BR9811048A - Processo para preparação de um composto - Google Patents
Processo para preparação de um compostoInfo
- Publication number
- BR9811048A BR9811048A BR9811048-9A BR9811048A BR9811048A BR 9811048 A BR9811048 A BR 9811048A BR 9811048 A BR9811048 A BR 9811048A BR 9811048 A BR9811048 A BR 9811048A
- Authority
- BR
- Brazil
- Prior art keywords
- compound
- general formula
- optionally substituted
- alkyl
- hydrogen
- Prior art date
Links
- 150000001875 compounds Chemical class 0.000 title abstract 5
- 238000004519 manufacturing process Methods 0.000 title 1
- WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 abstract 6
- 125000005843 halogen group Chemical group 0.000 abstract 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 3
- 125000000217 alkyl group Chemical group 0.000 abstract 3
- 229910052739 hydrogen Inorganic materials 0.000 abstract 3
- 239000001257 hydrogen Substances 0.000 abstract 3
- 238000000034 method Methods 0.000 abstract 3
- 125000003342 alkenyl group Chemical group 0.000 abstract 2
- 125000000304 alkynyl group Chemical group 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 230000000802 nitrating effect Effects 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid group Chemical class S(O)(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
- C07C201/06—Preparation of nitro compounds
- C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/40—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reactions not involving the formation of sulfonamide groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Cephalosporin Compounds (AREA)
Abstract
"PROCESSO PARA A PREPARAçãO DE UM COMPOSTO". Um processo para a preparação de um composto de fórmula geral (I) em que R^ 1^ é hidrogênio ou alquila C~ 1~-C~ 6~, alquenila C~ 2~-C~ 6~, ou alquinila C~ 2~-C~ 6~, qualquer um dos quais pode ser opcionalmente substituído por um ou mais substituintes selecionados a partir de halogênio e OH; ou COOR^ 4^, COR^ 6^, CONR^ 4^R^ 5^ ou CONHSO~ 2~R^ 4^; R^ 4^ e R^ 5^ são cada qual independentemente hidrogênio ou alquila C~ 1~-C~ 4~ opcionalmente substituídos por um ou mais átomos de halogênio; R^ 6^ é um átomo de halogênio ou um grupo R^ 4^; R^ 2^ é hidrogênio ou halo; R^ 3^ é alquila C~ 1~-C~ 4~, alquenila C~ 2~-C~ 4~ ou alquinila C~ 2~-C~ 4~, qualquer um dos quais pode ser opcionalmente substituído por um ou mais átomos de halogênio; ou halo; o processo compreendendo reagir um composto de fórmula geral (II) em que R^ 1^, R^ 2^ e R^ 3^ são como definidos para a fórmula geral (I) com um agente de nitração compreendendo ácidos nítrico e sulfúrico na presença de um solvente orgânico e na presença de anidrido acético, a razão molar de anidrido acético para o composto de fórmula geral (II) sendo de cerca de 1:1 a 3:1, <MU>caracterizado<MV> pelo fato de que os ácidos são adicionados sequencialmente à mistura da reação.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/901,545 US6028219A (en) | 1995-09-13 | 1997-07-28 | Process for the nitration of diphenylethers |
| PCT/GB1998/001991 WO1999005087A1 (en) | 1997-07-28 | 1998-07-07 | Nitration process for diphenyl ethers |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR9811048A true BR9811048A (pt) | 2000-09-05 |
Family
ID=25414397
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR9811048-9A BR9811048A (pt) | 1997-07-28 | 1998-07-07 | Processo para preparação de um composto |
Country Status (18)
| Country | Link |
|---|---|
| US (1) | US6028219A (pt) |
| EP (1) | EP1000010B1 (pt) |
| JP (1) | JP2001510818A (pt) |
