CA1340670C - Composition electoconductrice et methode de preparation - Google Patents

Composition electoconductrice et methode de preparation

Info

Publication number: CA1340670C
Authority: CA; Canada
Prior art keywords: silica; composition; antimony; slurry; network
Prior art date: 1988-09-16
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired - Fee Related

Application number

CA 611663

Other languages

English (en)

Inventor

Howard Richard Linton

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Milliken and Co

Original Assignee

EI Du Pont de Nemours and Co

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1988-09-16

Filing date

1989-09-15

Publication date

1999-07-20

1989-09-15 Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co

1999-07-20 Application granted granted Critical

1999-07-20 Publication of CA1340670C publication Critical patent/CA1340670C/fr

2016-07-20 Anticipated expiration legal-status Critical

Status Expired - Fee Related legal-status Critical Current

Links

239000000203 mixture Substances 0.000 title claims abstract description 74
238000000034 method Methods 0.000 title claims description 42
238000002360 preparation method Methods 0.000 title description 6
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 336
239000000843 powder Substances 0.000 claims abstract description 144
XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 claims abstract description 89
239000002245 particle Substances 0.000 claims abstract description 78
229910052787 antimony Inorganic materials 0.000 claims abstract description 63
229910001887 tin oxide Inorganic materials 0.000 claims abstract description 60
WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims abstract description 51
239000011159 matrix material Substances 0.000 claims abstract description 12
238000004519 manufacturing process Methods 0.000 claims abstract description 5
239000000377 silicon dioxide Substances 0.000 claims description 133
239000002002 slurry Substances 0.000 claims description 92
239000000243 solution Substances 0.000 claims description 83
239000000758 substrate Substances 0.000 claims description 57
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 56
239000011162 core material Substances 0.000 claims description 53
239000000463 material Substances 0.000 claims description 53
229910001868 water Inorganic materials 0.000 claims description 51
238000000576 coating method Methods 0.000 claims description 47
239000011248 coating agent Substances 0.000 claims description 43
229910052718 tin Inorganic materials 0.000 claims description 40
239000003973 paint Substances 0.000 claims description 31
150000003839 salts Chemical class 0.000 claims description 31
ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 27
AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims description 21
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 20
239000011247 coating layer Substances 0.000 claims description 18
TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 17
239000010445 mica Substances 0.000 claims description 17
229910052618 mica group Inorganic materials 0.000 claims description 17
239000007864 aqueous solution Substances 0.000 claims description 14
239000011521 glass Substances 0.000 claims description 13
229910052783 alkali metal Inorganic materials 0.000 claims description 11
150000001340 alkali metals Chemical class 0.000 claims description 11
229910052784 alkaline earth metal Inorganic materials 0.000 claims description 11
150000001342 alkaline earth metals Chemical class 0.000 claims description 11
238000001354 calcination Methods 0.000 claims description 11
229910052761 rare earth metal Inorganic materials 0.000 claims description 11
229910052723 transition metal Inorganic materials 0.000 claims description 11
150000003624 transition metals Chemical class 0.000 claims description 11
239000002253 acid Substances 0.000 claims description 10
229910052788 barium Inorganic materials 0.000 claims description 9
229910000019 calcium carbonate Inorganic materials 0.000 claims description 9
239000002904 solvent Substances 0.000 claims description 9
VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 8
229910052791 calcium Inorganic materials 0.000 claims description 8
239000012266 salt solution Substances 0.000 claims description 6
239000000725 suspension Substances 0.000 claims description 6
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
238000013019 agitation Methods 0.000 claims description 5
239000003513 alkali Substances 0.000 claims description 4
239000012298 atmosphere Substances 0.000 claims description 4
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 4
235000010216 calcium carbonate Nutrition 0.000 claims description 4
229910052500 inorganic mineral Inorganic materials 0.000 claims description 4
229910052914 metal silicate Inorganic materials 0.000 claims description 4
239000011707 mineral Substances 0.000 claims description 4
235000010755 mineral Nutrition 0.000 claims description 4
229910052760 oxygen Inorganic materials 0.000 claims description 4
239000001301 oxygen Substances 0.000 claims description 4
229910052925 anhydrite Inorganic materials 0.000 claims description 3
239000000835 fiber Substances 0.000 claims description 3
229910052909 inorganic silicate Inorganic materials 0.000 claims description 3
229910052749 magnesium Inorganic materials 0.000 claims description 3
