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CA2699579A1 - A kind of beverage as apple cider vinegar - Google Patents

A kind of beverage as apple cider vinegar Download PDF

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Publication number
CA2699579A1
CA2699579A1 CA2699579A CA2699579A CA2699579A1 CA 2699579 A1 CA2699579 A1 CA 2699579A1 CA 2699579 A CA2699579 A CA 2699579A CA 2699579 A CA2699579 A CA 2699579A CA 2699579 A1 CA2699579 A1 CA 2699579A1
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Prior art keywords
tank
liquid
fermentation
filtering
grade
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CA2699579A
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French (fr)
Inventor
Fang Mao Wang
Lin Dong
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Priority to CA2699579A priority Critical patent/CA2699579A1/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof containing fruit or vegetable juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
    • A23B70/00Preservation of non-alcoholic beverages
    • A23B70/30Preservation of non-alcoholic beverages by heating
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/02Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof containing fruit or vegetable juices
    • A23L2/04Extraction of juices
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/70Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12JVINEGAR; PREPARATION OR PURIFICATION THEREOF
    • C12J1/00Vinegar; Preparation or purification thereof

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Organic Chemistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • General Engineering & Computer Science (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

This invention involves a kind of beverage as apple cider vinegar. The composition proportions are as following: apple cider primary pulp 100, high fructose syrup 5-20, honey 0.1-10; the manufacturing process includes: pressing the juice from raw material, zymolysis, clarification, UHT(ultra-high temperature) treatment, deckle board filtering, sterilization, alcoholic fermentation, acetous fermentation, diatomaceous earth filtering and sterilization. This invention provides a kind of beverage as fruit vinegar which is healthy for body, rich in nutrition with unique flavors.

Description

Description Technology Field This invention involves in beverage industry, namely a kind of beverage as apple cider vinegar.

Technology Background The fruit vinegar is mainly made from fruits or processed from of cuts of fruits; it applies with the modern biology technology to brew the materials into a kind of sour seasoning with rich nutrition and unique flavors. It's working with both goods from fruits and table vinegar for health and nutrition benefits, and it's a new beverage with multi-functions of nutrition, health care and food therapy. In some important science studies we discovered that fruit vinegar is working in many functions:
drinking fruit vinegar can improve metabolism, adjust the acid-base balance and remove fatigue;
can reduce cholesterol; can enhance immune function, prevent cancer or anti cancer.
Fruit vinegar is rich in vitamins, amino acid and oxygen, can composite calcium acetate with calcium in human bodies, strengthen the absorbance for calcium;
drinking fruit vinegar can improve the blood circulation, and work in reduce blood pressure; drinking fruit vinegar can work in antibacterial, anti-inflammatory, and prevention and treatment of influenza; can help user lose some weight: fruit vinegar contains rich of amino acids, it not only speeds up the metabolism of carbon hydrate protein, but also improves the adipolysis process.

The general production method of apple cider vinegar is to put the sticky rice vinegar, peeled apple slices and honey together in a jar and shake well, seal the jar and place it in dark and cool place for a week; then open the seal, pour out the juice and add in with 3 times of water for a drink. There's another method to produce apple cider vinegar, it includes following steps: peeling and slicing of apples, washing, putting into wood or stainless steel containers and smashing; mixing the material with certain amount of wheat bran but keep the material wet; then adding in moldy bran at amount of about 3% of total material, stir completely; fermentation; adding in vinegar;
sterilization and storage.

Summary of Invention This invention provides a kind of beverage as fruit vinegar which is rich in nutrition with unique flavors.

This invention is adopting the following technical solution:

A kind of beverage as apple cider vinegar, it's made at the composition proportions as following: apple cider primary pulp 100, high fructose syrup 5-20, and honey 0.1-10.
The apple cider vinegar primary pulp is produced by the following steps:

Pressing: the raw materials, or the apples, are being pressed, filtered by deckle board, treated by UHT, and then get the apple cider primary pulp;

Zymolysis: the primary pulp is put into fermentation tank #1, added in with 0.3 /oo-0.5 /0o pectinase , and kept at the temperature at 50+5 C for a glycolysis, then get a setting for 1.5-2.5 hours.

Clarification: after the zymolysis step is done, open the fermentation tank for a stirring; during the stirring, add in gelating, silica solution and bentonite in sequence which take 0.1-5% of the total volume; every 5 minutes after adding in a material, a kind of clarification agent must be followed. When all the materials are added in, close the fermentation tank, stop the stirring, and get a setting for 1.5-2.5 hours.

UHT treatment: when the clarification step is done, open the fermentation tank #1 for a stirring, switch the valve to let the liquid flow from the discharge hole to fermentation tank #2 through an aseptic UHT machine; adjust the feed in temperature of the aseptic UHT machine to 110-120 C, and the discharging temperature of the aseptic UHT machine to 45-55 C.

Deckle board filtering: open the stirrer of fermentation tank #2, add in 5-20kg diatomaceous earth, let the liquid flow from a discharge hole to tank #2 through a deckle board filtering machine; turn on a filtering pump of a deckle board, let the liquid flow through a deckle board filtering machine circularly; observe through a sight glass inside the tunnel: if the liquid is clear and bright, should switch the valve to let the liquid flow to fermentation tank #1; during the filtering process, if see too much liquid in the collecting slot of the filtering machine, should turn on a return pump to let the liquid inside the collecting slot flow to fermentation tank #1;
during the filtering process, if see too little liquid, should stop the filtering process, loosen the deckle board, clear the filter residue, and resume a filtering;
after the filtering is done, clean fermentation tank #2.

Sterilization: open the stirrer and steam valve of fermentation tank #1, heat up the temperature inside the tank to 85 C, keep at this temperature for 15 minutes, then cool down to 28 C.

Alcoholic fermentation: take dry yeast at the weight of 0.3% of the total liquid and dissolve into some liquid having been UHT treated, for an activation of 10 minutes, then added into fermentation tank #1 and stir thoroughly; and then for a fermentation for 3 days.

Acetous fermentation:
1. Grade 1 seeds propagation: the liquid after alcoholic fermentation will be sent to Grade 1 seeds tank at a set amount of 50 kg, heated up to 85 C and kept at this temperature for 15 minutes, then cooled down to 32 C. Put microorganism already cultivated from the laboratory at amount of 5L to Grade 1 seeds tank through the feed in hole; turn on the stirrer and cultivate for 1-2 days.

2. Grade 2 seeds propagation: the liquid after alcoholic fermentation will be sent to Grade 2 seeds tank at a set amount of 500 kg, heated up to 85 C and kept at this temperature for 15 minutes, then cooled down to 32 C. Put microorganism already cultivated from Grade 1 seeds tank to Grade 2 seeds tank, turn on the stirrer, adjust the inspiration capacity to 3-5 m3 and cultivate for 1-2 days.
3. Acetous fermentation: the liquid after alcoholic fermentation will be sent to acetic acid tank #1 at a set amount of 5000kg, heat up to 85 C and keep at this temperature for 15 minutes, then cool down to 32 C; put the microorganism already cultivated from Grade 2 seeds tank to acetic acid tank #1, turn on the stirrer, adjust the inspiration capacity to 3-10 m3 and cultivate for 1-2 days.

Diatomaceous earth filtering and sterilization: Put 2.5 kg diatomaceous earth in a pre-coat tank, stir circularly inside the filtering machine, observe through a sight glass and until the liquid is clear and bright, put the liquid into a temporary tank;
switch the valve to let the liquid flow into a filtering machine continuously;
switch to ultra high temperature sterilization so the liquid inside the temporary tank will be treated with a sterilization by ultra high temperature; the primary pulp of apple cider vinegar is acquired after all these steps.

The benefits of this invention: this provides a kind of beverage as fruit vinegar which is rich in nutrition with unique flavors.

Detailed Method of Operations:

The following statement is a further description of the method of operations with examples:

Example 1:
A kind of beverage as apple cider vinegar in example 1, it's made at the composition proportions as following: apple cider primary pulp 100, high fructose syrup 5, and honey 0.1. The apple cider vinegar primary pulp is produced by the following steps:

Pressing: apples or apple slices after peeling and enucleating, are being pressed (to guarantee the purity) , filtered by deckle board, treated by UHT, and then get the apple cider primary pulp;

Zymolysis: the primary pulp is put into fermentation tank #1, added in with 0.3 /oo-0.5 /0o pectinase , and kept at the temperature at 50 5 C for a glycolysis, then get a setting for 2 hours.

Clarification: after the zymolysis step is done, open the fermentation tank for a stirring; during the stirring, add in gelating, silica solution and bentonite in sequence which take 0.1-5% of the total volume; every 5 minutes after adding in a material, a kind of clarification agent must be followed. When all the materials are added in, close the fermentation tank, stop the stirring, and get a setting for 2 hours.

UHT treatment: when the clarification step is done, open the fermentation tank #1 for a stirring, switch the valve to let the liquid flow from the discharge hole to fermentation tank #2 through an aseptic UHT machine; adjust the feed in temperature of the aseptic UHT machine to 110-120 C, and the discharging temperature of the aseptic UHT machine to 45-55 C.

Deckle board filtering: open the stirrer of fermentation tank #2, add in 5-20kg diatomaceous earth, let the liquid flow from a discharge hole to tank #2 through a deckle board filtering machine; turn on a filtering pump of a deckle board, let the liquid flow through a deckle board filtering machine circularly; observe through a sight glass inside the tunnel: if the liquid is clear and bright, should switch the valve to let the liquid flow to fermentation tank #1; during the filtering process, if see too much liquid in the collecting slot of the filtering machine, should turn on a return pump to let the liquid inside the collecting slot flow to fermentation tank #1;
during the filtering process, if see too little liquid, should stop the filtering process, loosen the deckle board, clear the filter residue, and resume a filtering;
after the filtering is done, clean fermentation tank #2.

Sterilization: open the stirrer and steam valve of fermentation tank #1, heat up the temperature inside the tank to 85 C, keep at this temperature for 15 minutes, then cool down to 28 C.

Alcoholic fermentation: take dry yeast at the weight of 0.3% of the total liquid and dissolve into some liquid having been UHT treated, for an activation of 10 minutes, then added into fermentation tank #1 and stir thoroughly; and then for a fermentation for 3 days.

Acetous fermentation:
1. Grade 1 seeds propagation: the liquid after alcoholic fermentation will be sent to Grade 1 seeds tank at a set amount of 50 kg, heated up to 85 C and kept at this temperature for 15 minutes, then cooled down to 32 C. Put microorganism already cultivated from the laboratory at amount of 5L to Grade 1 seeds tank through the feed in hole; turn on the stirrer and cultivate for 1-2 days.

2. Grade 2 seeds propagation: the liquid after alcoholic fermentation will be sent to Grade 2 seeds tank at a set amount of 500 kg, heated up to 85 C and kept at this temperature for 15 minutes, then cooled down to 32 C. Put microorganism already cultivated from Grade 1 seeds tank to Grade 2 seeds tank, turn on the stirrer, adjust the inspiration capacity to 3-5 m3 and cultivate for 1-2 days.

3. Acetous fermentation: the liquid after alcoholic fermentation will be sent to acetic acid tank #1 at a set amount of 5000kg, heat up to 85 C and keep at this temperature for 15 minutes, then cool down to 32 C; put the microorganism already cultivated from Grade 2 seeds tank to acetic acid tank #1, turn on the stirrer, adjust the inspiration capacity to 3-10 m3 and cultivate for 1-2 days.

Diatomaceous earth filtering and sterilization: Put 2.5 kg diatomaceous earth in a pre-coat tank, stir circularly inside the filtering machine, observe through a sight glass and until the liquid is clear and bright, put the liquid into a temporary tank;
switch the valve to let the liquid flow into a filtering machine continuously;
switch to ultra high temperature sterilization so the liquid inside the temporary tank will be treated with a sterilization by ultra high temperature; the primary pulp of apple cider vinegar is acquired after all these steps.

Example 2:
A kind of beverage as apple cider vinegar in example 2, it's made at the composition proportions as following: apple cider primary pulp 100, high fructose syrup 12.5, and honey 5. The method of productions is similar to example 1.
Example 3:
A kind of beverage as apple cider vinegar in example 3, it's made at the composition proportions as following: apple cider primary pulp 100, high fructose syrup 20, and honey 10. The method of productions is similar to example 1.

Claims (3)

1. A kind of beverage as apple cider vinegar. It's characterized with the composition proportions as following: apple cider primary pulp 100, high fructose syrup 5-20, and honey 0.1-10. The apple cider vinegar primary pulp is produced by the following steps:

Pressing: the raw materials, or the apples, are being pressed, filtered by deckle board, treated by UHT, and then get the apple cider primary pulp;

Zymolysis: the primary pulp is put into fermentation tank #1, added in with 0.3 Ù-0.5 Ù pectinase , and kept at the temperature at 50~5°C for a glycolysis, then get a setting for 1.5-2.5 hours.

Clarification: after the zymolysis step is done, open the fermentation tank for a stirring; during the stirring, add in gelating, silica solution and bentonite in sequence which take 0.1-5% of the total volume; every 5 minutes after adding in a material, a kind of clarification agent must be followed. When all the materials are added in, close the fermentation tank, stop the stirring, and get a setting for 2 hours.

UHT treatment: when the clarification step is done, open the fermentation tank #1 for a stirring, switch the valve to let the liquid flow from the discharge hole to fermentation tank #2 through an aseptic UHT machine; adjust the feed in temperature of the aseptic UHT machine to 110-120°C, and the discharging temperature of the aseptic UHT machine to 45-55°C.

Deckle board filtering: open the stirrer of fermentation tank #2, add in 5-20kg diatomaceous earth, let the liquid flow from a discharge hole to tank #2 through a deckle board filtering machine; turn on a filtering pump of a deckle board, let the liquid flow through a deckle board filtering machine circularly; observe through a sight glass inside the tunnel: if the liquid is clear and bright, should switch the valve to let the liquid flow to fermentation tank #1; during the filtering process, if see too much liquid in the collecting slot of the filtering machine, should turn on a return pump to let the liquid inside the collecting slot flow to fermentation tank #1;
during the filtering process, if see too little liquid, should stop the filtering process, loosen the deckle board, clear the filter residue, and resume a filtering;
after the filtering is done, clean fermentation tank #2.

Sterilization: open the stirrer and steam valve of fermentation tank #1, heat up the temperature inside the tank to 85°C, keep at this temperature for 15 minutes, then cool down to 28~3°C.

Alcoholic fermentation: take dry yeast at the weight of 0.3~1% of the total liquid and dissolve into some liquid having been UHT treated, for an activation of 10+3 minutes, then added into fermentation tank #1 and stir thoroughly; and then for a fermentation for 3 days.

Acetous fermentation:
1. Grade 1 seeds propagation: the liquid after alcoholic fermentation will be sent to Grade 1 seeds tank at a set amount of 50 kg, heated up to 85~5°C and kept at this temperature for 15~5 minutes, then cooled down to 32°C. Put microorganism already cultivated from the laboratory at amount of 5L to Grade 1 seeds tank through the feed in hole; turn on the stirrer and cultivate for 1-2 days.
2. Grade 2 seeds propagation: the liquid after alcoholic fermentation will be sent to Grade 2 seeds tank at a set amount of 500 kg, heated up to 85~5°C
and kept at this temperature for 15~5 minutes, then cooled down to 32°C. Put microorganism already cultivated from Grade 1 seeds tank to Grade 2 seeds tank, turn on the stirrer, adjust the inspiration capacity to 3-5 m3 and cultivate for 1-2 days.
3. Acetous fermentation: the liquid after alcoholic fermentation will be sent to acetic acid tank #1 at a set amount of 5000kg, heat up to 85~5°C and keep at this temperature for 15~5 minutes, then cool down to 32°C; put the microorganism already cultivated from Grade 2 seeds tank to acetic acid tank #1, turn on the stirrer, adjust the inspiration capacity to 3-10 m3 and cultivate for 1-2 days.

Diatomaceous earth filtering and sterilization: Put 2.5 kg diatomaceous earth in a pre-coat tank, stir circularly inside the filtering machine, observe through a sight glass and until the liquid is clear and bright, put the liquid into a temporary tank;
switch the valve to let the liquid flow into a filtering machine continuously;
switch to ultra high temperature sterilization so the liquid inside the temporary tank will be treated with a sterilization by ultra high temperature; the primary pulp of apple cider vinegar is acquired after all these steps.
CA2699579A 2010-04-14 2010-04-14 A kind of beverage as apple cider vinegar Abandoned CA2699579A1 (en)

Priority Applications (1)

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CA2699579A CA2699579A1 (en) 2010-04-14 2010-04-14 A kind of beverage as apple cider vinegar

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Application Number Priority Date Filing Date Title
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Publications (1)

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Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102433252A (en) * 2011-11-29 2012-05-02 广东省农业科学院蚕业与农产品加工研究所 Clarification method of fruit wine or fruit vinegar
CN103211258A (en) * 2013-04-22 2013-07-24 河南省淼雨饮品股份有限公司 Weight-losing apple vinegar health drink and preparation method thereof
CN103211257A (en) * 2013-04-22 2013-07-24 河南省淼雨饮品股份有限公司 Apple vinegar health care beverage for reducing blood sugar and preparation method thereof
CN104544423A (en) * 2013-10-23 2015-04-29 镇江市悦源醋业有限公司 Apple vinegar
CN104988048A (en) * 2015-06-25 2015-10-21 付俭 Preparation method of Hanfu apple table vinegar
CN105385556A (en) * 2015-12-07 2016-03-09 天津市百奥生物技术有限公司 Edible vinegar sterilizing method
CN105614574A (en) * 2016-01-04 2016-06-01 可口可乐装瓶商管理服务(上海)有限公司 Method for producing fruit pulp particle beverage
CN110777044A (en) * 2019-11-05 2020-02-11 山东农业大学 High-flavonoid apple vinegar and preparation method thereof
CN110885738A (en) * 2019-12-20 2020-03-17 甘肃康元食品有限责任公司 Immunity-enhancing table vinegar and preparation method thereof
CN112226331A (en) * 2020-10-28 2021-01-15 天地壹号饮料股份有限公司 Method for brewing apple vinegar by malic acid-lactic acid fermentation method
CN113136309A (en) * 2021-04-21 2021-07-20 大连工业大学 Preparation method of apple vinegar beverage
CN116574582A (en) * 2023-04-20 2023-08-11 镇江丹和醋业有限公司 A kind of floral-scented fruit vinegar containing rose-scented type and its preparation process
US12144364B2 (en) 2019-04-11 2024-11-19 Goli Nutrition Inc. Apple cider vinegar nutritional supplement

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102433252A (en) * 2011-11-29 2012-05-02 广东省农业科学院蚕业与农产品加工研究所 Clarification method of fruit wine or fruit vinegar
CN103211258A (en) * 2013-04-22 2013-07-24 河南省淼雨饮品股份有限公司 Weight-losing apple vinegar health drink and preparation method thereof
CN103211257A (en) * 2013-04-22 2013-07-24 河南省淼雨饮品股份有限公司 Apple vinegar health care beverage for reducing blood sugar and preparation method thereof
CN104544423A (en) * 2013-10-23 2015-04-29 镇江市悦源醋业有限公司 Apple vinegar
CN104988048A (en) * 2015-06-25 2015-10-21 付俭 Preparation method of Hanfu apple table vinegar
CN105385556A (en) * 2015-12-07 2016-03-09 天津市百奥生物技术有限公司 Edible vinegar sterilizing method
CN105614574A (en) * 2016-01-04 2016-06-01 可口可乐装瓶商管理服务(上海)有限公司 Method for producing fruit pulp particle beverage
US12144364B2 (en) 2019-04-11 2024-11-19 Goli Nutrition Inc. Apple cider vinegar nutritional supplement
US12185746B2 (en) 2019-04-11 2025-01-07 Goli Nutrition Inc. Apple cider vinegar nutritional supplement
CN110777044A (en) * 2019-11-05 2020-02-11 山东农业大学 High-flavonoid apple vinegar and preparation method thereof
CN110885738A (en) * 2019-12-20 2020-03-17 甘肃康元食品有限责任公司 Immunity-enhancing table vinegar and preparation method thereof
CN112226331A (en) * 2020-10-28 2021-01-15 天地壹号饮料股份有限公司 Method for brewing apple vinegar by malic acid-lactic acid fermentation method
CN113136309A (en) * 2021-04-21 2021-07-20 大连工业大学 Preparation method of apple vinegar beverage
CN116574582A (en) * 2023-04-20 2023-08-11 镇江丹和醋业有限公司 A kind of floral-scented fruit vinegar containing rose-scented type and its preparation process

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Effective date: 20140415