertilizers, methods of manufacture thereof, and uses |
| CA2965302C (en) | 2014-10-21 | 2023-06-13 | Rhodia Operations | Improved solvent systems for dicyandiamide and/or alkyl thiophosphoric triamide and use in agricultural applications |
| WO2016070184A1 (en) | 2014-10-31 | 2016-05-06 | Koch Agronomic Services, Llc | Nitrification inhibitor compositions and methods of making thereof |
| WO2017013573A1 (en) | 2015-07-20 | 2017-01-26 | Sabic Global Technologies B.V. | Fertilizer composition and methods of making and using same |
| BR112018001196B1 (en) | 2015-07-20 | 2021-10-26 | Sabic Global Technologies B.V. | FERTILIZER CORE PARTICLE, FERTILIZER GRAIN, AND, METHOD FOR PREPARING A FERTILIZER CORE PARTICLE |
| MY175600A (en) * | 2015-07-24 | 2020-07-01 | Koch Agronomic Services Llc | Composition containing n-(n-butyl) thiophosphoric triamide adducts and reaction products |
| EP3337774B1 (en) | 2015-08-17 | 2023-12-06 | Specialty Operations France | High temperature amine-stabilized dcd and/or alkyl thiophosphoric triamide solvent systems and use in agricultural applications |
| BR112018009872B1 (en) | 2015-11-16 | 2022-11-16 | Sabic Global Technologies B.V. | MANUFACTURING PROCESS OF A COATED FERTILIZER |
| CN108473383B (en) | 2015-11-16 | 2022-07-01 | 科氏农艺服务有限责任公司 | Composition containing N-n-butylthiophosphoric triamide adduct and reaction product |
| CN108349828A (en) | 2015-11-16 | 2018-07-31 | 沙特基础工业全球技术有限公司 | Coated granular fertilizer, its manufacturing method and application thereof |
| EP3196180A1 (en) | 2016-01-19 | 2017-07-26 | Borealis Chimie SAS | Method for obtaining at least one urea-based fertilizer composition |
| CN108602730A (en) | 2016-02-08 | 2018-09-28 | 沙特基础工业全球技术有限公司 | Method for preparing fertilizer seed core |
| BR112019010430A2 (en) * | 2017-01-19 | 2019-09-03 | Koch Agronomic Services Llc | optimized stability of urease inhibitor-containing compositions |
| BR112019014952A2 (en) | 2017-01-20 | 2020-04-07 | Koch Agronomic Services Llc | composition containing reaction products and n- (n-butyl) -thiophosphoric triamide adducts |
| WO2018193358A1 (en) | 2017-04-19 | 2018-10-25 | Sabic Global Technologies B.V. | Enhanced efficiency fertilizer with urease inhibitor and nitrification inhibitor in separate particles |
| AU2018255907B2 (en) | 2017-04-19 | 2023-02-02 | SABIC Agri-Nutrients Company | Enhanced efficiency fertilizer with urease inhibitor and nitrification inhibitor separated within the same particle |
| WO2018193345A1 (en) | 2017-04-20 | 2018-10-25 | Sabic Global Technologies B.V. | Enhanced efficiency fertilizer with embedded powder composition |
| AU2018313067B2 (en) | 2017-08-09 | 2024-02-08 | SABIC Agri-Nutrients Company | Extruded fertilizer granules with urease and/or nitrification inhibitors |
| CN109534936A (en) * | 2018-12-29 | 2019-03-29 | 河南心连心化肥有限公司 | A kind of multiple slow-release stable urea of high dispersive, process units and production technology |
| CN109912339B (en) * | 2019-02-15 | 2021-10-22 | 金正大诺泰尔化学有限公司 | A stable nitrogen fertilizer synergist and its preparation method and application |
Family Cites Families (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4101521A (en) | 1969-09-12 | 1978-07-18 | Ciba-Geigy Ag | Process for the manufacture of highly disperse solids consisting of crosslinked urea-formaldehyde polycondensation products |
| JPH06328449A (en) * | 1993-05-25 | 1994-11-29 | Sekisui Chem Co Ltd | Raw material supplying apparatus |
| US5704555A (en) * | 1993-08-02 | 1998-01-06 | Illinois Institute Of Technology | Single-screw extruder for solid state shear extrusion pulverization and method |
| US5698003A (en) * | 1995-12-19 | 1997-12-16 | Imc-Agrico Company | Formulation for fertilizer additive concentrate |
| US6013272A (en) * | 1996-12-19 | 2000-01-11 | Valent U.S.A. Corporation | Chemically stable, insecticidally active phosphoroamidothioate pellet compositions and methods for their manufacture |
| DE19721467A1 (en) * | 1997-05-22 | 1998-11-26 | Basf Ag | Process for the preparation of small-scale preparations of biologically active substances |
| JP2002053382A (en) * | 2000-08-08 | 2002-02-19 | Chisso Corp | Fertilizer |
| JP3656957B2 (en) * | 2001-01-16 | 2005-06-08 | 株式会社神戸製鋼所 | Biaxial continuous kneader and kneading method using the same |
| WO2004047974A1 (en) * | 2002-11-26 | 2004-06-10 | Universiteit Gent | Process and apparatus for continuous wet granulation of power material |
| US20050187123A1 (en) * | 2004-02-20 | 2005-08-25 | Shulong Li | Composition for removal of odors and contaminants from carpet and method |
| JP2006321669A (en) * | 2005-05-17 | 2006-11-30 | Chisso Corp | Granular organic slow-release nitrogenous fertilizer and crop cultivation method using the fertilizer |
| WO2007087180A2 (en) * | 2006-01-12 | 2007-08-02 | Agrotain International, L.L.C. | Additive containing n-(n-butyl) thiophosphoric triamide for urea-based fertilizer |
| EP1820788A1 (en) * | 2006-02-16 | 2007-08-22 | BASF Aktiengesellschaft | Preparations with improved urease-inhibiting properties and those preparations containing urea based fertilizers. |
| DK2001938T3 (en) * | 2006-03-31 | 2016-08-01 | Albemarle Corp | Process for the preparation of coated urea-formaldehyde polymers |
| WO2008002503A2 (en) * | 2006-06-23 | 2008-01-03 | Agrotain International, L.L.C. | Solid urea fertilizer |
| DK2046115T3 (en) * | 2006-07-26 | 2015-08-24 | Dow Agrosciences Llc | HERBICIDE COMPOSITIONS |
| JP2008114566A (en) * | 2006-11-08 | 2008-05-22 | Ngk Insulators Ltd | Screw type extruder |
| ES2841111T3 (en) * | 2007-05-23 | 2021-07-07 | Int Paper Co | Compositions and particles containing stabilized and / or activated cellulosic fibers and urease inhibitors, as well as methods of preparation and use of these |
| US20120148752A1 (en) * | 2008-09-12 | 2012-06-14 | Albemarle Corporation | Process for coating an active ingredient with a urea-formaldehyde polymer |
| JP5618266B2 (en) * | 2009-02-10 | 2014-11-05 | 国立大学法人高知大学 | Pesticides against Hemiptera pests, Thrips pests, or Mite pests |
| US20100206031A1 (en) * | 2009-02-17 | 2010-08-19 | Whitehurst Associates, Inc. | Amino alcohol solutions of N-(n-butyl)thiophosphoric triamide (NBPT) and urea fertilizers using such solutions as urease inhibitors |
| WO2011095314A2 (en) * | 2010-02-03 | 2011-08-11 | Grünenthal GmbH | Preparation of a powdery pharmaceutical composition by means of an extruder |
| WO2012009489A2 (en) * | 2010-07-15 | 2012-01-19 | Dow Agrosciences Llc | Solid herbicide compositions with built-in adjuvant |
-
2013
- 2013-02-14 US US14/376,796 patent/US20150031786A1/en not_active Abandoned
- 2013-02-14 JP JP2014556836A patent/JP2015513452A/en active Pending
- 2013-02-14 CA CA2863773A patent/CA2863773A1/en not_active Abandoned
- 2013-02-14 WO PCT/US2013/026189 patent/WO2013123229A1/en not_active Ceased
- 2013-02-14 EP EP13708275.6A patent/EP2814318A1/en not_active Withdrawn
- 2013-02-14 CN CN201380009403.6A patent/CN104254248A/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| EP2814318A1 (en) | 2014-12-24 |
| CN104254248A (en) | 2014-12-31 |
| JP2015513452A (en) | 2015-05-14 |
| WO2013123229A1 (en) | 2013-08-22 |
| US20150031786A1 (en) | 2015-01-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FZDE | Discontinued |
Effective date: 20190214 |