230000001376 precipitating effect Effects 0.000 claims description 3
229910052712 strontium Inorganic materials 0.000 claims description 3
229910052725 zinc Inorganic materials 0.000 claims description 3
229910052799 carbon Inorganic materials 0.000 claims description 2
229910002804 graphite Inorganic materials 0.000 claims description 2
239000010439 graphite Substances 0.000 claims description 2
230000003472 neutralizing effect Effects 0.000 claims description 2
239000004408 titanium dioxide Substances 0.000 claims description 2
OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims 2
BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims 1
229910052923 celestite Inorganic materials 0.000 claims 1
229910017604 nitric acid Inorganic materials 0.000 claims 1
239000010409 thin film Substances 0.000 abstract description 5
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 73
239000000047 product Substances 0.000 description 31
238000007792 addition Methods 0.000 description 29
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 25
FAPDDOBMIUGHIN-UHFFFAOYSA-K antimony trichloride Chemical compound Cl[Sb](Cl)Cl FAPDDOBMIUGHIN-UHFFFAOYSA-K 0.000 description 25
-1 e.g. Substances 0.000 description 24
229910021627 Tin(IV) chloride Inorganic materials 0.000 description 23
HPGGPRDJHPYFRM-UHFFFAOYSA-J tin(iv) chloride Chemical compound Cl[Sn](Cl)(Cl)Cl HPGGPRDJHPYFRM-UHFFFAOYSA-J 0.000 description 23
239000010408 film Substances 0.000 description 22
239000011550 stock solution Substances 0.000 description 19
239000004111 Potassium silicate Substances 0.000 description 16
NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 description 16
229910052913 potassium silicate Inorganic materials 0.000 description 16
235000019353 potassium silicate Nutrition 0.000 description 16
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 14
239000004115 Sodium Silicate Substances 0.000 description 12
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 12
239000000049 pigment Substances 0.000 description 12
229910052911 sodium silicate Inorganic materials 0.000 description 12
ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Inorganic materials O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 description 11
NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 11
239000010410 layer Substances 0.000 description 10
239000004698 Polyethylene Substances 0.000 description 9
238000000151 deposition Methods 0.000 description 9
229920000573 polyethylene Polymers 0.000 description 9
238000004876 x-ray fluorescence Methods 0.000 description 9
UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 8
238000004458 analytical method Methods 0.000 description 8
239000011230 binding agent Substances 0.000 description 8
238000006243 chemical reaction Methods 0.000 description 8
230000008021 deposition Effects 0.000 description 8
239000006185 dispersion Substances 0.000 description 8
238000001914 filtration Methods 0.000 description 8
238000012545 processing Methods 0.000 description 8
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 7
230000015572 biosynthetic process Effects 0.000 description 7
239000001110 calcium chloride Substances 0.000 description 7
229910001628 calcium chloride Inorganic materials 0.000 description 7
235000011148 calcium chloride Nutrition 0.000 description 7
229910052757 nitrogen Inorganic materials 0.000 description 7
239000011148 porous material Substances 0.000 description 7
238000001179 sorption measurement Methods 0.000 description 7
RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 6
238000002441 X-ray diffraction Methods 0.000 description 6
MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 6
239000002585 base Substances 0.000 description 6
239000011575 calcium Substances 0.000 description 6
239000010949 copper Substances 0.000 description 6
229910052802 copper Inorganic materials 0.000 description 6
125000002887 hydroxy group Chemical group [H]O* 0.000 description 6
239000003981 vehicle Substances 0.000 description 6
150000001462 antimony Chemical class 0.000 description 5
230000001427 coherent effect Effects 0.000 description 5
239000008367 deionised water Substances 0.000 description 5
229910021641 deionized water Inorganic materials 0.000 description 5
238000011068 loading method Methods 0.000 description 5
238000001556 precipitation Methods 0.000 description 5
OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 5
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 4
229910000410 antimony oxide Inorganic materials 0.000 description 4
238000001035 drying Methods 0.000 description 4
238000000635 electron micrograph Methods 0.000 description 4
238000002156 mixing Methods 0.000 description 4
229920000642 polymer Polymers 0.000 description 4
QHGNHLZPVBIIPX-UHFFFAOYSA-N tin(ii) oxide Chemical group [Sn]=O QHGNHLZPVBIIPX-UHFFFAOYSA-N 0.000 description 4
229920000877 Melamine resin Polymers 0.000 description 3
239000011324 bead Substances 0.000 description 3
239000004359 castor oil Substances 0.000 description 3
235000019438 castor oil Nutrition 0.000 description 3
239000013078 crystal Substances 0.000 description 3
239000012634 fragment Substances 0.000 description 3
ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 description 3
239000000543 intermediate Substances 0.000 description 3
JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 description 3
238000006386 neutralization reaction Methods 0.000 description 3
229920003023 plastic Polymers 0.000 description 3
239000004033 plastic Substances 0.000 description 3
229920000728 polyester Polymers 0.000 description 3
229910052708 sodium Inorganic materials 0.000 description 3
239000011734 sodium Substances 0.000 description 3
239000007787 solid Substances 0.000 description 3
239000002345 surface coating layer Substances 0.000 description 3
UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 2
229910021626 Tin(II) chloride Inorganic materials 0.000 description 2
GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 2
230000002378 acidificating effect Effects 0.000 description 2
230000002411 adverse Effects 0.000 description 2
229910052782 aluminium Inorganic materials 0.000 description 2
230000005540 biological transmission Effects 0.000 description 2
239000003054 catalyst Substances 0.000 description 2
239000003518 caustics Substances 0.000 description 2
150000001805 chlorine compounds Chemical class 0.000 description 2
238000000280 densification Methods 0.000 description 2
238000011161 development Methods 0.000 description 2
238000007865 diluting Methods 0.000 description 2
238000011156 evaluation Methods 0.000 description 2
238000000605 extraction Methods 0.000 description 2
238000011049 filling Methods 0.000 description 2
238000009472 formulation Methods 0.000 description 2
230000005484 gravity Effects 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
238000011065 in-situ storage Methods 0.000 description 2
238000010348 incorporation Methods 0.000 description 2
150000002500 ions Chemical class 0.000 description 2
238000002955 isolation Methods 0.000 description 2
NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical class O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
229910052751 metal Inorganic materials 0.000 description 2
239000002184 metal Substances 0.000 description 2
150000002902 organometallic compounds Chemical class 0.000 description 2
230000003647 oxidation Effects 0.000 description 2
238000007254 oxidation reaction Methods 0.000 description 2
229920005989 resin Polymers 0.000 description 2
239000011347 resin Substances 0.000 description 2
238000004062 sedimentation Methods 0.000 description 2
238000003756 stirring Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
239000006228 supernatant Substances 0.000 description 2
238000012360 testing method Methods 0.000 description 2
238000005979 thermal decomposition reaction Methods 0.000 description 2
KSBAEPSJVUENNK-UHFFFAOYSA-L tin(ii) 2-ethylhexanoate Chemical group [Sn+2].CCCCC(CC)C([O-])=O.CCCCC(CC)C([O-])=O KSBAEPSJVUENNK-UHFFFAOYSA-L 0.000 description 2
239000011701 zinc Substances 0.000 description 2
PTTPXKJBFFKCEK-UHFFFAOYSA-N 2-Methyl-4-heptanone Chemical compound CC(C)CC(=O)CC(C)C PTTPXKJBFFKCEK-UHFFFAOYSA-N 0.000 description 1
JVKRKMWZYMKVTQ-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]pyrazol-1-yl]-N-(2-oxo-3H-1,3-benzoxazol-6-yl)acetamide Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C=1C=NN(C=1)CC(=O)NC1=CC2=C(NC(O2)=O)C=C1 JVKRKMWZYMKVTQ-UHFFFAOYSA-N 0.000 description 1
WBIQQQGBSDOWNP-UHFFFAOYSA-N 2-dodecylbenzenesulfonic acid Chemical compound CCCCCCCCCCCCC1=CC=CC=C1S(O)(=O)=O WBIQQQGBSDOWNP-UHFFFAOYSA-N 0.000 description 1
206010067484 Adverse reaction Diseases 0.000 description 1
238000004438 BET method Methods 0.000 description 1
241000270299 Boa Species 0.000 description 1
101100537266 Caenorhabditis elegans tin-13 gene Proteins 0.000 description 1
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
206010010071 Coma Diseases 0.000 description 1
229910017974 NH40H Inorganic materials 0.000 description 1
CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
239000004110 Zinc silicate Substances 0.000 description 1
150000001242 acetic acid derivatives Chemical class 0.000 description 1
239000003377 acid catalyst Substances 0.000 description 1
150000007513 acids Chemical class 0.000 description 1
NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
230000002730 additional effect Effects 0.000 description 1
239000000654 additive Substances 0.000 description 1
230000001464 adherent effect Effects 0.000 description 1
230000006838 adverse reaction Effects 0.000 description 1
230000001476 alcoholic effect Effects 0.000 description 1
229910052910 alkali metal silicate Inorganic materials 0.000 description 1
XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
FAWGZAFXDJGWBB-UHFFFAOYSA-N antimony(3+) Chemical class [Sb+3] FAWGZAFXDJGWBB-UHFFFAOYSA-N 0.000 description 1
239000007900 aqueous suspension Substances 0.000 description 1
DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 description 1
XDFCIPNJCBUZJN-UHFFFAOYSA-N barium(2+) Chemical compound [Ba+2] XDFCIPNJCBUZJN-UHFFFAOYSA-N 0.000 description 1
230000009286 beneficial effect Effects 0.000 description 1
DAMJCWMGELCIMI-UHFFFAOYSA-N benzyl n-(2-oxopyrrolidin-3-yl)carbamate Chemical compound C=1C=CC=CC=1COC(=O)NC1CCNC1=O DAMJCWMGELCIMI-UHFFFAOYSA-N 0.000 description 1
229910021538 borax Inorganic materials 0.000 description 1
239000004303 calcium sorbate Substances 0.000 description 1
239000006229 carbon black Substances 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
239000007795 chemical reaction product Substances 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
238000005229 chemical vapour deposition Methods 0.000 description 1
239000004927 clay Substances 0.000 description 1
238000004040 coloring Methods 0.000 description 1
238000005056 compaction Methods 0.000 description 1
239000008139 complexing agent Substances 0.000 description 1
150000001875 compounds Chemical class 0.000 description 1
239000004020 conductor Substances 0.000 description 1
239000007771 core particle Substances 0.000 description 1
230000007812 deficiency Effects 0.000 description 1
238000001514 detection method Methods 0.000 description 1
235000014113 dietary fatty acids Nutrition 0.000 description 1
238000010790 dilution Methods 0.000 description 1
239000012895 dilution Substances 0.000 description 1
125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
YGANSGVIUGARFR-UHFFFAOYSA-N dipotassium dioxosilane oxo(oxoalumanyloxy)alumane oxygen(2-) Chemical compound [O--].[K+].[K+].O=[Si]=O.O=[Al]O[Al]=O YGANSGVIUGARFR-UHFFFAOYSA-N 0.000 description 1
238000007598 dipping method Methods 0.000 description 1
239000012153 distilled water Substances 0.000 description 1
ZOIVSVWBENBHNT-UHFFFAOYSA-N dizinc;silicate Chemical compound [Zn+2].[Zn+2].[O-][Si]([O-])([O-])[O-] ZOIVSVWBENBHNT-UHFFFAOYSA-N 0.000 description 1
229940060296 dodecylbenzenesulfonic acid Drugs 0.000 description 1
229920001971 elastomer Polymers 0.000 description 1
239000000806 elastomer Substances 0.000 description 1
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239000000194 fatty acid Substances 0.000 description 1
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150000004665 fatty acids Chemical class 0.000 description 1
239000000945 filler Substances 0.000 description 1
239000000706 filtrate Substances 0.000 description 1
QYFRTHZXAGSYGT-UHFFFAOYSA-L hexaaluminum dipotassium dioxosilane oxygen(2-) difluoride hydrate Chemical compound O.[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[O--].[F-].[F-].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O QYFRTHZXAGSYGT-UHFFFAOYSA-L 0.000 description 1
238000009616 inductively coupled plasma Methods 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
239000002198 insoluble material Substances 0.000 description 1
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XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
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230000001788 irregular Effects 0.000 description 1
229910052622 kaolinite Inorganic materials 0.000 description 1
239000004816 latex Substances 0.000 description 1
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239000007788 liquid Substances 0.000 description 1
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238000002844 melting Methods 0.000 description 1
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229910044991 metal oxide Inorganic materials 0.000 description 1
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238000000465 moulding Methods 0.000 description 1
229910052627 muscovite Inorganic materials 0.000 description 1
150000002823 nitrates Chemical class 0.000 description 1
230000003287 optical effect Effects 0.000 description 1
239000003960 organic solvent Substances 0.000 description 1
150000003891 oxalate salts Chemical class 0.000 description 1
230000037361 pathway Effects 0.000 description 1
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150000002910 rare earth metals Chemical class 0.000 description 1
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230000000717 retained effect Effects 0.000 description 1
238000012216 screening Methods 0.000 description 1
238000000926 separation method Methods 0.000 description 1
150000004760 silicates Chemical class 0.000 description 1
RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 1
235000012239 silicon dioxide Nutrition 0.000 description 1
235000010339 sodium tetraborate Nutrition 0.000 description 1
239000006104 solid solution Substances 0.000 description 1
238000002336 sorption--desorption measurement Methods 0.000 description 1
238000001228 spectrum Methods 0.000 description 1
238000005507 spraying Methods 0.000 description 1
239000007858 starting material Substances 0.000 description 1
229910000018 strontium carbonate Inorganic materials 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
239000002344 surface layer Substances 0.000 description 1
239000000454 talc Substances 0.000 description 1
229910052623 talc Inorganic materials 0.000 description 1
YEAUATLBSVJFOY-UHFFFAOYSA-N tetraantimony hexaoxide Chemical compound O1[Sb](O2)O[Sb]3O[Sb]1O[Sb]2O3 YEAUATLBSVJFOY-UHFFFAOYSA-N 0.000 description 1
239000010936 titanium Substances 0.000 description 1
229910052719 titanium Inorganic materials 0.000 description 1
238000012546 transfer Methods 0.000 description 1
229910000326 transition metal silicate Inorganic materials 0.000 description 1
238000004627 transmission electron microscopy Methods 0.000 description 1
YGBFTDQFAKDXBZ-UHFFFAOYSA-N tributyl stiborite Chemical compound [Sb+3].CCCC[O-].CCCC[O-].CCCC[O-] YGBFTDQFAKDXBZ-UHFFFAOYSA-N 0.000 description 1
BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 description 1
125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
229920002554 vinyl polymer Polymers 0.000 description 1
238000005406 washing Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1
239000008096 xylene Substances 0.000 description 1
235000019352 zinc silicate Nutrition 0.000 description 1

Landscapes

Paints Or Removers (AREA)
Pigments, Carbon Blacks, Or Wood Stains (AREA)

CA 611663 1988-09-16 1989-09-15 Composition electoconductrice et methode de preparation Expired - Fee Related CA1340670C (fr)

Applications Claiming Priority (4)

Application Number	Priority Date	Filing Date
US32088A	1988-09-16	1988-09-16
US32089A	1989-08-02	1989-08-02
US245,183		1989-08-02
US386,765		1989-08-02

Publications (1)

Publication Number	Publication Date
CA1340670C true CA1340670C (fr)	1999-07-20

Family

ID=33422352

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
CA 611663 Expired - Fee Related CA1340670C (fr)	1988-09-16	1989-09-15	Composition electoconductrice et methode de preparation

Country Status (1)

Country	Link
CA (1)	CA1340670C (fr)

1989
- 1989-09-15 CA CA 611663 patent/CA1340670C/fr not_active Expired - Fee Related

Publication	Publication Date	Title
US5236737A (en)	1993-08-17	Electroconductive composition and process of preparation
US5585037A (en)	1996-12-17	Electroconductive composition and process of preparation
EP0743654B1 (fr)	2000-01-19	Composition électroconductrice et procédé de préparation
KR100394889B1 (ko)	2003-11-14	침상 전기전도성 산화주석 미세입자 및 그의 제조방법
US7226503B2 (en)	2007-06-05	Effect pigments based on coated glass flakes
US5292551A (en)	1994-03-08	Process for producing electroconductive powders
US5534193A (en)	1996-07-09	White electroconductive powders with antimony and tin oxides
CA1340670C (fr)	1999-07-20	Composition electoconductrice et methode de preparation
JP3609159B2 (ja)	2005-01-12	針状導電性アンチモン含有酸化錫微粉末及びその製造方法
JP2005330163A (ja)	2005-12-02	導電性酸化錫粉末、その製造方法、導電性ペースト及び導電性塗料
JP3515625B2 (ja)	2004-04-05	針状導電性酸化錫微粉末およびその製造方法
JPH08217445A (ja)	1996-08-27	針状導電性酸化錫微粉末およびその製造方法
JP3557688B2 (ja)	2004-08-25	短冊状導電性粉末とその製造方法および用途
JPH05116930A (ja)	1993-05-14	白色導電性粉末

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2006-07-20	MKLA	Lapsed