| KR (1) | KR100571093B1 (pt) |
| CN (1) | CN1176899C (pt) |
| AR (1) | AR015137A1 (pt) |
| AT (1) | ATE224865T1 (pt) |
| AU (1) | AU8346998A (pt) |
| BR (1) | BR9811048A (pt) |
| CA (1) | CA2291438C (pt) |
| DE (1) | DE69808300T2 (pt) |
| DK (1) | DK1000010T3 (pt) |
| ES (1) | ES2180186T3 (pt) |
| HU (1) | HUP0002525A3 (pt) |
| IL (1) | IL133151A (pt) |
| TW (1) | TW436472B (pt) |
| WO (1) | WO1999005087A1 (pt) |
| ZA (1) | ZA986637B (pt) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9930369D0 (en) * | 1999-12-22 | 2000-02-09 | Zeneca Ltd | Chemical process |
| DE10196234B4 (de) * | 2000-05-26 | 2008-04-30 | Engelhard Lyon S.A. | Verfahren zur Herstellung eines Verbundprodukts aus Kollagen für die Gewebebildung und seine Verwendung |
| DE102007010161A1 (de) * | 2007-03-02 | 2008-09-04 | Saltigo Gmbh | Verfahren zur Nitrierung substituierter Benzole in Gegenwart von Propionsäure |
| CN102329255B (zh) * | 2011-10-31 | 2013-11-13 | 江苏长青农化股份有限公司 | 定向硝化合成氟磺胺草醚工艺 |
| CN103387524B (zh) * | 2013-07-23 | 2015-04-15 | 山东科源化工有限公司 | 一种氟磺胺草醚的制备方法 |
| CN112358400A (zh) * | 2020-10-22 | 2021-02-12 | 烟台大学 | 一种微反应器中硝化合成三氟羧草醚的方法 |
| CN115403488B (zh) * | 2021-05-27 | 2024-07-19 | 江苏联化科技有限公司 | 氟磺胺草醚的制备方法 |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5248173B2 (pt) * | 1973-02-20 | 1977-12-08 | ||
| US4031131A (en) * | 1975-09-29 | 1977-06-21 | Rohm And Haas Company | Process for preparing phenoxybenzoic acids |
| GB1478428A (en) * | 1975-12-11 | 1977-06-29 | Ishihara Sangyo Kaisha Kk | Substituted diphenylethers and herbicidal composition thereof |
| DE2960664D1 (en) * | 1978-01-19 | 1981-11-19 | Ici Plc | Diphenyl ether compounds useful as herbicides; methods of using them, processes for preparing them, and herbicidal compositions containing them |
| DE3071736D1 (en) * | 1979-06-22 | 1986-10-09 | Rhone Poulenc Agrochimie | Process for preparing 2-nitro-5-(substituted-phenoxy) benzoic acids and salts thereof |
| US4400530A (en) * | 1980-06-27 | 1983-08-23 | Ppg Industries, Inc. | Process for preparing substituted diphenyl ethers |
| US4594440A (en) * | 1981-07-27 | 1986-06-10 | Rhone:Pulenc, Inc. | Process for recovering and purifying herbicidal phenoxybenzoic acid derivatives |
| US4405805A (en) * | 1981-07-27 | 1983-09-20 | Rhone-Poulenc, Inc. | Process for recovering and purifying herbicidal phenoxybenzoic acid derivatives |
| US4424393A (en) * | 1981-08-24 | 1984-01-03 | Ppg Industries, Inc. | Process of preparation of substituted diphenyl ethers |
| US4743703A (en) * | 1981-10-19 | 1988-05-10 | Rohm And Haas Company | Herbicidal 4-fluoroalkyl-4'-nitrodiphenyl ethers |
| US4429146A (en) * | 1982-04-15 | 1984-01-31 | Gaf Corporation | Substituted diphenyl ether herbicides and process for use |
| DE3247669A1 (de) * | 1982-12-23 | 1984-06-28 | Basf Ag, 6700 Ludwigshafen | Neue phenylglyoxylsaeurederivate, verfahren zu ihrer herstellung und ihre verwendung zur bekaempfung unerwuenschten pflanzenwuchses |
| DE3322817A1 (de) * | 1983-06-24 | 1985-01-10 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von nitrierten diphenylethern |
| EP0147798B1 (en) * | 1984-01-03 | 1989-11-23 | General Electric Company | Nitration reactions with acid anhydride promoters |
| HU190222B (en) * | 1984-01-17 | 1986-08-28 | Budapesti Vegyimuevek,Hu | Fungicide comprising substituted phenoxy-benzaldehyde as active substance |
| HU193194B (en) * | 1984-01-17 | 1987-08-28 | Budapesti Vegyimuevek | Fungicide compositions containing phenoxy-benzaldehyde derivatives as active substances and process for preparing the active substances |
| GB8628109D0 (en) * | 1986-11-25 | 1986-12-31 | Ici Plc | Chemical process |
| HU200538B (en) * | 1987-06-16 | 1990-07-28 | Budapesti Vegyimuevek | Herbicidal compositons with improves selectivity and process for producing the two active ingredients in one reaction step |
| PT101207A (pt) * | 1993-02-26 | 1994-08-31 | Inst Nac De Engenharia E Tecno | Processo para a nitracao de compostos aromaticos em condicoes suaves e nao corrosivas |
| DE69503936T2 (de) * | 1994-02-17 | 1998-12-10 | Zeneca Ltd., London | Verfahren zur Phosgenierung in Gegenwart des Acetonitrils |
| GB9518705D0 (en) * | 1995-09-13 | 1995-11-15 | Zeneca Ltd | Chemical process |
| DK0937015T3 (da) * | 1996-11-01 | 2001-11-19 | Syngenta Ltd | Nitreringsfremgangsmåde |
-
1997
- 1997-07-28 US US08/901,545 patent/US6028219A/en not_active Expired - Lifetime
-
1998
- 1998-07-07 CN CNB988076101A patent/CN1176899C/zh not_active Expired - Lifetime
- 1998-07-07 KR KR1020007000887A patent/KR100571093B1/ko not_active Expired - Lifetime
- 1998-07-07 HU HU0002525A patent/HUP0002525A3/hu unknown
- 1998-07-07 DE DE69808300T patent/DE69808300T2/de not_active Expired - Fee Related
- 1998-07-07 DK DK98933766T patent/DK1000010T3/da active
- 1998-07-07 EP EP98933766A patent/EP1000010B1/en not_active Expired - Lifetime
- 1998-07-07 WO PCT/GB1998/001991 patent/WO1999005087A1/en not_active Ceased
- 1998-07-07 AT AT98933766T patent/ATE224865T1/de not_active IP Right Cessation
- 1998-07-07 CA CA002291438A patent/CA2291438C/en not_active Expired - Lifetime
- 1998-07-07 IL IL13315198A patent/IL133151A/en not_active IP Right Cessation
- 1998-07-07 BR BR9811048-9A patent/BR9811048A/pt not_active Application Discontinuation
- 1998-07-07 ES ES98933766T patent/ES2180186T3/es not_active Expired - Lifetime
- 1998-07-07 JP JP2000504089A patent/JP2001510818A/ja active Pending
- 1998-07-07 AU AU83469/98A patent/AU8346998A/en not_active Abandoned
- 1998-07-13 TW TW087111326A patent/TW436472B/zh not_active IP Right Cessation
- 1998-07-24 ZA ZA986637A patent/ZA986637B/xx unknown
- 1998-07-27 AR ARP980103687A patent/AR015137A1/es active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| IL133151A (en) | 2002-11-10 |
| TW436472B (en) | 2001-05-28 |
| ES2180186T3 (es) | 2003-02-01 |
| KR20010022308A (ko) | 2001-03-15 |
| EP1000010A1 (en) | 2000-05-17 |
| AU8346998A (en) | 1999-02-16 |
| DK1000010T3 (da) | 2003-02-03 |
| CA2291438C (en) | 2007-10-16 |
| CN1176899C (zh) | 2004-11-24 |
| AR015137A1 (es) | 2001-04-18 |
| HUP0002525A2 (hu) | 2000-11-28 |
| ATE224865T1 (de) | 2002-10-15 |
| US6028219A (en) | 2000-02-22 |
| EP1000010B1 (en) | 2002-09-25 |
| DE69808300D1 (de) | 2002-10-31 |
| JP2001510818A (ja) | 2001-08-07 |
| IL133151A0 (en) | 2001-03-19 |
| WO1999005087A1 (en) | 1999-02-04 |
| CN1266422A (zh) | 2000-09-13 |
| DE69808300T2 (de) | 2003-05-15 |
| KR100571093B1 (ko) | 2006-04-13 |
| ZA986637B (en) | 1999-01-28 |
| CA2291438A1 (en) | 1999-02-04 |
| HUP0002525A3 (en) | 2001-02-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B25D | Requested change of name of applicant approved | ||
| B25G | Requested change of headquarter approved | ||
| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] | ||
| B08G | Application fees: restoration [chapter 8.7 patent gazette] | ||
| B25G | Requested change of headquarter approved | ||
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: INDEFIRO O PRESENTE PEDIDO DE PATENTE DE ACORDO COM ART. 8O DA LPI. |
|
| B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |