[go: up one dir, main page]

BRPI0411739A - componente inorgánico compatìvel catiÈnico, composição de cuidado oral, e, método de fabricar um dentifrìcio - Google Patents

componente inorgánico compatìvel catiÈnico, composição de cuidado oral, e, método de fabricar um dentifrìcio

Info

Publication number
BRPI0411739A
BRPI0411739A BRPI0411739-5A BRPI0411739A BRPI0411739A BR PI0411739 A BRPI0411739 A BR PI0411739A BR PI0411739 A BRPI0411739 A BR PI0411739A BR PI0411739 A BRPI0411739 A BR PI0411739A
Authority
BR
Brazil
Prior art keywords
toothpaste
manufacturing
cationic
oral care
care composition
Prior art date
Application number
BRPI0411739-5A
Other languages
English (en)
Inventor
Michael Prencipe
Thomas J Boyd
M Teresa R Carale
Original Assignee
Colgate Palmolive Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=33555804&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=BRPI0411739(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from US10/601,474 external-priority patent/US20040258631A1/en
Application filed by Colgate Palmolive Co filed Critical Colgate Palmolive Co
Publication of BRPI0411739A publication Critical patent/BRPI0411739A/pt

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
    • A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Cosmetics (AREA)
  • Medicinal Preparation (AREA)

Abstract

"COMPONENTE INORGáNICO COMPATìVEL CATIÈNICO, COMPOSIçãO DE CUIDADO ORAL, E, MéTODO DE FABRICAR UM DENTIFRìCIO". Um particulado inorgânico compatível catiónico que compreende sílica substancialmente revestida com um tensoativo não iónico, tal como um óleo de hidrocarboneto hidrogenado etoxilado. Composições que compreendem o particulado compatível catiónico e um ativo catiónico, tal como cloreto de cetil piridínio ou um éster de etil lauril arginina, também são fornecidos.
BRPI0411739-5A 2003-06-23 2004-06-23 componente inorgánico compatìvel catiÈnico, composição de cuidado oral, e, método de fabricar um dentifrìcio BRPI0411739A (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US10/601,474 US20040258631A1 (en) 2003-06-23 2003-06-23 Oral care compositions exhibiting antiplaque and breath freshening properties
US10/875,063 US8865135B2 (en) 2003-06-23 2004-06-23 Stable dentifrice compositions
PCT/US2004/020033 WO2005000253A1 (en) 2003-06-23 2004-06-23 Stable dentifrice compositions

Publications (1)

Publication Number Publication Date
BRPI0411739A true BRPI0411739A (pt) 2006-08-08

Family

ID=33555804

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0411739-5A BRPI0411739A (pt) 2003-06-23 2004-06-23 componente inorgánico compatìvel catiÈnico, composição de cuidado oral, e, método de fabricar um dentifrìcio

Country Status (14)

