CA2115141A1 - Glucomannane de type konjac clarifie et dissous a froid - Google Patents

Glucomannane de type konjac clarifie et dissous a froid

Info

Publication number: CA2115141A1
Authority: CA; Canada
Prior art keywords: konjac; clarified; gel; sol; turbidity
Prior art date: 1991-08-08
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Abandoned

Application number

CA002115141A

Other languages

English (en)

Inventor

William C. Snow

Donald W. Renn

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

FMC Corp

Original Assignee

Individual

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1991-08-08

Filing date

1992-08-07

Publication date

1993-02-18

1992-08-07 Application filed by Individual filed Critical Individual

1993-02-18 Publication of CA2115141A1 publication Critical patent/CA2115141A1/fr

Status Abandoned legal-status Critical Current

Links

241001312219 Amorphophallus konjac Species 0.000 title claims abstract description 211
235000001206 Amorphophallus rivieri Nutrition 0.000 title claims abstract description 211
229920002752 Konjac Polymers 0.000 title claims abstract description 211
239000000252 konjac Substances 0.000 title claims abstract description 210
235000010485 konjac Nutrition 0.000 title claims abstract description 210
LUEWUZLMQUOBSB-FSKGGBMCSA-N (2s,3s,4s,5s,6r)-2-[(2r,3s,4r,5r,6s)-6-[(2r,3s,4r,5s,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5s,6r)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-4,5-dihydroxy-2-(hydroxymethyl)oxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@@H](O[C@@H]2[C@H](O[C@@H](OC3[C@H](O[C@@H](O)[C@@H](O)[C@H]3O)CO)[C@@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O LUEWUZLMQUOBSB-FSKGGBMCSA-N 0.000 title claims abstract description 57
229920002581 Glucomannan Polymers 0.000 title claims abstract description 57
229940046240 glucomannan Drugs 0.000 title claims abstract description 57
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 75
229910052757 nitrogen Inorganic materials 0.000 claims abstract description 38
239000012535 impurity Substances 0.000 claims abstract description 35
239000000203 mixture Substances 0.000 claims abstract description 19
238000000034 method Methods 0.000 claims description 75
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 65
238000000605 extraction Methods 0.000 claims description 56
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical group CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 47
229910001868 water Inorganic materials 0.000 claims description 46
235000013312 flour Nutrition 0.000 claims description 40
239000003795 chemical substances by application Substances 0.000 claims description 24
150000003839 salts Chemical class 0.000 claims description 20
239000000416 hydrocolloid Substances 0.000 claims description 18
238000010438 heat treatment Methods 0.000 claims description 17
238000001035 drying Methods 0.000 claims description 11
230000015572 biosynthetic process Effects 0.000 claims description 10
238000004519 manufacturing process Methods 0.000 claims description 10
GJCOSYZMQJWQCA-UHFFFAOYSA-N 9H-xanthene Chemical compound C1=CC=C2CC3=CC=CC=C3OC2=C1 GJCOSYZMQJWQCA-UHFFFAOYSA-N 0.000 claims description 9
235000010418 carrageenan Nutrition 0.000 claims description 9
229920001525 carrageenan Polymers 0.000 claims description 9
239000000701 coagulant Substances 0.000 claims description 9
229920001285 xanthan gum Polymers 0.000 claims description 9
229920000936 Agarose Polymers 0.000 claims description 8
239000002253 acid Substances 0.000 claims description 8
239000000679 carrageenan Substances 0.000 claims description 8
229940113118 carrageenan Drugs 0.000 claims description 8
238000005352 clarification Methods 0.000 claims description 8
UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 8
239000002738 chelating agent Substances 0.000 claims description 5
238000007710 freezing Methods 0.000 claims description 3
230000008014 freezing Effects 0.000 claims description 3
239000003960 organic solvent Substances 0.000 claims description 3
230000001376 precipitating effect Effects 0.000 claims description 3
239000003638 chemical reducing agent Substances 0.000 claims 5
230000005251 gamma ray Effects 0.000 claims 1
239000000499 gel Substances 0.000 abstract description 137
239000000047 product Substances 0.000 description 53
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 34
239000000706 filtrate Substances 0.000 description 33
239000000463 material Substances 0.000 description 19
238000007792 addition Methods 0.000 description 15
238000001914 filtration Methods 0.000 description 15
DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 14
229910017974 NH40H Inorganic materials 0.000 description 13
230000008569 process Effects 0.000 description 13
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 12
239000002585 base Substances 0.000 description 11
239000007788 liquid Substances 0.000 description 11
230000002829 reductive effect Effects 0.000 description 11
239000000843 powder Substances 0.000 description 9
230000009467 reduction Effects 0.000 description 9
239000007858 starting material Substances 0.000 description 9
FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 8
239000001506 calcium phosphate Substances 0.000 description 8
108090000623 proteins and genes Proteins 0.000 description 8
102000004169 proteins and genes Human genes 0.000 description 8
239000003513 alkali Substances 0.000 description 7
238000009835 boiling Methods 0.000 description 7
239000000084 colloidal system Substances 0.000 description 7
235000013305 food Nutrition 0.000 description 7
150000002500 ions Chemical class 0.000 description 7
238000012545 processing Methods 0.000 description 7
229920002472 Starch Polymers 0.000 description 6
VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 6
230000008901 benefit Effects 0.000 description 6
230000015556 catabolic process Effects 0.000 description 6
229920002678 cellulose Polymers 0.000 description 6
239000001913 cellulose Substances 0.000 description 6
238000006243 chemical reaction Methods 0.000 description 6
238000006731 degradation reaction Methods 0.000 description 6
235000019698 starch Nutrition 0.000 description 6
238000003756 stirring Methods 0.000 description 6
229920002134 Carboxymethyl cellulose Polymers 0.000 description 5
235000019739 Dicalciumphosphate Nutrition 0.000 description 5
KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 5
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
229910052782 aluminium Inorganic materials 0.000 description 5
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 5
NEFBYIFKOOEVPA-UHFFFAOYSA-K dicalcium phosphate Chemical compound [Ca+2].[Ca+2].[O-]P([O-])([O-])=O NEFBYIFKOOEVPA-UHFFFAOYSA-K 0.000 description 5
229910000390 dicalcium phosphate Inorganic materials 0.000 description 5
229940038472 dicalcium phosphate Drugs 0.000 description 5
239000012153 distilled water Substances 0.000 description 5
229940079593 drug Drugs 0.000 description 5
239000003814 drug Substances 0.000 description 5
238000002474 experimental method Methods 0.000 description 5
-1 glucomannan Chemical class 0.000 description 5
238000011065 in-situ storage Methods 0.000 description 5
238000002844 melting Methods 0.000 description 5
239000002245 particle Substances 0.000 description 5
239000000243 solution Substances 0.000 description 5
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 4
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 4
238000002835 absorbance Methods 0.000 description 4
239000000872 buffer Substances 0.000 description 4
239000001110 calcium chloride Substances 0.000 description 4
229910001628 calcium chloride Inorganic materials 0.000 description 4
235000011148 calcium chloride Nutrition 0.000 description 4
230000000052 comparative effect Effects 0.000 description 4
239000006185 dispersion Substances 0.000 description 4
230000000694 effects Effects 0.000 description 4
239000004744 fabric Substances 0.000 description 4
238000001879 gelation Methods 0.000 description 4
150000004676 glycans Chemical class 0.000 description 4
230000008018 melting Effects 0.000 description 4
238000002156 mixing Methods 0.000 description 4
230000004048 modification Effects 0.000 description 4
238000012986 modification Methods 0.000 description 4
229920001282 polysaccharide Polymers 0.000 description 4
239000005017 polysaccharide Substances 0.000 description 4
238000002360 preparation method Methods 0.000 description 4
239000011780 sodium chloride Substances 0.000 description 4
238000012360 testing method Methods 0.000 description 4
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
BFSVOASYOCHEOV-UHFFFAOYSA-N 2-diethylaminoethanol Chemical compound CCN(CC)CCO BFSVOASYOCHEOV-UHFFFAOYSA-N 0.000 description 3
229920000161 Locust bean gum Polymers 0.000 description 3
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
230000002411 adverse Effects 0.000 description 3
230000002776 aggregation Effects 0.000 description 3
238000004220 aggregation Methods 0.000 description 3
238000013019 agitation Methods 0.000 description 3
150000001298 alcohols Chemical class 0.000 description 3
150000001450 anions Chemical class 0.000 description 3
229910000389 calcium phosphate Inorganic materials 0.000 description 3
235000011010 calcium phosphates Nutrition 0.000 description 3
239000001768 carboxy methyl cellulose Substances 0.000 description 3
235000010948 carboxy methyl cellulose Nutrition 0.000 description 3
239000008112 carboxymethyl-cellulose Substances 0.000 description 3
230000001112 coagulating effect Effects 0.000 description 3
238000005345 coagulation Methods 0.000 description 3
230000015271 coagulation Effects 0.000 description 3
238000000576 coating method Methods 0.000 description 3
238000001816 cooling Methods 0.000 description 3
238000000502 dialysis Methods 0.000 description 3
239000000835 fiber Substances 0.000 description 3
239000010408 film Substances 0.000 description 3
239000012467 final product Substances 0.000 description 3
230000036571 hydration Effects 0.000 description 3
238000006703 hydration reaction Methods 0.000 description 3
230000007062 hydrolysis Effects 0.000 description 3
238000006460 hydrolysis reaction Methods 0.000 description 3
150000008040 ionic compounds Chemical class 0.000 description 3
229940025902 konjac mannan Drugs 0.000 description 3
239000000711 locust bean gum Substances 0.000 description 3
235000010420 locust bean gum Nutrition 0.000 description 3
239000000155 melt Substances 0.000 description 3
235000019799 monosodium phosphate Nutrition 0.000 description 3
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 3
239000003973 paint Substances 0.000 description 3
239000008363 phosphate buffer Substances 0.000 description 3
238000001556 precipitation Methods 0.000 description 3
230000002441 reversible effect Effects 0.000 description 3
AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 description 3
229910052938 sodium sulfate Inorganic materials 0.000 description 3
235000011152 sodium sulphate Nutrition 0.000 description 3
238000003860 storage Methods 0.000 description 3
239000000126 substance Substances 0.000 description 3
QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 3
238000010792 warming Methods 0.000 description 3
OMDQUFIYNPYJFM-XKDAHURESA-N (2r,3r,4s,5r,6s)-2-(hydroxymethyl)-6-[[(2r,3s,4r,5s,6r)-4,5,6-trihydroxy-3-[(2s,3s,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]methoxy]oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)O)[C@H](O)[C@H](O)[C@H](O)O1 OMDQUFIYNPYJFM-XKDAHURESA-N 0.000 description 2
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
GUTLYIVDDKVIGB-OUBTZVSYSA-N Cobalt-60 Chemical compound [60Co] GUTLYIVDDKVIGB-OUBTZVSYSA-N 0.000 description 2
102000004190 Enzymes Human genes 0.000 description 2
108090000790 Enzymes Proteins 0.000 description 2
229920000926 Galactomannan Polymers 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
239000005909 Kieselgur Substances 0.000 description 2
229910019142 PO4 Inorganic materials 0.000 description 2
VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 description 2
238000005903 acid hydrolysis reaction Methods 0.000 description 2
150000008043 acidic salts Chemical class 0.000 description 2
239000000908 ammonium hydroxide Substances 0.000 description 2
239000011575 calcium Substances 0.000 description 2
OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
150000001768 cations Chemical class 0.000 description 2
239000003153 chemical reaction reagent Substances 0.000 description 2
239000011248 coating agent Substances 0.000 description 2
239000008367 deionised water Substances 0.000 description 2
229910021641 deionized water Inorganic materials 0.000 description 2
235000011850 desserts Nutrition 0.000 description 2
229940061607 dibasic sodium phosphate Drugs 0.000 description 2
BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 description 2
238000005553 drilling Methods 0.000 description 2
238000001962 electrophoresis Methods 0.000 description 2
239000012530 fluid Substances 0.000 description 2
238000004108 freeze drying Methods 0.000 description 2
239000011491 glass wool Substances 0.000 description 2
238000000227 grinding Methods 0.000 description 2
238000010348 incorporation Methods 0.000 description 2
239000004615 ingredient Substances 0.000 description 2
125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 description 2
GVALZJMUIHGIMD-UHFFFAOYSA-H magnesium phosphate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GVALZJMUIHGIMD-UHFFFAOYSA-H 0.000 description 2
239000004137 magnesium phosphate Substances 0.000 description 2
229910000157 magnesium phosphate Inorganic materials 0.000 description 2
229960002261 magnesium phosphate Drugs 0.000 description 2
235000010994 magnesium phosphates Nutrition 0.000 description 2
238000005259 measurement Methods 0.000 description 2
229910052751 metal Inorganic materials 0.000 description 2
239000002184 metal Substances 0.000 description 2
238000003801 milling Methods 0.000 description 2
229940045641 monobasic sodium phosphate Drugs 0.000 description 2
229910000403 monosodium phosphate Inorganic materials 0.000 description 2
230000036961 partial effect Effects 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 2
239000010452 phosphate Substances 0.000 description 2
239000004033 plastic Substances 0.000 description 2
229920003023 plastic Polymers 0.000 description 2
239000003495 polar organic solvent Substances 0.000 description 2
229920001223 polyethylene glycol Polymers 0.000 description 2
238000012216 screening Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
239000011734 sodium Substances 0.000 description 2
239000001632 sodium acetate Substances 0.000 description 2
235000017281 sodium acetate Nutrition 0.000 description 2
229910000162 sodium phosphate Inorganic materials 0.000 description 2
239000007787 solid Substances 0.000 description 2
239000008107 starch Substances 0.000 description 2
239000008399 tap water Substances 0.000 description 2
235000020679 tap water Nutrition 0.000 description 2
238000002834 transmittance Methods 0.000 description 2
JVIPLYCGEZUBIO-UHFFFAOYSA-N 2-(4-fluorophenyl)-1,3-dioxoisoindole-5-carboxylic acid Chemical compound O=C1C2=CC(C(=O)O)=CC=C2C(=O)N1C1=CC=C(F)C=C1 JVIPLYCGEZUBIO-UHFFFAOYSA-N 0.000 description 1
125000000022 2-aminoethyl group Chemical group [H]C([*])([H])C([H])([H])N([H])[H] 0.000 description 1
RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
229920001817 Agar Polymers 0.000 description 1
229920000945 Amylopectin Polymers 0.000 description 1
241001474374 Blennius Species 0.000 description 1
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 description 1
229920001425 Diethylaminoethyl cellulose Polymers 0.000 description 1
239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 1
241000196324 Embryophyta Species 0.000 description 1
101100073738 Escherichia coli (strain K12) kgtP gene Proteins 0.000 description 1
PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
206010073306 Exposure to radiation Diseases 0.000 description 1
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
241001527806 Iti Species 0.000 description 1
235000010627 Phaseolus vulgaris Nutrition 0.000 description 1
244000046052 Phaseolus vulgaris Species 0.000 description 1
239000002202 Polyethylene glycol Substances 0.000 description 1
229910000831 Steel Inorganic materials 0.000 description 1
239000002250 absorbent Substances 0.000 description 1
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238000010521 absorption reaction Methods 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
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238000005904 alkaline hydrolysis reaction Methods 0.000 description 1
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229940124326 anaesthetic agent Drugs 0.000 description 1
230000003444 anaesthetic effect Effects 0.000 description 1
238000004458 analytical method Methods 0.000 description 1
239000003242 anti bacterial agent Substances 0.000 description 1
230000002421 anti-septic effect Effects 0.000 description 1
229940088710 antibiotic agent Drugs 0.000 description 1
229940064004 antiseptic throat preparations Drugs 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
235000015173 baked goods and baking mixes Nutrition 0.000 description 1
235000013361 beverage Nutrition 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
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150000001720 carbohydrates Chemical class 0.000 description 1
235000014633 carbohydrates Nutrition 0.000 description 1
239000000969 carrier Substances 0.000 description 1
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235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
238000012377 drug delivery Methods 0.000 description 1
238000009837 dry grinding Methods 0.000 description 1
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235000021060 food property Nutrition 0.000 description 1
238000009472 formulation Methods 0.000 description 1
239000011521 glass Substances 0.000 description 1
150000002334 glycols Chemical class 0.000 description 1
239000008187 granular material Substances 0.000 description 1
229940005740 hexametaphosphate Drugs 0.000 description 1
150000004677 hydrates Chemical class 0.000 description 1
239000007943 implant Substances 0.000 description 1
230000002401 inhibitory effect Effects 0.000 description 1
239000002198 insoluble material Substances 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
150000002576 ketones Chemical class 0.000 description 1
235000013372 meat Nutrition 0.000 description 1
238000002483 medication Methods 0.000 description 1
150000007522 mineralic acids Chemical class 0.000 description 1
230000007935 neutral effect Effects 0.000 description 1
MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 description 1
150000007524 organic acids Chemical class 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
239000000123 paper Substances 0.000 description 1
239000008188 pellet Substances 0.000 description 1
239000010451 perlite Substances 0.000 description 1
235000019362 perlite Nutrition 0.000 description 1
229920000728 polyester Polymers 0.000 description 1
238000006116 polymerization reaction Methods 0.000 description 1
238000010298 pulverizing process Methods 0.000 description 1
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239000005297 pyrex Substances 0.000 description 1
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239000000376 reactant Substances 0.000 description 1
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238000004064 recycling Methods 0.000 description 1
238000009877 rendering Methods 0.000 description 1
238000010008 shearing Methods 0.000 description 1
229910052708 sodium Inorganic materials 0.000 description 1
235000019982 sodium hexametaphosphate Nutrition 0.000 description 1
GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 description 1
239000001488 sodium phosphate Substances 0.000 description 1
235000011008 sodium phosphates Nutrition 0.000 description 1
238000001179 sorption measurement Methods 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
239000012798 spherical particle Substances 0.000 description 1
238000001694 spray drying Methods 0.000 description 1
239000003381 stabilizer Substances 0.000 description 1
229910001220 stainless steel Inorganic materials 0.000 description 1
239000010935 stainless steel Substances 0.000 description 1
230000003068 static effect Effects 0.000 description 1
239000010959 steel Substances 0.000 description 1
239000006228 supernatant Substances 0.000 description 1
230000002195 synergetic effect Effects 0.000 description 1
239000001577 tetrasodium phosphonato phosphate Substances 0.000 description 1
239000010409 thin film Substances 0.000 description 1
230000000699 topical effect Effects 0.000 description 1
230000009466 transformation Effects 0.000 description 1
229910052723 transition metal Inorganic materials 0.000 description 1
150000003624 transition metals Chemical class 0.000 description 1
RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
238000003828 vacuum filtration Methods 0.000 description 1
239000011345 viscous material Substances 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1
238000001238 wet grinding Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/006—Heteroglycans, i.e. polysaccharides having more than one sugar residue in the main chain in either alternating or less regular sequence; Gellans; Succinoglycans; Arabinogalactans; Tragacanth or gum tragacanth or traganth from Astragalus; Gum Karaya from Sterculia urens; Gum Ghatti from Anogeissus latifolia; Derivatives thereof
- C08B37/0087—Glucomannans or galactomannans; Tara or tara gum, i.e. D-mannose and D-galactose units, e.g. from Cesalpinia spinosa; Tamarind gum, i.e. D-galactose, D-glucose and D-xylose units, e.g. from Tamarindus indica; Gum Arabic, i.e. L-arabinose, L-rhamnose, D-galactose and D-glucuronic acid units, e.g. from Acacia Senegal or Acacia Seyal; Derivatives thereof
- C08B37/009—Konjac gum or konjac mannan, i.e. beta-D-glucose and beta-D-mannose units linked by 1,4 bonds, e.g. from Amorphophallus species; Derivatives thereof
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
- A23L29/244—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin from corms, tubers or roots, e.g. glucomannan
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/206—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin
- A23L29/256—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of vegetable origin from seaweeds, e.g. alginates, agar or carrageenan
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/269—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of microbial origin, e.g. xanthan or dextran
- A23L29/27—Xanthan not combined with other microbial gums

Landscapes

Chemical & Material Sciences (AREA)
Health & Medical Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Polymers & Plastics (AREA)
Engineering & Computer Science (AREA)
Food Science & Technology (AREA)
Nutrition Science (AREA)
Dispersion Chemistry (AREA)
Emergency Medicine (AREA)
Materials Engineering (AREA)
Medicinal Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Organic Chemistry (AREA)
Biochemistry (AREA)
Molecular Biology (AREA)
General Health & Medical Sciences (AREA)
Preparation Of Fruits And Vegetables (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)
Jellies, Jams, And Syrups (AREA)

CA002115141A 1991-08-08 1992-08-07 Glucomannane de type konjac clarifie et dissous a froid Abandoned CA2115141A1 (fr)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
US74213691A	1991-08-08	1991-08-08
US742,136		1991-08-08

Publications (1)

Publication Number	Publication Date
CA2115141A1 true CA2115141A1 (fr)	1993-02-18

Family

ID=24983632

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA002115141A Abandoned CA2115141A1 (fr)	1991-08-08	1992-08-07	Glucomannane de type konjac clarifie et dissous a froid

Country Status (6)

Country	Link
EP (1)	EP0646133A1 (fr)
JP (1)	JP2687046B2 (fr)
AU (1)	AU663333B2 (fr)
CA (1)	CA2115141A1 (fr)
HU (1)	HUT68444A (fr)
WO (1)	WO1993002571A1 (fr)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US6162906A (en) *	1991-08-08	2000-12-19	Fmc Corporation	Clarified konjac glucomannan
US5718969A (en) *	1993-08-25	1998-02-17	Fmc Corporation	Nonaggregating hydrocolloid microparticulates, intermediates therefor, and processes for their preparation
US5455344A (en) *	1993-09-03	1995-10-03	Fmc Corporation	Agarose compositions for nucleic acid sequencing
EP1137396B1 (fr) *	1998-12-05	2004-09-29	Imperial Chemical Industries PLC	Systemes d'emulsification et emulsions
US20020019447A1 (en) *	2000-07-03	2002-02-14	Renn Donald Walter	Physical forms of clarified hydrocolloids of undiminished properties and method of producing same
US6586590B1 (en)	2000-07-03	2003-07-01	Marine Bioproducts International	Clarified hydrocolloids of undiminished properties and method of producing same
JP6089308B2 (ja) *	2015-05-12	2017-03-08	隆澤村	膨潤した変性マンナン及び熱不可逆ゲル化物又は食品の製造方法
CN107141505A (zh) *	2017-05-15	2017-09-08	陕西科技大学	一种魔芋葡甘聚糖抗菌海绵的制备方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2508726A (en) *	1946-06-27	1950-05-23	Gen Mills Inc	Precipitation of mannogalactans and glucomannans from aqueous sols
US2599771A (en) *	1950-07-19	1952-06-10	Gen Mills Inc	Gels of carboxyalkyl ethers of carbohydrate gums
US2767167A (en) *	1953-07-06	1956-10-16	Gen Mills Inc	Process of reducing the viscosity of gums
US3034974A (en)	1958-01-28	1962-05-15	Gen Foods Corp	Polysaccharide extraction by irradiation
US3346556A (en)	1965-10-14	1967-10-10	Marine Colloids Inc	Treatment of manno galactan gums
US3928322A (en) *	1970-12-30	1975-12-23	Shimizu Manzo Shoten Kk	Konjac mannan
US4427704A (en) *	1979-04-11	1984-01-24	Mars Limited	Food product thickened or gelled with carrageenan and glucomannan
JPS59227267A (ja) *	1983-06-07	1984-12-20	Kazuo Hara	コンニヤクの利用方法
GB8431699D0 (en)	1984-12-14	1985-01-30	Mars G B Ltd	Gel system
JPH02231044A (ja) *	1989-03-01	1990-09-13	Toki Bussan Kk	食物繊維加工食品

1992
- 1992-08-07 CA CA002115141A patent/CA2115141A1/fr not_active Abandoned
- 1992-08-07 WO PCT/US1992/006591 patent/WO1993002571A1/fr not_active Ceased
- 1992-08-07 JP JP5503860A patent/JP2687046B2/ja not_active Expired - Lifetime
- 1992-08-07 EP EP92914652A patent/EP0646133A1/fr not_active Withdrawn
- 1992-08-07 AU AU24494/92A patent/AU663333B2/en not_active Ceased
- 1992-08-07 HU HU9400345A patent/HUT68444A/hu unknown

Also Published As

Publication number	Publication date
AU2449492A (en)	1993-03-02
HUT68444A (en)	1995-06-28
JP2687046B2 (ja)	1997-12-08
EP0646133A1 (fr)	1995-04-05
HU9400345D0 (en)	1994-05-30
WO1993002571A1 (fr)	1993-02-18
JPH07500727A (ja)	1995-01-26
EP0646133A4 (fr)	1994-05-25
AU663333B2 (en)	1995-10-05

Publication	Publication Date	Title
US4952686A (en)	1990-08-28	Soluble dried cassia alloy gum composition and process for making same
EP1833904B1 (fr)	2010-04-21	Composition à base de gomme xanthane dispersable dans l'eau
AU662553B2 (en)	1995-09-07	Clarified konjac glucomannan
CA2115141A1 (fr)	1993-02-18	Glucomannane de type konjac clarifie et dissous a froid
Baker	1948	High-polymer pectins and their deesterification
Akesowan	2002	Viscosity and gel formation of a konjac flour from Amorphophallus oncophyllus
Morris	1990	Biotechnically produced carbohydrates with functional properties for use in food systems
US5733593A (en)	1998-03-31	Rapidly hydratable konjac flour
JP3023244B2 (ja)	2000-03-21	低強度寒天およびその製造方法
CA2274081C (fr)	2004-06-01	Procede pour l'amelioration de l'exploitabilite et de l'ouvrabilite d'endosperme de guar, et produit obtenu selon ce procede
Ooraikul et al.	1974	Starch and pectic substances as affected by a freeze‐thaw potato granule process
US5366671A (en)	1994-11-22	Method of producing a glucomannan sponge
JP4250776B2 (ja)	2009-04-08	糖質−蛋白質複合体およびその製造法
BeMiller	1989	Gums
JPH06254393A (ja)	1994-09-13	保水剤およびその製造方法
Soni et al.	1989	Physicochemical properties of Careya arborea and Aesculus assamica starches
Mohammadi et al.	1987	Xerophytic gourd root starches. Part V: structural characteristics, gelatinization properties and rheologic behavior of coyote gourd starch (Cucurbita digitata Gray)
JPH0624472B2 (ja)	1994-04-06	固形状ゲルとその製法
Heinrichs	1970	Comparative study of pentosans in Triticale and its parental species

Legal Events

Date	Code	Title	Description
1994-02-07	EEER	Examination request
1998-05-12	FZDE	Discontinued
2023-05-26	FZDE	Discontinued	Effective date: 19980512