Country Link
US (1) US8865135B2 (pt)
EP (1) EP1635774B2 (pt)
AT (1) ATE369114T1 (pt)
AU (1) AU2004251727B2 (pt)
BR (1) BRPI0411739A (pt)
CA (1) CA2530399C (pt)
CO (1) CO5650217A2 (pt)
DE (1) DE602004008072T3 (pt)
DK (1) DK1635774T4 (pt)
ES (1) ES2291908T5 (pt)
MX (1) MXPA05013498A (pt)
PL (1) PL1635774T5 (pt)
RU (1) RU2347556C2 (pt)
WO (1) WO2005000253A1 (pt)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100173993A1 (en) * 2003-02-06 2010-07-08 Sawyer Anthony J Controlled release biocidal salts
AU2006226505B2 (en) * 2005-03-21 2012-04-19 Glaxosmithkline Consumer Healthcare (Uk) Ip Limited Alkyl sulfate free and orthophosphate free dentifrice compostion comprising a fluoride source and a silica dental abrasive
US20060263444A1 (en) 2005-05-19 2006-11-23 Xintian Ming Antimicrobial composition
US20070014740A1 (en) * 2005-07-15 2007-01-18 Colgate-Palmolive Company Oral compositions having cationic active ingredients
MX2009008476A (es) * 2007-02-07 2009-08-20 Miret Lab Nueva combinacion de conservadores cationicos con componentes enmascaradores de sabor.
CN102458385A (zh) 2009-05-08 2012-05-16 3M创新有限公司 口腔护理方法和套件
TW201103566A (en) * 2009-06-16 2011-02-01 Grace W R & Co Cation compatible metal oxides and oral care compositions containing the metal oxides
US11052029B2 (en) 2009-06-16 2021-07-06 W. R. Grace & Co.-Conn. Cation compatible metal oxides and oral care compositions containing the metal oxides
EP2549993A4 (en) * 2010-03-23 2014-08-06 Gojo Ind Inc ANTIMICROBIAL COMPOSITIONS
DE102010013272A1 (de) * 2010-03-29 2011-09-29 Beiersdorf Ag Mikrobiologisch stabile anwendungsfreundliche Zubereitung mit Verdickern
MX2012013955A (es) 2010-06-23 2013-01-24 Colgate Palmolive Co Composiciones terapeuticas bucales.
DE102012007212A1 (de) 2012-04-11 2013-10-17 Merz Pharma Gmbh & Co. Kgaa Zubereitung zur topischen Anwendung auf Schleimhäuten mit Polyhexanid als Wirkstoff
US11684069B2 (en) 2013-09-13 2023-06-27 3M Innovative Properties Company Cationic antiseptic compositions
CN107106451B (zh) * 2014-12-23 2021-11-09 高露洁-棕榄公司 口腔护理组合物
WO2018201119A1 (en) * 2017-04-29 2018-11-01 Nevada Naturals Inc. Biofilm penetrating compositions and methods
US12447119B2 (en) 2019-03-18 2025-10-21 Sunstar Americas, Inc. Oral care composition

Family Cites Families (75)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3151027A (en) * 1961-06-07 1964-09-29 Procter & Gamble Abrasive for dentifrice composition
JPS4926046B1 (pt) * 1969-12-30 1974-07-05
GB1352420A (en) 1971-06-18 1974-05-08 Ajinomoto Kk Arginine derivatives their production and their use
FR2143557A1 (en) 1971-06-29 1973-02-09 Ajinomoto Kk Antimicrobial n-acyl basic amino acid derivs - useful as antiseptics, preservatives, disinfectants etc
US4255579A (en) * 1974-05-20 1981-03-10 Sterling Drug Inc. 11-Substituted hexahydro-2,6-methano-3-benzazocines
CA1063357A (en) * 1974-05-21 1979-10-02 James J. Benedict Abrasive composition
US4022881A (en) * 1974-06-18 1977-05-10 Beecham Group Limited Dentifrice
JPS5123571A (ja) 1974-08-21 1976-02-25 Hitachi Ltd Chunyujushikoteiho
US4098878A (en) * 1974-10-29 1978-07-04 Colgate-Palmolive Company Toothpaste containing milled alpha-alumina trihydrate
US4198392A (en) * 1975-06-23 1980-04-15 The Procter & Gamble Company Oral compositions containing bis-biguanides with reduced staining tendencies
DE2633651A1 (de) 1975-08-01 1977-02-17 Procter & Gamble Bis-biguanido-verbindungen und dieselben enthaltende mund- und/oder zahnpflegemittel
US4042679A (en) * 1975-11-07 1977-08-16 Colgate-Palmolive Company Antibacterial oral composition
US4097604A (en) * 1975-12-18 1978-06-27 Oxford Hill, Ltd. Method of treating and controlling gingivitis
US4118472A (en) * 1976-08-16 1978-10-03 Colgate-Palmolive Company Antibacterial oral composition
US4225579A (en) * 1979-02-27 1980-09-30 Israel Kleinberg Means and method for improving defenses against caries
JPS5915084B2 (ja) 1979-07-03 1984-04-07 株式会社トクヤマ 改質シリカの製法
US4469674A (en) * 1981-09-03 1984-09-04 Richardson-Vicks Inc. Stable oral compositions containing zinc and fluoride compounds
US4499068A (en) * 1982-08-26 1985-02-12 Johnson & Johnson Products, Inc. Oral compositions comprising NG -alkyl derivatives of arginine
US4477428A (en) * 1982-08-26 1984-10-16 Johnson & Johnson Products, Inc. Oral compositions comprising N.sup.α,NG -diacyl derivatives of arginine
US4499067A (en) * 1982-08-26 1985-02-12 Johnson & Johnson Products, Inc. Oral compositions comprising NG -acyl derivatives of arginine
GB8312663D0 (en) * 1983-05-09 1983-06-15 Ici Plc Bisbiguanide compounds
GB8312661D0 (en) 1983-05-09 1983-06-15 Ici Plc Bisbiguanide derivatives
GB8312662D0 (en) 1983-05-09 1983-06-15 Ici Plc Polyether bisbiguanide
JPS6092208A (ja) 1983-10-25 1985-05-23 Kao Corp 塩化ナトリウム含有歯磨組成物
US4567174A (en) * 1984-05-07 1986-01-28 Imperial Chemical Industries Plc Bis(1-substituted biguanide) derivatives
JPS6156214A (ja) 1984-08-28 1986-03-20 Nippon Kokan Kk <Nkk> 高炉シヤフト下部サンプラ−
US4837008A (en) * 1985-04-09 1989-06-06 Peroxydent Group Periodontal composition and method
US4695463A (en) * 1985-05-24 1987-09-22 Warner-Lambert Company Delivery system for active ingredients and preparation thereof
GB2210264A (en) 1987-10-02 1989-06-07 Richardson Vicks Ltd Antigingival/antiplaque compositions
EP0422803A3 (en) * 1989-10-11 1991-06-05 Beecham Group p.l.c. Dentifrice comprising cationic antibacterial agent
JPH03291211A (ja) 1990-04-09 1991-12-20 Lion Corp 毛髪化粧料
JP2946105B2 (ja) 1990-04-24 1999-09-06 花王株式会社 口腔用組成物
JPH0684294B2 (ja) 1990-05-29 1994-10-26 サンスター株式会社 口腔用組成物
JPH0684293B2 (ja) 1990-05-29 1994-10-26 サンスター株式会社 口腔用組成物
GB9021061D0 (en) * 1990-09-27 1990-11-07 Unilever Plc Encapsulating method and products containing encapsulated material
US5180577A (en) * 1990-10-09 1993-01-19 Colgate-Palmolive Stabilized bis biguanide/anionic active ingredient compositions
JP3208880B2 (ja) 1992-07-13 2001-09-17 ソニー株式会社 磁気ディスク装置
GB9221593D0 (en) * 1992-10-14 1992-11-25 Boots Co Plc Oral hygiene composition
CA2132014C (en) * 1993-01-14 2001-07-24 Gianni Baffelli Toothpaste
JPH08506611A (ja) † 1993-02-12 1996-07-16 キャボット コーポレイション 界面活性剤変性シリカ
US5891857A (en) * 1996-02-20 1999-04-06 Vanderbilt University Characterized BRCA1 and BRCA2 proteins and screening and therapeutic methods based on characterized BRCA1 and BRCA2 proteins
US5762911A (en) 1996-03-05 1998-06-09 The Research Foundation Of State University Of New York Anti-caries oral compositions
JPH09286712A (ja) 1996-04-18 1997-11-04 Sunstar Inc 口腔用組成物
FR2751635B1 (fr) * 1996-07-23 1998-10-02 Rhone Poulenc Chimie Silice compatible avec les aromes, son procede de preparation et compositions dentifrices la contenant
DE19646392A1 (de) * 1996-11-11 1998-05-14 Lohmann Therapie Syst Lts Zubereitung zur Anwendung in der Mundhöhle mit einer an der Schleimhaut haftklebenden, Pharmazeutika oder Kosmetika zur dosierten Abgabe enthaltenden Schicht
US20030206874A1 (en) * 1996-11-21 2003-11-06 The Proctor & Gamble Company Promoting whole body health
CA2235655C (en) * 1997-04-24 2008-01-22 Sunstar Inc. Oral compositions comprising porous calcium carbonate
AU7472398A (en) 1997-05-09 1998-11-27 Medlogic Global Corporation Compositions for cosmetic applications
US5780015A (en) * 1997-05-14 1998-07-14 Colgate Palmolive Company Dentifrice for the treatment of dentinal hypersensitivity having limited astringency
AU4428197A (en) 1997-09-18 1999-04-05 Wm. Wrigley Jr. Company Chewing gum containing physiological cooling agents
US6228347B1 (en) * 1997-12-01 2001-05-08 Thione International, Inc. Antioxidant gel for gingival conditions
US5874068A (en) * 1997-12-08 1999-02-23 Warner-Lambert Company Stabilized antiplaque and antigingivitis oral compositions containing N.sup.α -alkyl-L-arginine alkyl ester salts
JPH11255629A (ja) 1998-01-08 1999-09-21 Sunstar Inc 口腔用組成物
US6086648A (en) * 1998-04-07 2000-07-11 Norton Company Bonded abrasive articles filled with oil/wax mixture
US6479036B1 (en) * 1998-06-05 2002-11-12 Crosfield Limited Particulate materials for use in dentifrice compositions
JP2000256155A (ja) 1999-03-09 2000-09-19 Sunstar Inc 口腔用組成物
US6290933B1 (en) * 2000-05-09 2001-09-18 Colgate-Palmolive Company High cleaning dentifrice
US20030133883A1 (en) * 2001-06-14 2003-07-17 Finnegan Mary Beth Oral care compositions containing grapefruit seed extract
US20020068039A1 (en) * 2000-07-28 2002-06-06 Pan Pauline C. Oral care compositions containing grapefruit seed extract
US6685921B2 (en) * 2000-10-25 2004-02-03 The Procter & Gamble Company Dental care compositions
US6447758B1 (en) * 2001-05-02 2002-09-10 Colgate Palmolive Company Cationic antibacterial dentifrice exhibiting superior foaming properties
WO2002091378A1 (en) * 2001-05-10 2002-11-14 Koninklijke Philips Electronics N.V. Signal processor and apparatus for reproducing information
ATE536170T1 (de) 2001-08-09 2011-12-15 Miret Lab Verwendung von kationischen tensiden in kosmetischen mitteln
CA2455983C (en) 2001-08-09 2010-06-01 Joan Baptista Urgell Beltran Preservative systems and their use in cosmetic preparations
US6419903B1 (en) * 2001-08-20 2002-07-16 Colgate Palmolive Company Breath freshening film
PT1437946E (pt) 2001-10-25 2012-07-25 Miret Lab Utilização de um conservante catiónico em produtos alimentares
GB0126244D0 (en) 2001-11-01 2002-01-02 Ineos Silicas Ltd Oral compositions
ES2344002T3 (es) * 2001-11-15 2010-08-16 Laboratorios Miret, S.A. Uso de surfactante cationico como potenciador de la actividad antimicrobiana en desodorantes y cuidado oral.
JP4229842B2 (ja) 2002-02-22 2009-02-25 ルバンス セラピュティックス インク． Ｌ−アルギニンオリゴマーを含む化粧品処方
US20040258631A1 (en) * 2003-06-23 2004-12-23 Boyd Thomas J. Oral care compositions exhibiting antiplaque and breath freshening properties
US20040258629A1 (en) * 2003-06-23 2004-12-23 Boyd Thomas J. Antiplaque confectionery dental composition
US8287843B2 (en) * 2003-06-23 2012-10-16 Colgate-Palmolive Company Antiplaque oral care compositions
US20040258630A1 (en) * 2003-06-23 2004-12-23 Boyd Thomas J. Antiplaque breath freshening consumable film
MXPA05013499A (es) * 2003-06-23 2006-03-09 Colgate Palmolive Co Composiciones de enjuague bucal que contienen sales de n-acil-arginina alquil ester.
US20040258632A1 (en) * 2003-06-23 2004-12-23 Boyd Thomas J. Stable aqueous antiplaque oral compositions

Also Published As

Publication number Publication date
RU2347556C2 (ru) 2009-02-27
RU2006101695A (ru) 2006-06-10
DE602004008072T2 (de) 2008-04-24
MXPA05013498A (es) 2006-03-09
US20050031551A1 (en) 2005-02-10
CO5650217A2 (es) 2006-06-30
EP1635774A1 (en) 2006-03-22
CA2530399C (en) 2012-08-21
AU2004251727A1 (en) 2005-01-06
US8865135B2 (en) 2014-10-21
PL1635774T5 (pl) 2011-06-30
ATE369114T1 (de) 2007-08-15
DE602004008072T3 (de) 2011-05-12
PL1635774T3 (pl) 2007-12-31
WO2005000253A1 (en) 2005-01-06
ES2291908T5 (es) 2011-05-25
AU2004251727B2 (en) 2010-06-17
ES2291908T3 (es) 2008-03-01
CA2530399A1 (en) 2005-01-06
EP1635774B1 (en) 2007-08-08
DE602004008072D1 (de) 2007-09-20
DK1635774T3 (da) 2007-12-17
EP1635774B2 (en) 2011-01-26
DK1635774T4 (da) 2011-05-30

Similar Documents

Publication Publication Date Title
BRPI0411739A (pt) componente inorgánico compatìvel catiÈnico, composição de cuidado oral, e, método de fabricar um dentifrìcio
AU2003298712A1 (en) Methods and compositions for applying pharmacologic agents to the ear
MY145080A (en) Benzimidazole, benzthiazole and benzoxazole derivatives and their use as lta4h modulators
BRPI0519481A2 (pt) glicopirrolato em preparaÇÕes cosmÉticas
NO20034490D0 (no) Fremgangsmåte for sammensetting av absorberende gjenstand til personlig stell
DE60329318D1 (de) 4-oxochinolinverbindungen und deren verwendung als hiv-integrase-inhibitoren
MX2008006586A (es) Composicion edulcorante de alta potencia con un agente antiinflamatorio y composiciones edulcoradas con la misma
AR043150A1 (es) Composicion oral que contiene enzimas con estabilidad mejorada
BRPI0518973A2 (pt) xampu condicionador contendo partÍculas de silicone estabilizadas
ATE426597T1 (de) Benzamidderivate und deren verwendung als glucokinaseaktivierende mittel
ATE459621T1 (de) Benzisoxazolpiperidinverbindungen und verfahren zu deren anwendung
DE602007012551D1 (de) Haarkonditionierungszusammensetzungen gegen schuppen
NO20043013L (no) Tetrahydrokinolin analoger som muskarine agonister
DE60315762D1 (de) Titanoxid-Dispersionszusammensetzung
NO20052534D0 (no) Oksazolidinon- og/eller isokazolinderivater som antibakterielle stoffer
ATE548019T1 (de) Hautaufhellende mittel, zusammensetzungen und verfahren
DK1608344T3 (da) Orale cladribin-formuleringer
CY1111768T1 (el) Νεος παραγοντας μειωσης τριγλυκεριδιου
BRPI0406734A (pt) Composição termiticida, e, método para controlar térmitas
ATE256124T1 (de) Substituierte benzimidazole, ihre herstellung und ihre verwendung als mittel gegen parasitäre protozoen
FR2821551B1 (fr) Utilisations de derives de polyaminoacides comme agents hydratants, et compositions cosmetiques ou pharmaceutiques les comprenant
DE602005025764D1 (de) Kosmetische zusammensetzung mit polyorganosiloxan und ihre anwendung
TW200612999A (en) Stable dentifrice compositions
FR2894825B1 (fr) Nouvelle association d&#39;un inhibiteur du courant if sinusal et d&#39;un inhibiteur de l&#39;enzyme de conversion et les compositions pharmaceutiques qui la contiennent
WO2007027519A3 (en) Compositions and methods for darkening keratinous fibers

Legal Events

Date Code Title Description
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B15K Others concerning applications: alteration of classification

Free format text: A CLASSIFICACAO ANTERIOR ERA: A61K 7/00

Ipc: A61K 8/25 (2006.01), A61K 8/44 (2006.01), A61K 8/4

B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: INDEFIRO O PEDIDO DE ACORDO COM O ARTIGO 8 C/C 13 DA LPI.

B12B Appeal against refusal [chapter 12.2 patent gazette]
B08F Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette]
B08K Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette]