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AU2014203147B2 - High level haloxyfop emulsifiable concentrate formulation - Google Patents

High level haloxyfop emulsifiable concentrate formulation Download PDF

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AU2014203147B2
AU2014203147B2 AU2014203147A AU2014203147A AU2014203147B2 AU 2014203147 B2 AU2014203147 B2 AU 2014203147B2 AU 2014203147 A AU2014203147 A AU 2014203147A AU 2014203147 A AU2014203147 A AU 2014203147A AU 2014203147 B2 AU2014203147 B2 AU 2014203147B2
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ionic surfactant
haloxyfop
teric
surfactant
agriculturally acceptable
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AU2014203147A1 (en
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Ross Rainbird
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Imtrade Australia Pty Ltd
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Imtrade Australia Pty Ltd
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Abstract

11/06/14,jb20952 cap specification.doex,222 - 222 An emulsifiable concentrate formulation of haloxyfop or at least one haloxyfop derivative or a mixture thereof including: haloxyfop or at least one haloxyfop derivative or a mixture thereof comprising at least 650 g/L of the emulsifiable concentrate formulation on a gram haloxyfop acid equivalent per litre basis, at least one solid, liquid-containing or liquid agriculturally acceptable surfactant, and, optionally, at least one agriculturally acceptable solvent, wherein the liquid components of the emulsifiable concentrate formulation form a solubilising moiety for haloxyfop or haloxyfop derivative and wherein the weight ratio of haloxyfop or haloxyfop derivative to solubilising moiety is greater than 2, preferably greater than 3, and more preferably greater than 4.

Description

FIELD OF THE INVENTION [0001] This invention relates to liquid formulations of the selective herbicide haloxyfop. In particular the invention relates to emulsifiable concentrate formulations of haloxyfop that contain a high level of active agent.
BACKGROUND OF THE INVENTION [0002] Haloxyfop is a member of the aryloxyphenoxy-propionate (or
FOP) class of herbicides. Other members of the class include diclofop-methyl, fluazifop-P-butyl and quizalofop-P-methyl. FOPs are generally used for the post-emergent control of grasses in broad-leaf crops.
[0003] Haloxyfop in formulations may be presented as haloxyfop acid (molecular weight 361.7), haloxyfop methyl ester (molecular weight 375.73), or as another haloxyfop acid derivative. Different enantiomers of haloxyfop have different herbicidal activity, and it is usual that the most active enantiomer is used in formulations. It is conventional to quote the amount of haloxyfop in a formulation on an acid equivalent basis. Thus for example a formulation containing haloxyfop-methyl at 540 g/L will be quoted as containing haloxyfop at 520 g/L on an acid-equivalent (a.e.) basis.
[0004] Teachings in patent literature have included combinations of
FOPs and safeners to increase weed control (US 2006/0014643), the use of delayed-release liquid formulations of fatty acid synthase inhibitors (including FOPs), for example, microcapsule formulations or wax dispersions, and the use of FOPs as synergistic agents in conjunction with herbicidal 2-phenyl-4(hetero-)aryloxypyrimidines.
11/06/14,jb20952 cap specification.docx,2
-22014203147 11 Jun2014 [0005] A range of haloxyfop emulsifiable concentrates comprising 520 g/L Haloxyfop have been sold in Australia by the following organisations or businesses: 4 Farmers (as Haloxyfop 520), Agri West (as AW Harpoon 520), Imtrade Australia (as Chemag Haloxyfop 520, and as Imtrade haloxyfop 520 EC), Chemforce 2010 (as Chemforce Haloxyfop 520), Grow Choice (as Choice Halofop 520), Conquest Crop Protection (as Conquest Recon 520), Ospray (as Convict), Crop Care Australasia (as Exert 520), Farmalinx (as Farmalinx Haloxyfop 520 EC), Farmoz (as Farmoz Firepower), Macspred (as Generex Haloxyfop, and as Macspred Halomac 520), Fandmark Operations (as Genfarm Haloxyfop 520), Echem Australia (as Halox 520), Sipcam Pacific Australia (as Inquest), Kenso Corporation (as Kenso Agcare Haloxyken 520), Shandong rainbow International (as Rainbow Haloxyfop 520), Rygel Australia (as Rygel Haloxyfop 520), Dow Agrosciences Australia (as verdict 520), and Agricultural Product Services (as Whitestar Haloxyfop 520).
[0006] Each of the above commercially available haloxyfop EC formulations contains at most 520 g/E of haloxyfop active ingredient (acid equivalent basis), which suggests that 520 g/L represents an upper practical limit in the amount of haloxyfop that can be packaged in EC form using methods currently known to the art.
[0007] Many general characteristics of emulsifiable concentrate formulations have been described in US 2003/0072776 (Sun et al., filed July 2001). The Sun specification provides the following teachings about emulsifiers, solvents and optional ingredients.
Emulsifiers [0008] The emulsifiers of the emulsifiable concentrates comprise at least one emulsifier, which may be a non-ionic surfactant, an ionic surfactant, or a blend of both types of surfactants. It is also possible that an emulsifier in an emulsifiable concentrate may be a cationic surfactant. Useful non-ionic
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-32014203147 11 Jun2014 surfactants are said to include alkoxylated block polymers, alkoxylated alcohols, alkoxylated alkylphenols, alkoxylated amines, alkoxylated amides, alkoxylated fatty esters, alkoxylated oils, fatty esters, alkoxylated fatty acids, sorbitan derivatives, and the like.
[0009] It is possible that the emulsifier comprises a zwitterionic surfactant (i.e., a surfactant which simultaneously carries anionic and cationic charge). Examples of zwitterioninc surfactants include betaine surfactants.
[0010] Typical ionic surfactants found in emulsifiers include alkylaryl sulfonates; alkylarylsulfonic acids; carboxylated alcohol ethoxylates and alkylphenol ethoxylates; carboxylic acids/fatty acids; diphenyl sulfonate derivatives; olefin sulfonates; phosphate esters; phosphorus organic derivatives; quaternary surfactants; sulfates and sulfonates of oils and fatty acids; sulfates and sulfonates of ethoxylated alkylphenols; sulfates of ethoxylated alcohols; sulfates of fatty esters; sulfonates of dodecyl and tridecylbenzenes; sulfonates of naphthalene and alkyl naphthalene; sulfonates of petroleum; sulfosuccinamates; alkanolamides; alkoxylated amines (with low EO values); sarcosine derived surfactants such as, ammonium lauroyl sarcosinate, and the like.
[0011] Preferred emulsifiers may be alkoxylated alcohols and alkyphenols, preferably of from about 4 to about 50 ethylene oxide units and a hydrophobe of from about 4 to about 16 carbon atoms. Other preferred surfactants may be alkylphenol EO/PO block copolymers, e.g., that sold under the trade name WITCONOL NS 108 LQ, and alkoxylated amine salts of ethoxylated alkylphenol sulfates, e.g., that supplied under the trade name WITCOLATE 1335 by Crompton Corporation, Witco Group.
[0012] Developing an effective emulsifier package (blend of emulsifiers) requires careful screening of potential emulsifiers (surfactants), conducting emulsion tests according to prescribed methods or established
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-42014203147 11 Jun2014 laboratory protocols, and optimizing the performance of the most promising emulsifier(s). The screening of potential emulsifier packages is dependent upon pesticide active type, and solvents. Those skilled in the art of EC technology understand the importance of hydrophilic-lipophilic balance and surfactant choice for such formulations. The emulsifier (surfactant) is preferably present at from about 1 to about 50 weight percent of the emulsifiable concentrate, more preferably from about 3 to about 10 weight percent.
Solvents [0013] The selection of a suitable solvent system is made by taking into consideration the solubility of the active(s) and the chemical and toxicological profiles of the solvent(s). The solvents include all EPA approved solvents, and the list of suitable solvents may include aliphatic paraffinic oils, such as kerosene or refined paraffins; aromatic solvents, such as xylenes; C9-C12 aromatic solvents, such as supplied under the trade names AROMATIC 100, 150, and 200 (as sold by Exxon Chemical), ISOPAR L, SOLVESSO 100, 150, and 200; chlorinated hydrocarbons, such as chlorobenzene; alcohols, such as butanol and benzyl alcohol; ketones, such as cyclohexanone and N-methyl pyrollidone; and ethers, such as diethylene glycol and diethoxol. In addition, the solvent may include vegetable oils, methylated vegetable oils, petrol-oils, sugar esters of fatty acids, e.g., sucrose esters, and the like.
[0014] Preferred solvents may be C9-C12 hydrocarbon solvents because of their low cost and their ability to solubilize many pesticide toxicants.
[0015] Sun teaches that the solvent may be present at from 0 to about weight percent of the emulsifiable concentrate, preferably from about 20 to about 50 weight percent.
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-52014203147 11 Jun2014
Optional Ingredients [0016] Other additives may be included in emulsifiable concentrate formulations of active ingredient and at levels less than about 5 weight percent. Such additives can include, for example, an antifreeze, a pH buffer, a finely divided hydrophobic filler, a perfume, an antifoam, a stenching agent, or an embittering agent (the latter two agents to discourage ingestions).
[0017] Sun also teaches that emulsifiable concentrates according to the invention disclosed therein can be diluted with water to a desired solids or active ingredient level and applied to the targets using suitable means. Typically according to Sun, the amount of active component in the final formulations prior to dilution is from about 1 to about 95 weight percent.
[0018] Hereafter in this specification, the term “haloxyfop” will be taken to refer to each and any haloxyfop acid or haloxyfop acid derivative moiety present in the formulation.
[0019] In the present specification, the term “solubilising moiety for haloxyfop” is to be taken to refer to any liquid system in which haloxyfop is miscible, including liquid systems that include conventional agriculturally acceptable solvents and also liquid systems that include conventional agriculturally acceptable liquid, or liquid-containing, surfactants, provided that haloxyfop dissolves in said liquid systems. A solubilising moiety for haloxyfop may contain one, two or even more liquid components. The weight of a solubilising moiety for haloxyfop is taken to be the sum of weights of liquid components that constitute the solubilising moiety system for haloxyfop. For the avoidance of doubt, if a solubilising moiety for haloxyfop happens to include one or more solubilised solids (e.g. a solid dissolved surfactant), the weight of the solubilising moiety for haloxyfop is taken to be the sum of the weights of the liquid components of the solubilising moiety system for haloxyfop, but does not include the weights of non-haloxyfop solid
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-62014203147 11 Jun2014 components that may be dissolved. The term “agriculturally acceptable solvent for haloxyfop” will be taken to refer to solvents for haloxyfop wherein each component of the solvent has been approved for inclusion in an agricultural formulation in at least one country. “Agriculturally acceptable” means registered or otherwise approved for use in agriculture in at least one country.
[0020] Haloxyfop-methyl quantities are to be calculated in terms of haloxyfop acid equivalent.
[0021] The “haloxyfop /solubilising moiety ratio” in a haloxyfop EC, which may be calculated by dividing the weight of haloxyfop moieties (as acidequivalent weights) in a given weight of haloxyfop EC formulation by the weight of the solubilising moiety for haloxyfop in the same weight of haloxyfop EC formulation, is an important ratio in terms of:
1. The quantity of solvent released to the environment as a consequence of applying a given amount of haloxyfop formulation to a cultivation zone;
2. The amount of high-quality packaging material that is utilised in carrying a given amount of haloxyfop active ingredient to a cultivation zone;
3. The amount of used packaging material that needs to be recycled or otherwise disposed of after applying a given amount of haloxyfop active ingredient to a cultivation zone;
4. The contact toxicity of haloxyfop EC formulation to a farm worker;
5. The flammability of haloxyfop EC formulation;
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-72014203147 11 Jun2014
6. The vapour pressure of solvent (frequently aromatic hydrocarbon) that is released to air in a given time after a spill has occurred;
7. The weight of goods that must be carried by a farm worker in applying a given amount of haloxyfop active ingredient to a cultivation zone;
8. The cost of freight (volume and weight basis) in transporting the haloxyfop formulation from factory to field;
9. The capacity to demonstrate superior formulation expertise to farmers.
[0022] Most, if not all, of the above parameters are improved when a given amount of haloxyfop in an EC formulation is associated with a lesser amount of solubilising moiety, i.e., when the haloxyfop/ solubilising moiety ratio is greater.
[0023] As an illustration of prior art one may consider, a conventional commercial haloxyfop EC formulation with a density of 1160 g/L and consisting of the following ingredients:
Component Parts by Weight g/L
Haloxyfop-P-methyl 97.4% technical 554.6
Diethylene glycol monomethyl ether 525.4
Ionic surfactant (60% solid in 40% 2-ethylhexanol), e.g. alkylbenzenesulfonic acid, calcium salt (e.g. Ninate 60E) 10
Non-ionic surfactant (solvent-free solid) e.g. alkyl polyoxyalkylene ether (e.g. Termul 203) 70
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-82014203147 11 Jun2014 [0024] In the above formulation haloxyfop (as methyl ester, molecular weight = 375.73) is present at 0.974 x 554.6 = 540 parts by weight. This corresponds to 520 parts by weight of haloxyfop acid equivalent, molecular weight 361.7). Solubilising moiety is present at 525.4 + 0.4x10 = 529.4 parts by weight. The haloxyfop/solubilising moiety ratio is thus 520/525.4 = 0.99. The prior art formulation may be referred to as Haloxyfop 520, reflecting the weight content of haloxyfop acid equivalents.
DESCRIPTION OF THE INVENTION [0025] According to one aspect of the present invention there is provided an emulsifiable concentrate formulation of haloxyfop or haloxyfop derivatives including haloxyfop or at least a haloxyfop derivative and an agriculturally acceptable solvent for haloxyfop, wherein the weight ratio of haloxyfop moieties on an acid equivalent basis to solvent is greater than 2, preferably greater than 3 and more preferably greater than 4.
[0026] An emulsifiable concentrate formulation of haloxyfop or haloxyfop derivative or mixture thereof including: haloxyfop or haloxyfop derivative or mixture thereof comprising at least 650 g/L of the emulsifiable concentrate formulation on a haloxyfop acid equivalent basis, at least one solid, liquid-containing or liquid agriculturally acceptable surfactant, and, optionally, at least one agriculturally acceptable solvent, wherein the liquid components of the emulsifiable concentrate formulation form a solubilising moiety for haloxyfop or haloxyfop derivative and wherein the weight ratio of haloxyfop or haloxyfop derivative to solubilising moiety is greater than 2, preferably greater than 3, and more preferably greater than 4.
[0027] The agriculturally acceptable solvent comprises at least one member of the set consisting of alkane compounds, aromatic compounds, alkylaryl compounds, alcohol-containing compounds, ether-containing compounds, ester-containing compounds, ketone-containing compounds,
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-92014203147 11 Jun2014 lactam-containing compounds, amide-containing compounds, and chlorinated compounds.
[0028] The agriculturally acceptable solvent may include at least one member of the set consisting of solvent naphtha (petroleum), heavy aromatic fraction, xylene, toluene, pyrrolidones including N-alkylated pryrrolidones such as n-methyl pyrrolidone, cyclohexanone, acetone, glycol ethers such as diethyleneglycol monomethyl ether (including the material sold under the trade name Carbitol), ethyleneglycolmonobutylethers (including the material sold under the trade name Butyl Glysolv), Propylene glycol monomethyl ether (including the material sold under the trade name Glysolv PM), methanol, ethanol, isopropanol, decanol, paraffins, hexane, and acetic acid C6-Cs branched alkyl ester (including the material sold under the trade name Exxate 700).
[0029] Preferably, the agriculturally acceptable solvent may include at least one member of the set consisting of glycol ethers and alkyl glycol ethers.
[0030] More preferably, the agriculturally acceptable solvent may comprise at least one member of the set consisting of methyl, ethyl or butyl ethers of ethylene glycol or diethylene glycol or triethylene glycol or propylene glycol or dipropylene glycol.
[0031] Alternatively, the agriculturally acceptable solvent may include at least one member of the set consisting of diethylene glycol monoethyl ether, propylene glycol monomethyl ether, and ethylene glycol monobutyl ether.
[0032] The agriculturally acceptable solvent may comprise less than
350 g/L, preferably less than 280 g/L, and more preferably less than 220 g/L of the emulsifiable concentrate formulation.
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- 102014203147 11 Jun2014 [0033] The agriculturally acceptable solvent may be in the range of 80 350 g/L, preferably in the range of 120 - 280 g/L, and more preferably in the range of 160 - 220 g/L.
[0034] An emulsifiable concentrate formulation according to the present invention may include at least one agriculturally acceptable surfactant, and wherein the cumulative amount (net of carrier solvent) of the at least one agriculturally acceptable surfactants is at least 30 g/L, preferably at least 45, and more preferably at least 60 g/L.
[0035] The at least one agriculturally acceptable surfactant may comprise a non-ionic surfactant.
[0036] The at least one agriculturally acceptable non-ionic surfactant may be chosen from the categories in the set consisting of alkoxylated block polymers, alkoxylated alcohols, alkoxylated alkylphenols, alkoxylated amines, alkoxylated amides, alkoxylated fatty esters, alkoxylated oils, fatty esters, alkoxylated fatty acids, and sorbitan derivatives.
[0037] The non-ionic surfactant may comprise at least one member of the set consisting of (i) ethylene oxide/propylene oxide block copolymers and block copolymer derivatives including alkyl derivatives, and (ii) alkyl phenol ethoxylates wherein the alkyl chain has between 7 and 11 carbon atoms and there are 7 to 11 ethylene oxide moieties (average basis).
[0038] The at least one agriculturally acceptable non-ionic surfactant may be chosen from the set consisting of (i) butyl ethylene oxide/propylene oxide copolymer having an average molecular weight in the range 2000 - 4000, (ii) alcohol alkoxylate with ethylene oxide 22-28 moles and propylene oxide 25-35 moles and a PO/EO ratio of about 1.2/1, and (iii) nonylphenol with 8 or 9 or 10 ethoxylates (average basis).
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2014203147 11 Jun2014
- 11 [0039] The cumulative amount (net of carrier solvent if any) of nonionic surfactant may comprise at least 30 g/L, preferably at least 45 g/L, and more preferably at least 60 g/L.
[0040] Alternatively, in an emulsifiable concentrate formulation according to the present invention, the at least one agriculturally acceptable surfactant may comprise an anionic surfactant.
[0041] The at least one agriculturally acceptable ionic surfactant may be chosen from the categories in the set consisting of alkylaryl sulfonates; alkylarylsulfonic acids; carboxylated alcohol ethoxylates and alkylphenol ethoxylates; carboxylic acids/fatty acids; diphenyl sulfonate derivatives; olefin sulfonates; phosphate esters; phosphorus organic derivatives; sulfates and sulfonates of oils and fatty acids; sulfates and sulfonates of ethoxylated alkylphenols; sulfates of ethoxylated alcohols; sulfates of fatty esters; sulfonates of dodecyl and tridecylbenzenes; sulfonates of naphthalene and alkyl naphthalene; sulfonates of petroleum; sulfosuccinamates; alkoxylated amines; sarcosine derived surfactants, such as ammonium lauroyl sarcosinate, and alkoxylates as above other than ethoxylates (such as propoxylates, butoxylates).
[0042] The at least one agriculturally acceptable ionic surfactant may be chosen from the set consisting of linear and branched alkylbenzenesulphonates and salts thereof which may be provided as a solution in a solvent such as calcium C10-C14 alkylbenzenesulfonate (including materials sold under the trade name NANSA EVM70/2E which is carried in 2 ethylhexanol or under the trade name Ninate 60E which is also carried in 2 ethylhexanol), alkyl sulphates such as sodium lauryl sulphate (including material sold under the trade name Empicol LX/N), alkyl ether sulfates such as sodium lauryl ether (2EO) sulphate (including material sold under the trade name Emipmin KESX70/AU), alkyl phosphates (including material sold under the trade names Alkanate PA100, Alkanate PG30, and Alkanate PL50), alkyl
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- 122014203147 11 Jun2014 ether phosphates (including material sold under the trade name Alkanate PK100), alkylphenol ether sulfate/tallow amine ethoxylate salts (including materials sold under the trade names Toximul TANS-5, Toximul TANS-6, Toximul TANS-8, Toximul TANS-15), and alcohol ether sulphate/tallow amine ethoxylate salts (including materials sold under the trade names Toximul TAABS-5, Toximul TAABS-8).
[0043] Preferably, the at least one agriculturally acceptable ionic surfactant may be chosen from the set consisting of linear and branched alkylbenzenesulphonates and salts thereof which may be provided as a solution in a solvent such as calcium C10-C14 alkylbenzenesulfonate (including materials sold under the trade name NANSA EVM70/2E which is carried in 2 ethylhexanol, and material sold under the trade name Ninate 60E which is also carried in 2-ethyl hexanol), alkylphenol ether sulfate/tallow amine ethoxylate salts (including materials sold under the trade names Toximul TANS-5, Toximul TANS-6, Toximul TANS-8, )and alcohol ether sulphate/tallow amine ethoxylate salts (including materials sold under the trade names Toximul TAABS-5).
[0044] An emulsifiable concentrate formulation according to the present invention may include at least one agriculturally acceptable ionic surfactant, wherein the cumulative amount (net of carrier solvent) of the at least one agriculturally acceptable anionic surfactants is at least 8 g/L, preferably at least 11 g/L, and more preferably at least 14 g/L.
[0045] An emulsifiable concentrate formulation according to the present invention may include at least one agriculturally acceptable non-ionic surfactant wherein the cumulative amount (net of carrier solvent) of the at least one agriculturally acceptable non-ionic surfactant is at least 40 g/L, preferably at least 60 g/L, and more preferably at least 80 g/L.
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2014203147 11 Jun2014
- 13 [0046] An emulsifiable concentrate formulation according to the present invention may comprise about 700 - 950 g/L haloxyfop-P-methyl, 160 200 g/L diethyleneglycolmonoethyl ether, 45 - 70 g/L non-ionic surfactant comprising ethylene oxide-propylene oxide block copolymer moieties of molecular weight 1500 - 4500 , and 14 - 18 g/L of C12-C16 linear or branched calcium alkyl benzene sulfonate.
[0047] An emulsifiable concentrate formulation according to the present invention has the density of at least 1.00 g/ml and preferably at least 1.15 g/ml.
[0048] Formulations incorporating diluted emulsifiable concentrate according to the present invention may be used for selectively killing or suppressing weeds such as barley grass, brome grass, paradoxa grass, volunteer cereals, wild oats, musky or ferny leaf Storksbill, common crowsfoot, common storksbill, long or shiny leaf storksbill, couch grass, Rhodes grass, Australian millet, barnyard grass, green panic, Johnson grass, liverseed grass, Mossman river grass, summer grass, slender rats tail grass, Buffel grass, kikuyu, paspalum spp, starai spp, annual ryegrass, lesser canary grass, Rope twitch, Erodium spp.
DESCRIPTION OF PREFERRED EMBODIMENTS AND EXAMPLES OF THE INVENTION [0049] In order that the present invention may be more readily comprehended, one or more preferred embodiments are described hereinafter.
EXAMPLE 1 [0050] The following haloxyfop emulsifiable concentrate according to the invention was made by mixing the following components:
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- 142014203147 11 Jun2014
Component Parts by Weight (g/L)
Haloxyfop-P-methyl 94% tech 994.5
Diethyleneglycol monoethyl ether 183.2
Alkylbenzenesulfonic acid, calcium salt (60% solid in 40% 2-ethylhexanol) e.g. Ninate 60E 26.2
Alkyl polyoxyalkylene ether e.g. Termul 203. (solvent-free solid) 61.1
[0051] In the above formulation haloxyfop (as methyl ester, molecular weight = 375.73) is present at 0.94 x 994.5 = 934.83 parts by weight. This corresponds to 900 parts by weight of haloxyfop acid equivalent (molecular weight 361.7). Solubilising moiety is present at 183.2 + 0.4x26.2 = 193.68 parts by weight. The haloxyfop/solubilising moiety ratio is thus 900/193.68 = 4.65. The density of the formulation is 1265 g/L.
[0052] In Example 1, the formulation procedure for a nominal 10,000 L batch of the material is as follows, with steps being identified numerically as 1.1, 1.2, 1.3, and so on:
[0053] 1.1 Ensure formulation vessel is empty and clean.
[0054] 1.2 Charge the formulation vessel with solvent as follows with agitator off:
1. Diethylene glycol monethyl ether 1550 kg
[0055] 1.3 Charge the formulation vessel with active ingredient, with intermittent agitation following the addition of every 1000 kg or so. As haloxyfop-P-methyl technical material can be of such a viscosity that the material is not amenable to pumping at temperatures of the order of 30°C and
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- 15 below (depending on the ambient temperature and the means of transferring the material to the formulation), gentle heating may be required to establish a lower viscosity liquid form prior to processing:
2. Haloxyfop-P-methyl 94% Tech 9945 kg
[0056] 1.4 Charge the formulation vessel with the surfactants and remaining solvent as follows, clearing residual surfactant from any pumps or process lines used with the remaining complement of solvent:
3. Alkylbenzenesulfonic acid, calcium salt in 2ethylhexanol (e.g. Ninate 60E) 262 kg
4. Alkyl polyoxyalkylene ether (e.g. Termul 203) 611kg
5. Diethylene glycol monethyl ether 282 kg
[0057] 1.5 Continue agitating for a minimum of 30 minutes following the addition of the last ingredient.
[0058] 1.6 Sample approximately IL of product, ensuring it is representative of the formulation.
[0059] 1.7 Sub-sample 250mL from the original IL sample, and subject it to the following testing regime:
[0060] 1.7.1 Specific gravity (CIPAC MT3.1)
1.7.2 pH 1% aqueous (CIPAC MT75.3)
1.7.3 Emulsion characteristics (CIPAC MT36.1)
1.7.4 Persistent foam (CIPAC MT47.2)
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- 162014203147 11 Jun2014
1.7.5 Active constituent (Haloxyfop-P-methyl) content (using a validated method meeting the requirements of APVMA).
[0061] 1.8 If specific gravity is within the bounds of the acceptable range listed in the specification, record the value and proceed to the next test. If specific gravity is outside of the bounds of the acceptable range listed in the specification, agitate the formulation charge until specific gravity is constant. If still outside of the bounds of the acceptable range, quarantine batch for further investigations and possible rework.
[0062] 1.9 If pH 1% aqueous is satisfactory, record the results and proceed to the next test. If pH 1% aqueous is outside the bounds of the acceptable range listed in the specification, quarantine the batch for further investigations and possible rework.
[0063] 1.10 If emulsion stability in standard hard water is satisfactory, record the results and proceed to the next test. If emulsion stability is outside the bounds of the acceptable range listed in the specification, adjust the contents of surfactants (Alkylbenzenesulfonic acid, calcium salt in 2ethylhexanol (Ninate 60E) and Alkyl polyoxyalkylene ether (Termul 203)). After suitable agitation time to ensure homogeneity, resample and retest.
Repeat adjustment process until emulsion stability is within the bounds of the acceptable range.
[0064] 1.11 If persistent foaming characteristics are satisfactory, record the results and proceed to the next test. If persistent foaming characteristics are outside the bounds of the acceptable range quarantine the batch for further investigations and possible rework.
[0065] 1.12 If the active constituent level is satisfactory, record results. If the active constituent level is outside the bounds of the acceptable range listed in the specification, adjust the level accordingly by adding
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- 172014203147 11 Jun2014 additional diethylene glycol monethyl ether (where the active content is high) or additional haloxyfop-P-methyl active constituent (where the active content is low). After suitable agitation time to ensure homogeneity, resample and retest. Repeat adjustment process until active constituent levels are within the bounds of the acceptable range.
[0066] 1.13 Catalogue and store a retention sample of approximately 200 g.
Tests for Confirming the Suitability of the Formulation of Example 1 [0067] For the test method identified by the prefix CIPAC, refer to
International Pesticides Analytical Council (CIPAC) published methodology.
Parameter Test Method Required Outcome Observed Outcome
appearance visual homogeneous liquid homogeneous liquid
assay validated chromatographic method, 98-102% accuracy, linearity R>0.99 875 to 925g/F 899g/F
pH(l%) CIPAC MT 75.3 4- 10 7.4
Spec Gravity (SG) CIPAC MT 3.1 1.00-3.00 1.265
Emulsion characteristics CIPAC MT 47.2 <2 ml cream and < trace oil after 30 min, complete resuspension after 24 hrs complies
Persistent foaming CIPAC MT 47.2 < 60 ml after 1 min 5 mF
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2014203147 11 Jun2014
cold stability visual no phase separation complies
viscosity 20°C Brookfield viscometer 0 - 2000 cPs 330 cPs
viscosity 5°C Brookfield viscometer 0 - 2000 cPs 1350 cPs
long term performance As above, after storage at 54°C for 2 weeks CIPAC MT 46.1 complies complies
Flash point of most volatile component Abel closed cup (diethylene glycol monoethyl ether) >60°C 96°C
Trials [0068] Series of trials were conducted to ascertain suitable solvent surfactant combinations. The haloxyfop used in the trials was haloxyfop technical (either 94% or 95% purity).
Solvents and Surfactants [0069] Table A identifies the solvents used in the trials and contains comments and identifying acronyms (where such were used).
TABLE A
Name Description Comments
Recosol 150 Petroleum-based aromatic hydrocarbon distillate fraction Equivalent to Solvesso 150, also designated R150, distillation range approx 180 - 210°C, flash point approx 66°C
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Recosol 100 Petroleum-based aromatic hydrocarbon distillate fraction Equivalent to Solvesso 100, also designated R100, distillation range approx 160 - 180 °C, flash point approx 50°C
Recosol 200 Petroleum-based aromatic hydrocarbon distillate fraction Equivalent to Solvesso 200, also designated R200, distillation range approx 220 plus°C, flash point approx 100°C
Butyl Glysolv Ethylene glycol monobutyl ether
Ethylene glycol monobutyl ether EGMBE, EGME
Diethylene glycol monoethyl ether DGME, DGMEE
Dimethyl Succinate
Dimethyl Adipate
N methyl pyrrolidone NMP
Exxate 700 C6-C8 acetate, acetic acid C6-C8 branched alkyl ester
toluene
xylene
acetone
Propylene glycol monomethyl ether PGME, PGMME
Propylene glycol
Diethylene glycol
Dipropylene glycol
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-20[0070] Table B identifies in general terms the surfactants used in the trials and Table C contains more details on the surfactants, including sources.
TABLE B
Name General Description Category (A,N,C) A=anionic N=non-ionic C=cationic
Termul 200 Nonylphenol alkoxylate N
Termul 203 Polypropyleneglycol alkoxylate N
Toximul 8320 Butanol alkoxylate N
Toximul TANS 5 Low-solvent alkylphenol ether sulphate/tallow amine ethoxylated salt A,N,C
Toximul TANS 6 Low-solvent alkylphenol ether sulphate/tallow amine ethoxylated salt A,N,C
Toximul TANS 8 Low-solvent alkylphenol ether sulphate/tallow amine ethoxylated salt A,N,C
Toximul TANS 15 Low-solvent alkylphenol ether sulphate/tallow amine ethoxylated salt A,N,C
Toximul TAABS 5 Low-solvent branched alcohol ether sulphate/tallow amine ethoxylated salt A,N,C
Toximul TAABS 8 Low-solvent branched alcohol ether sulphate/tallow amine ethoxylated salt A,N,C
NANSA EVM 70 Calcium alkylbenzenesulfonate in 2 ethylhexyl alcohol A
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Ninate 60E Calcium alkylbenzenesulfonate in 2 ethylhexyl alcohol A
Rhodacal 60/BE-C Calcium alkylbenzenesulfonate in 2 ethylhexyl alcohol A
Rhodacal 70 Calcium alkylbenzenesulfonate in 2 ethylhexyl alcohol A
Rhodacal 70B Calcium alkylbenzenesulfonate in 2 ethylhexyl alcohol A
Kemmat HF60 Calcium dodecyl lbenzenesulfonate A
Teric N2 Nonylphenol-2-EO N
Teric N8 N onylphenol- 8 -EO N
Teric N9 Nonylphenol-9-EO N
Teric N10 Nonylphenol-10-EO N
Teric N13 Nonylphenol-13 -EO N
Teric N15 Nonylphenol-15-EO N
Teric N20 Nonylphenol-20-EO N
Teric N30 Nonylphenol-30-EO N
Termul 1284 Castor oil-36-EO N
Termul 1285 Castor oil-54-EO N
Teric PE62 EO/PO block copolymer N
Teric PE64 EO/PO block copolymer N
Teric PE68 EO/PO block copolymer N
Makon TSP 16 Tristyryl-16-EO N
Pluronic PE 6400 PE/PO/PE block copol N
Pluronic PE 6800 PE/PO/PE block copol N
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TABLE C -22-
Name
Termul 200 Nonylphenol 9 EO/IOPO, HLB 16.1, solid
Orisurf 200 Equivalent to Termul 200
Termul 203 Alcohol alkoxylate, HLB 17.5 PO-EO-PO triblock, 35PO-25EO-30PO
Toximul 8320 Stepan, Butyl EO/PO block, HLB 12
Toximul TANS 5 Stepan, HLB 8. Ether sulphate component is anionic, tallow amine ethoxylate can be non-ionic or cationic depending on pH and chemical environment
Toximul TANS 6 Stepan, HLB. 10 Ether sulphate component is anionic, tallow amine ethoxylate can be non-ionic or cationic depending on pH and chemical environment
Toximul TANS 8 Stepan, HLB 12. Ether sulphate component is anionic, tallow amine ethoxylate can be non-ionic or cationic depending on pH and chemical environment
Toximul TANS 15 Stepan, HLB 14. Ether sulphate component is anionic, tallow amine ethoxylate can be non-ionic or cationic depending on pH and chemical environment
Toximul TAABS 5 Stepan, class of anionic detergent blend. Ether sulphate component is anionic, tallow amine ethoxylate can be non-ionic or cationic depending on pH and chemical environment
Toximul TAABS 8 Stepan, class of anionic detergent blend. Ether sulphate component is anionic, tallow amine ethoxylate can be non-ionic or cationic depending on pH and chemical environment.
NANSA EVM70 Linear alkylate 70% active may be in various solvents such as isobutanol or 2-ethyl hexanol
Ninate 60E Stepan, 60% active linear calcium alkylbenzenesulfonate in 2-ethylhexanol, 60% active
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Rhodacal 60/BE-C Rhodia, mixture of linear dodecylbenzene sulfonate calcium salt, 60% active
Rhodacal 70 Rhodia, branched dodecylbenzene sulfonate calcium salt, 70% active
Rhodacal 70B Rhodia, mixture of linear dodecylbenzene sulfonate calcium salt, 70% active
Kemmat HF60 Handan Xindiya, calcium dodecylbenzene sulfonate 60% active
Teric N2 Huntsman nonylphenolethoxlate
Teric N8 Huntsman nonylphenolethoxlate
Teric N9 Huntsman nonylphenolethoxlate
Teric N10 Huntsman nonylphenolethoxlate
Teric N13 Huntsman nonylphenolethoxlate
Teric N15 Huntsman nonylphenolethoxlate
Teric N20 Huntsman nonylphenolethoxlate
Teric N30 Huntsman nonylphenolethoxlate
Termul 1284 Huntsman, paste, HLB 12.6
Termul 1285 Huntsman, paste, HLB 14.4
Teric PE62 Huntsman PE/PO diblock copol 17 moles EO, HLB 7
Teric PE64 Huntsman PE/PO diblock copol, 25 moles EO, HLB 15
Teric PE68 Huntsman PE/PO diblock copol, 150 moles EO, HLB 29
Makon TSP 16 Stepan, HLB 13
Pluronic PE 6400 BASF, triblock copol PE/PO/PE, 1750 g/mol polypropylene glycol block, 40% polyethyleneglycol in molecule
Pluronic PE 6800 BASF, triblock copol PE/PO/PE, 1750 g/mol polypropylene glycol block, 80% polyethyleneglycol in molecule
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Varying Non-Ionic Surfactant at Constant Surfactant Ratio [0071] In this set of trials all haloxyfop formulations contained haloxyfop at a loading of 900 g/L. In each formulation trialled, a single anionic surfactant was used, namely that supplied under the trade name Ninate 60E (calcium C10-C16 alkylbenzenesulfonate, linear, CAS # 68584-23-6, as 60% in 2-ethylhexanol supplied by Stepan). In each formulation in these trials, a single solvent was used, namely, diethylene glycol monoethyl ether.
[0072] A range of non-ionic surfactants was used in this set of trials as follows, with the surfactant being identified initially by the trade name under which it was supplied:
Termul 200 (alkylphenol poly-ether EO/PO (ethyleneoxide/propylene oxide) block copolymer, 9 mol EO, 10 mol PO, CAS #37251-69-7, manufactured by Huntsman),
Teric N2 (nonylphenol 2-EO, manufactured by Huntsman),
Teric N8 (nonylphenol 8-EO, manufactured by Huntsman),
Teric N10 (nonylphenol 10-E, manufactured by Huntsman),
Teric N13 (nonylphenol 13-EO, manufactured by Huntsman),
Teric N20 (nonylphenol 20-EO, manufactured by Huntsman),
Termul 203 (alcohol alkoxylate, HLB 17.5, manufactured by
Huntsman),
Termul 1284 (castor oil PEG 36 CAS #61791-12-6, manufactured by Huntsman),
Termul 1285 (castor oil PEG 54 (polyethylene glycol) CAS #61791-12-6, manufactured by Huntsman),
Teric PE62 (EO/PO block copolymer, 17 moles EO, HLB = 7, CAS # 9003-11-6, manufactured by Huntsman),
Teric PE64 (EO/PO block copolymer, 25 Moles EO, HLB = 15, CAS # 9003-11-6, manufactured by Huntsman),
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-25 Teric PE 68 (EO/PO block copolymer, 150 Moles EO, HLB = 29, CAS # 9003-11-6, manufactured by Huntsman),
Toximul 8320 (polyoxyalkylene glycol ether, manufactured by
Stepan),
TSP 16 (tristyrylphenol ethoxylate, HLB = 13, CAS #99734-095, manufactured by Stepan company),
Pluronic PE 6400 (PE/PO/PE block copol, PO block mol wt 1750, 40% PE in molecule, contains CAS # 9003-11-6, manufactured by BASF), and
Pluronic PE 6800 (PE/PO/PE block copol, PO block mol wt 1750, 80% PE in molecule, contains CAS # 9003-11-6, manufactured by BASF).
[0073] The weight ratio of anionic to non-ionic surfactants was kept constant at 30:70. Termul 203 was selected as the control non-ionic surfactant. More details of the trials are set out in Appendix 1, which Appendix forms part of this Specification.
[0074] All formulations, apart from the control formulation, failed in terms of emulsion stability and/or cold temperature stability.
[0075] In Table 2 and subsequent Tables, which summarise the results of the trials, the following indicators apply:
E - Emulsion characteristics ascertained at 5% aq.
CTS - Cold temperature stability assessed at 2°C HLB - Hydrophilic Lipophilic Balance P - Pass
F - Fail
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TABLE 1
Trial using different non-ionic surfactants at constant surfactant ratio
(Control: Termul 203 as non-ionic surfactant Ionic Surfactant: Ninate 60E Solvent: Diethylene Glycol Monoethyl Ether)
Summary 30:70
of Results (a)
Code Name E CTS
A. Alkoxylate Alkyl Phenol
IA1 Termul 200 FAIL F P
B. Nonyl Phenol Ethoxylates
IA2 Teric N2 FAIL F P
IA3 Teric N8 FAIL F P
IA4 Teric N10 FAIL F P
IA5 Teric N13 FAIL F P
IA6 Teric N20 PASS P P
C. Castor Oil Ethoxylates
IA7 Termul 1284 FAIL F P
IA8 Termul 1285 FAIL F P
D. Block Co-polymer
IA9 Termul 203 PASS P P
IA10 TSP 16 FAIL F P
IA11 Teric PE62 FAIL F P
IA12 Teric PE64 FAIL F P
IA13 Teric PE68 FAIL F F
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IA14 Pluronic PE6400 FAIL F P
IA15 Pluronic PE6800 FAIL F F
Varying Non-Ionic Surfactants (Nonyl phenol ethoxylated combinations at
Varying Surfactant Ratios) [0076] Formulations containing haloxyfop at a loading of 900 g/L and using combinations of non-ionic surfactants, being nonyl phenol ethoxylates, and a single ionic surfactant, namely that supplied under the trade name Ninate 60E, with the ratios of the surfactants being varied were trialled. More details of these trials are set out in Appendix 2, which Appendix forms part of this specification. All formulations gave satisfactory results for cold temperature stability but unsatisfactory results for emulsion characteristics.
TABLE 2
Trial using different non-ionic surfactants (Nonyl phenol ethoxylated combination) at varying surfactant ratio
(Control: Termul 203 as non-ionic surfactant Ionic Surfactant: Ninate 60E Solvent: Diethylene Glycol Monoethyl Ether)
Summary of Results
Code Name E CTS
A. Nonyl Phenol Ethoxylates
DI Ninate: Teric N20 (10:90) FAIL F P
D2 Ninate: Teric N13: Teric N20 (10:10:80) FAIL F P
D3 Ninate:Teric N13:Teric N20 (5:10:85) FAIL F P
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D4 Ninate:Teric N10:Teric N20 (10:10:80) FAIL F P
D5 Ninate:Teric N10:Teric N20 (5:10:85) FAIL F P
D6 Ninate:Teric N8:Teric N20 (10:10:80) FAIL F P
D7 Ninate:Teric N8:Teric N20 (5:10:85) FAIL F P
D8 Ninate:Teric N2:Teric N20 (10:5:85) FAIL F P
D9 Ninate:Teric N2:Teric N20 (5:5:90) FAIL F P
Varying Non-Ionic Surfactants (Block Copolymer Combinations) at Varying
Surfactant Ratios [0077] Formulations containing haloxyfop at a loading of 900 g/L, and using combinations of non-ionic surfactants, being block copolymers, and a single ionic surfactant, being that supplied under the trade name Ninate 60E, with the ratios of the surfactants being varied were trialled. More details of these trials are set out in Appendix 3, which Appendix forms part of this specification. All formulations gave unsatisfactory results for both emulsion characteristics and cold temperature stability.
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TABLE 3
Trial using different non-ionic surfactants (co block polymer combination) at varying surfactant ratio
(Control: Termul 203 as non-ionic surfactant Ionic Surfactant: Ninate 60E Solvent: Diethylene Glycol Monoethyl Ether)
Summary of Results
Code Name E CTS
A. Nonyl Phenol Ethoxylates
El Ninate: Teric PE62: Teric PE68 (40:28:32) FAIL F F
E2 Ninate: Teric PE 62: Teric PE68 (30:36:34) FAIL F F
E3 Ninate: Teric PE 62: Teric PE68 (20:45:35) FAIL F F
E4 Ninate: Teric PE 62: Teric PE68 (10:53:37) FAIL F F
E5 Ninate: Teric PE 64: Teric PE68 (40:45:15) FAIL F F
E6 Ninate: Teric PE 64: Teric PE68 (30:57:13) FAIL F F
E7 Ninate: Teric PE 64: Teric PE68 (20:70:10) FAIL F F
E8 Ninate: Teric PE 64: Teric PE68 (10:83:7) FAIL F F
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Varying Non-Ionic Surfactant (Block Co-Polymer Combinations) at Varying
Surfactant Ratios in the Absence of Solvent [0078] Formulations containing haloxyfop at a loading of 900 g/L, and incorporating combinations of non-ionic surfactants, being block co-polymers, and a single ionic surfactant, being that supplied under the trade name Ninate 60E, with no solvent being present, and with the ratios of surfactants being varied, were trialled. More details of these trials are set out in Appendix 4, which Appendix forms part of this specification. All formulations gave unsatisfactory results for both emulsion characteristics and cold temperature stability.
TABLE 4
Trial using different non-ionic surfactants (co block polymer combination) at varying surfactant ratio without solvents
(Control: Termul 203 as non-ionic surfactant Ionic Surfactant: Ninate 60E Solvent: None)
Summary of Results
Code Name E CTS
A. Nonyl Phenol Ethoxylates
FI Ninate: Teric PE62: Teric PE68 (40:28:32) FAIL F F
F2 Ninate: Teric PE 62: Teric PE68 (30:36:34) FAIL F F
F3 Ninate: Teric PE 62: Teric PE68 (20:45:35) FAIL F F
F4 Ninate: Teric PE 62: Teric PE68 (10:53:37) FAIL F F
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L5 Ninate: Teric PE 64: Teric PE68 (40:45:15) FAIL F F
L6 Ninate: Teric PE 64: Teric PE68 (30:57:13) FAIL F F
L7 Ninate: Teric PE 64: Teric PE68 (20:70:10) FAIL F F
L8 Ninate: Teric PE 64: Teric PE68 (10:83:7) FAIL F F
Varying Loading Only [0079] In each formulation in this set of trials, the ionic surfactant was that supplied under the trade name Ninate 60E and the non-ionic surfactant was that supplied under the trade name Termul 203, with the solvent being diethylene glycol monoethyl ether. More details of these trials are set out in Appendix 5, which Appendix forms part of this specification.
[0080] The formulations contained loadings of 950 g/L, 1000 g/L and
1050 g/L of haloxyfop, respectively. All were found to be stable, although there was a marked increase in viscosity as the loading increased with all formulations exhibiting unsatisfactory viscosity at 5°C.
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TABLE 5
Trial using different non-ionic surfactants at constant surfactant ratio
(Control: Termul 203 as non-ionic surfactant Ionic Surfactant: Ninate 60E Solvent: Diethylene Glycol Monoethyl Ether)
Summary of Results 30:70 Viscosity, cPs
Code Name E CTS @ 20°C @ 5°C
A. Block Co-polymer
FI Termul 203 (Haloxyfop 950) FAIL P P 477 4,350
F2 Termul 203 (Haloxyfop 1000) FAIL P P 912 10,100
F3 Termul 203 (Haloxyfop 1050) PASS P P 1,840 25,000
Varying Solvent at Constant Surfactant Ratio [0081] In each formulation in this set of trials, the ionic surfactant was that supplied under the trade name Ninate 60E, the non-ionic surfactant was that supplied under the trade name Termul 203, and the solvent was propylene glycol mono methyl ether (PGME). More details of these trials are set out in Appendix 6, which Appendix forms part of this specification.
[0082] The formulations contained loadings of 950 g/L, 1000 g/L and
1050 g/L of haloxyfop, respectively. All formulations exhibited satisfactory emulsion characteristics and cold temperature stability, but only the formulation having a loading of 950 g/L haloxyfop met the viscosity criteria. This may indicate that 950 g/L may be an upper limit for haloxyfop loading according to the invention.
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TABLE 6
Trial using different non-ionic surfactants at constant surfactant ratio
(Control: Termul 203 as non-ionic surfactant Ninate 60E as Ionic Surfactant Solvent: Propylene Glycol Monoethyl Ether ((PGME))
Summary of Results 30:70 Viscosity, cPs
Code Name E CTS @ 5°C @ 20°C
A. Block Co-polymer
Hl Haloxyfop 950 PASS P P 1850 350
H2 Haloxyfop 1000 PASS P P 7100 635
H3 Haloxyfop 1050 PASS P P 57000 1660
Varying Ionic Surfactants at Constant Surfactant Ratio [0083] In these formulations the haloxyfop loading was maintained at substantially 900 g/L. The non-ionic surfactant was that as supplied under the trade mark Termul 203 and the solvent was diethylene glycol monoethyl ether. A single ionic surfactant chosen from a range of ionic surfactants was used in each instance, the range constituting members of the groups calcium dodecylebenzene sulphates, alkylphenol ether sulfate/tallow amine ethoxylated salts, and branched alcohol ether sulfate/tallow amine ethoxylated salts. The ratio of ionic to non-ionic surfactant was kept at 30:70. More details of these trials are set out in Appendix 7, which Appendix forms part of this specification.
[0084] All formulations, apart from that containing Toximul TAAPS 8, exhibited satisfactory emulsion characteristics and cold temperature stability.
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TABLE7
Trial using different ionic surfactants at constant surfactant ratio
(Control: Termul 203 as non-ionic surfactant Ionic Surfactant: Ninate 60E Solvent: Diethylene Glycol Monoethyl Ether)
Summary of Results 30:70
Code Name E CTS
A. Calcium Dodecylbenzene Sulphonate
IA9 Ninate 60E PASS P P
IB9 Rhodacal 60//BE-C PASS P P
IC9 Kemmat HF60 PASS P P
ID9 Nansa EVM 70/2E PASS P P
IE9 Rhodacal 70 PASS P P
IF9 Rhodacal 70B PASS P P
B. Alkylphenol ether sulfate/tallow amine ethoxylated salts
IG9 Toximul TANS 5 PASS P P
IH9 Toximul TANS 6 PASS P P
119 Toximul TANS 8 PASS P P
C. Branched alcohol ether sulfate/tallow amine ethoxylated salts
IJ9 Toximul TAABS 5 PASS P P
IK9 Toximul TAABS 8 PASS P P
Varying Solvents at Constant Surfactant Ratio [0085] In these trials the haloxyfop loading was maintained at substantially 900 g/L, the ionic surfactant was that as supplied under the trade
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-35 name Ninate 60E, the non-ionic surfactant was that as supplied under the trade name Termul 203, and the ionic surfactant:non-ionic surfactant ratio was maintained at 30:70. More details of the trials are set out in Appendix 8, which Appendix forms part of this specification.
[0086] Only these formulations in which the solvent was diethylene glycol monoethyl ether or propylene glycol monomethyl ether exhibited satisfactory emulsion characteristics and cold temperature stability.
TABLE 8
Trial using different solvent surfactants at constant surfactant ratio (Control: Termul 203 as non-ionic surfactant Ionic Surfactant: Ninate 60E)
Summary of Results 30:70
Code Name E CTS
Solvents
IA9 Diethylene glycol monoethyl ether (DGME) Pass P P
IIA9 Recosol 150 Pail F P
IIIA9 Recosol 200 Pail F P
IVA9 Xylene Pail F P
VA9 Toluene Pail F P
VIA9 Acetone Pail F P
VIIA9 Dimethyl adipate Pail F F
VIIIA9 Dimethyl succinate Pail F F
IXA9 NMP Fail F P
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XA9 Ethylene glycol mo no butyl ether Pass P P
XIA9 Propylene glycol monomethyl ether (PGME) Pass P P
XIIA9 Propylene glycol Fail N/A F
XIIIA9 Diethylene glycol Fail N/A F
XIVA9 Dipropylene glycol Fail F F
Varying Surfactant Loading at Constant Surfactant Ratio [0087] In these formulations the haloxyfop loading was maintained at substantially 900 g/L, the ionic surfactant used was that as supplied under the trade name Ninate 60E, the non-ionic surfactant was that as supplied under the trade name Termul 203, the ratio of ionic to non-ionic surfactant was maintained at 30:70, and the solvent was diethylene glycol monoethyl ether. The total surfactant loading was varied. More details of the trials are set out in Appendix 9, which Appendix forms part of this specification.
[0088] Decreasing the total surfactant loading below 80% of the control loading resulted in unsatisfactory emulsion characteristics.
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TABLE9
Trial using different surfactant loadings at constant surfactant ratio (Control: Termul 203 as non-ionic surfactant
Ionic Surfactant: Ninate 60E Solvent: Diethylene Glycol Monoethyl Ether)
Code Name Summary of Results E CTS HLB
A. Haloxyfop 900 (Control Formulation)
J1 Original ratio 60:40 of surfactant At 80% surfactant loading Pass P P 15.55
J2 Original ratio 60:40 of surfactant At 60% surfactant loading Pass P P 15.55
J3 Original ratio 60:40 of surfactant At 40% surfactant loading Fail F P 15.56
J4 Original ratio 60:40 of surfactant At 20% surfactant loading Fail F P 15.58
Varying Haloxyfop Loading and Varying Non-Ionic Surfactant [0089] In these trials the haloxyfop was set at one of 900 g/L, 800 g/L and 700 g/L and a number of formulations at those loadings using one of a range of non-ionic surfactants, being nonyl phenol ethoxylates, and a block copolymer, were prepared. The ionic surfactant used was that as supplied under the trade name Ninate 60E, and the solvent was diethylene glycol monoethyl ether. The ionic surfactantmon-ionic surfactant ratio was maintained at 30:70. More details of those trials are set out in Appendix 10, which Appendix forms part of this specification.
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TABLE 10
Trials by varying non-ionic surfactant at different Haloxyfop loading (900 g/L, 800 g/L and 700 g/L) (Control: Termul 203 as non-ionic surfactant Ninate 60E as ionic surfactant DGME as Solvent) Trials were done using the following loading: Haloxyfop tech: varies (900 g/L, 800 g/L, 700 g/L) Solvent (DGME): ~ 185 g/L Anionic Surfactant (Ninate 60E): ~ 30 g/L Non-ionic Surfactant - Nonyl phenol ethoxylates (e.g., Teric N20, N30, N13, N15, N9) and block co-polymer (Toximul 8320): ~ 62-66 g/L
Code Name Summary of Results E CTS HLB
Haloxyfop loading @ 900 g/L
4a Toximul 8320 Pass P P 11.53
4b Teric N20 Pass P P 14.20
4c Teric N30 Fail F P 15.07
4d Teric N13 Pass P P 13.14
4e Teric N15 Fail F P 13.57
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4f Teric N9 Pass P P 12.08
Haloxyfop loading @ 800 g/L
4g Toximul 8320 Pass P P 11.57
4h Teric N20 Pail F P 15.22
4i Teric N30 Pail F P 14.39
4j Teric N13 Pail F P 13.65
4k Teric N15 Fail F P 12.95
41 Teric N9 Pass P P 12.08
Haloxyfop loading @ 700 g/L
4m Toximul 8320 Pass P P 11.55
4n Teric N20 Fail F P 15.13
4o Teric N30 Fail F P 14.32
4p Teric N13 Fail F P 13.63
4q Teric N15 Fail F P 13.00
4r Teric N9 Fail F P 12.12
Varying ionic Surfactant and Non-Ionic Surfactant at Constant Surfactant Ratio [0091] The haloxyfop loading in the formulations used in these trials was maintained at substantially 900 g/L, the solvent used was diethylene glycol monoethyl ether, the non-ionic surfactant used was either a nonyl phenol ethoxylate as supplied under the trade name Teric N9 or a block co-polymer as supplied under the trade name Termul 8320. The ionic surfactant used was one selected from a range and the ionic surfactant:non-ionic surfactant ratio was maintained at 30:70. More details of the trials are set out in Appendix 11, which Appendix forms part of this specification.
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TABLE 11
Trials using different anionic surfactants and non-ionic surfactants at constant surfactant ratio
(Control: Termul 203 as non-ionic surfactant Ninate 60E as ionic surfactant DGME as Solvent) Trials were done using the following loading:
Haloxyfop tech: 900 g/L
Solvent (DGME): ~ 175 g/L Anionic Surfactant: varies (Kemmat HF60, Nansa 70EVM, Rhodacal 70, Rhodacal 70B: ~ 26-33 g/L Non-ionic Surfactant (Nonyl phenol ethoxylate - Teric N9) or (Block copolymer - Toximul 8320: ~ 61-67 g/L
Code Name Summary of Results E CTS HLB
Solvents
4s T8320 / Kemmat HF60 Pass P P 11.72
4t T8320 / Nansa 70 EVM Pass P P 11.72
4u T8320 / Rhodacal 70 Fail F P 11.70
4v T8320 / Rhodacal 70B Fail F P 10.85
4w TN9 / Kemmat HF60 Fail F P 12.27
4x TN9/Nansa 70 EVM Pass P P 12.23
4y TN9 / Rhodacal 70 Pass P P 12.25
4z TN9 / Rhodacal 70B Pass P P 11.49
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-41 Varying Solvents at Constant Surfactant Ratio [0093] Further trials were carried out on formulations having a haloxyfop loading of 900 g/L. The ionic surfactant used was that as supplied under the trade name Ninate 60E and the non-ionic surfactant used was that as supplied under the trade name Termul 203, with the anionic surfactantmonionic surfactant ratio being set at 30:70. More details of these trials are set out in Appendix 12, which Appendix forms part of this specification.
[0094] Solvents giving rise to satisfactory formulations were ethylene glycol monobutyl ether (EGME), (e.g., butyl glysolv), toluene, and acetone. Dimethyl succinate and dimethyl adipate were not effective solvents and no homogenous solutions were obtained with these solvents. The unsatisfactory formulations did not exhibit desired emulsion characteristics.
TABLE 12
Trials using different solvents (Control: Termul 203 as non-ionic surfactant Ninate 60E as ionic surfactant DGME as Solvent) Trials were done using the following loading: Haloxyfop tech: 900 g/L Solvent varies (e.g., R150, R200, EGME, Dimethyl succinate, Toluene, Acetone, Dimethyl adipate, xylene, NMP and Exxate 700): ~ 160-190 g/L Anionic Surfactant (Ninate 60E): ~ 25-29 g/L Non-ionic Surfactant (Block co-polymer - Toximul 8320: ~ 60-64 g/L
Code Name Summary of Results E CTS HLB
Solvents
4ae R200 Fail F P 11.54
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4af EGME Pass P P 11.56
4ag R150 Fail F P 11.53
4ah EGME Pass P P 11.55
4ai Dimethyl Succinate Fail * * * 11.55
4aj Toluene Pass P P 11.55
4ak Acetone Pass P P 11.54
4al Dimethyl Adipate Fail * * * 11.52
4am Xylene Fail F P 11.56
4an NMP Fail F P 11.53
4ao Exxate 700 Fail F P 11.56
Examples of Formulations Exhibiting Satisfactory Characteristics [0095] Examples of haloxyfop formulations prepared according to the present invention which exhibit satisfactory characteristics (as demonstrated by the trials discussed above) are set out in Table 13 for ease of reference.
TABLE 13
Trial Code Appendix Haloxyfop Loading g/L Solvent & Loading g/L Ionic Surfactant & Loading g/L Non-Ionic Surfactant & Loading g/L
IA9 1 899 (+95) DGME 183.5 Ninate 60E 27 Termul 203 63
Hl 6 950 (+100) PGME 126 Ninate 60E 26 Termul 203 61
IB9 7 898 (+94) DGME 187 Rhodacal 60/BE-C 27 Termul 203 60
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IC9 7 896 (+94) DGME 187 Kemmat HF60 28 Termul 203 61
ID9 7 899 (+95) DGME 184 Nansa EVM 70/2E 27 Termul 203 62
IE9 7 896 (+94) DGME 187 Rhodacal 70 28 Termul 203 62
IF9 7 897 (+94) DGME 186 Rhodacal 70B 26 Termul 203 62
IG9 7 897 (+94) DGME 186 Toximul TANS 5 27 Termul 203 61
IH9 7 896 (+94) DGME 185 Toximul TANS 6 29 Termul 203 62
119 7 901 (+95) DGME 183 Toximul TANS 8 26 Termul 203 61
U9 7 897 (+94) DGME 187 Toximul TAABS 5 26 Termul 203 62
XIA9 8 900 (+95) PGME 184 Ninate 60E 26 Termul 203 61
J1 9 900 (+95) DGME 196 Ninate 60E 21 Termul 203 49
4a 10 900 (+95) DGME 184 Ninate 60E 29 Toximul 8320 62
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4f 10 901 (+95) DGME 188 Ninate 60E 30 Teric N9 66
4g 10 802 (+84) DGME 274 Ninate 60E 25 Toximul 8320 64
41 10 802 (+84) DGME 266 Ninate 60E 28 Teric N9 61
4m 10 703 (+95) DGME 338 Ninate 60E 28 Toximul 8320 65
4s 11 900 (+95) DGME 175 Kemmat HF60 26 Toximul 8320 67
4t 11 900 (+95) DGME 176 Nansa EVM 70/2E 26 Toximul 8320 68
4af 12 900 (+95) EGME 166 Ninate 60E 27 Toximul 8320 64
Note 1: Ninate 60E given weight includes carrier solvent
Note 2: Rhodacal 60/BE-C given weight includes carrier solvent Note 3: Kemmat HF60 given weight includes carrier solvent Note 4: Nansa EVM 70/2E given weight includes carrier solvent Note 5: Rhodacal 70 given weight includes carrier solvent Note 6: Other anionic surfactants, weight includes carrier solvent Note 7: EGME = ethyleneglycolmonobutyl ether = butyl glysolv Note 8: PGME = propyleneglycolmonoethyl ether
Source of Technical Grade Active (Haloxyfop-P-methyl (CAS# 72619-32-0)):
Manufactured by Jinan Luba Chemicals Co Ltd, 26 South Xizhou Road, Lichen, Jinan, P.R. CHINA;
Purchased from Zhejiang Chemical Industrial Co Ltd, P.R. CHINA
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-45 Agronomic Trial [0096] Haloxyfop 900 and Haloxyfop 520 were compared in the field for brome and wild oat control, and for crop phyto toxicity. Plot size was 2.5m x 10m, 3 replicates. Treatments were applied with a hand boom. % wild oat and brome grass were assessed visually. The results were:
• At all rates (50 ml/ha, 100 ml/ha and 200 ml/ha for Haloxyfop 520 and 29 ml/ha, 58 ml/ha and 116 ml/ha for Haloxyfop 900) there was found to be 100% control of wild oats and brome grass.
• Speed of kill was observed to be slightly faster at higher rates used with both formulations.
• No phytotoxicity was observed from either Haloxyfop 520 or Haloxyfop 900, even in the double rate treatments.
• Both Haloxyfop 520 and Haloxyfop 900 mixed well in the field.
• None of the ryegrass present in the trial was controlled by the haloxyfop formulations because the ryegrass was resistant to Fops (common in the trial area of Wycheproof, Victoria, Australia).
[0097] The complete disclosures of any patents, patent documents, and publications cited herein are incorporated by reference in their entirety as if each were individually incorporated. Various modifications and alterations to this invention will become apparent to those skilled in the art without departing from the scope and spirit of this invention. It should be understood that this
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-462014203147 11 Jun2014 invention is not intended to be unduly limited by the illustrative embodiments and examples set forth herein and that such examples and embodiments are presented by way of example only with the scope of the invention intended to be limited only by the claims set forth herein as follows.
[0098] Throughout this specification and the claims which follow, unless the context requires otherwise, the word “comprise”, and variations such as “comprises” or “comprising”, will be understood to imply the inclusion of a stated integer or step or group of integers or steps but not the exclusion of any other integer or step or group of integers or steps.
[0099] The reference in this specification to any prior publication (or information derived from it), or to any matter which is known, is not, and should not be taken as an acknowledgment or admission or any form of suggestion that that prior publication (or information derived from it) or known matter forms part of the common general knowledge in the field of endeavour to which this specification relates.
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APPENDIX 1
Trial # IA1
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 200 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 200 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 200: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) CAS# Function Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 72619-32-0 Active ingredient 4978.3 899
Solvent used: Diethylene Glycol Monoethyl Ether 111-90-0 Solvent 917.5 183
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) CABS ( 68584-23-6) & 2-ethyl hexanol (104-76-7) Surfactant 136.7 27
Alkoxylated alkyl phenol used: Termul 200 (non-ionic surfactant) 37251-69-7 Surfactant 313.3 63
Total 6345.8
RESULTS OF FORMULATION
Parameter Method Required Results Remarks
Appearance Visual Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay Validated chromatographic method (Accuracy: 98-102%) (Linearity: R > 0.99) (Precision: s/average < 2%) 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution MT 75.3 6 to 8 n/a
Specific gravity (temperature at 20C) CIPAC MT 3.1 1.25 to 1.27 n/a
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Emulsion characteristics CIPAC MT 36.1 <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming CIPAC MT 47.2 <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) MT75.3 Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) MT 192 0 to 2000cPs n/a
Viscosity (temperature at 20C) MT 192 0 to 2000cPs n/a
Long Term Performance Various as per above Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IA2
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N2 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N2 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N2: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4979.2 899
eg. Haloxyfop Tech (94% purity)
Solvent 925.8 185
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used: Diethylene Glycol Monoethyl Ether
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 135.0 27
Nonyl Phenol ethoxylates used: Teric N2 (non-ionic surfactant) 305.0 61
Total 6345.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # IA3
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N8 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N8 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N8: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 897
Solvent used: Diethylene Glycol Monoethyl Ether 934.2 186
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 132.5 26
Nonyl Phenol ethoxylates used: Teric N8 (non-ionic surfactant) 313.3 62
Total 6350.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IA4
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N10 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N10 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N10: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4971.7 899
Solvent used: Diethylene Glycol Monoethyl Ether 925.0 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 132.5 26
Nonyl Phenol ethoxylates 304.2 61
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used: Teric N10 (non-ionic surfactant)
Total 6333.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IA5
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N13 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N13 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N13: Diethylene Glycol monoethyl ether
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-53 FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4967.5 899
Solvent used: Diethylene Glycol Monoethyl Ether 932.5 187
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 127.5 26
Nonyl Phenol ethoxylates used: Teric N13 (non-ionic surfactant) 302.5 61
Total 6330.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IA6
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N20 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4980.8 899
Solvent used: Diethylene Glycol Monoethyl Ether 917.5 183
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 133.3 27
Nonyl Phenol ethoxylates used: Teric N20 (non-ionic surfactant) 313.3 63
Total 6345.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
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Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2ml cream ©bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # IA7
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 1284 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 1284 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 1284: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4974.2 899
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 922.5 184
Calcium C10-16 alkyl benzenesulfonic acid 135.0 27
3472646v 1
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Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant)
Castor Oil Ethoxylates used: Termul 1284 (non-ionic surfactant) 305.8 61
Total 6337.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # IA8
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 1285 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 1285 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 1285: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4968.3 899
Solvent used: Diethylene Glycol Monoethyl Ether 921.7 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 136.7 27
Castor Oil Ethoxylates used: Termul 1285 (non-ionic surfactant) 304.2 61
Total 6330.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2- pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4978.3 899
Solvent used: Diethylene Glycol Monoethyl Ether 917.5 183
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 136.7 27
Block Co-polymer used: Termul 203 (non-ionic surfactant) 313.3 63
Total 6345.8
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 899g/L Passed
pH at 1 % aq. Solution 6 to 8 7.35 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.266 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.3ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 25ml Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1212cps Passed
Viscosity (temperature at 20C) 0 to 2000cPs 315cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # IA10
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using TSP 16 as non-ionic surfactants against Ninate 60E
Ratio of N60E: TSP 16 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: TSP 16: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4979.2 895
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eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 946.7 188
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 133.3 26
Block Co-polymer used: TSP 16 (non-ionic surfactant) 311.7 62
Total 6370.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # IA11
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE 62 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE 62 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE 62: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.3 899
Solvent used: Diethylene Glycol Monoethyl Ether 926.7 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 132.5 26
Block Co-polymer used: Teric PE 62 (non-ionic surfactant) 307.5 61
Total 6340.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IA12
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE 64 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE 64 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE 64: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4982.5 899
Solvent used: Diethylene Glycol Monoethyl Ether 924.2 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 138.3 28
Block Co-polymer 303.3 60
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used: Teric PE 64 (non-ionic surfactant)
Total 6348.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IA13
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE 68 as non-ionic surfactants against Ninate 60E Ratio of N60E: Teric PE 68 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE 68: Diethylene Glycol monoethyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4977.5 900
Solvent used: Diethylene Glycol Monoethyl Ether 917.5 183
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 136.7 27
Block Co-polymer used: Teric PE 68 (non-ionic surfactant) 306.7 61
Total 6338.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, formed lumps Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # IA14
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Pluronic 6400 as non-ionic surfactants against Ninate 60E Ratio of N60E: Pluronic 6400 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Pluronic 6400: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 899
Solvent used: Diethylene Glycol Monoethyl Ether 926.7 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 130.0 26
Block Co-polymer used: Pluronic 6400 (non-ionic surfactant) 310.0 62
Total 6336.7
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # IA15
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Pluronic 6800 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Pluronic 6800 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Pluronic 6800: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.5 900
Solvent used: Diethylene Glycol Monoethyl Ether 925.8 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 128.3 26
Block Co-polymer used: Teric PE 68 (non-ionic surfactant) 304.2 61
Total 6330.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, formed lumps Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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APPENDIX 2
Trial # D1
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N20 (10:90)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.1 900
Solvent used: Diethylene Glycol Monoethyl Ether 890.7 178
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 47.1 9
Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 418.6 84
Total 6328.6
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml oil&cream @bottom Failed
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Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # D2
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N13 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N13: Teric N20 (10:10:80)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N13: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4975.0 901
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 892.9 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 46.4 9
used: Ninate 60E (anionic surfactant)
Nonyl phenol ethoxylated 46.4 9
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used: Teric N13 (non-ionic surfactant)
Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 367.9 74
Total 6328.6
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # D3
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N13 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N13: Teric N20 (5:10:85)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N13: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4975.0 899
Solvent used: Diethylene Glycol Monoethyl Ether 895.7 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 22.1 4
Nonyl phenol ethoxylated used: Teric N13 (non-ionic surfactant) 50.0 10
Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 395.0 79
Total 6337.9
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # D4
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N10 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N10: Teric N20 (10:10:80)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N10: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4975.7 900
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 894.3 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 45.7 9
used: Ninate 60E (anionic surfactant)
Nonyl phenol ethoxylated 46.4 9
used: Teric N10 (non-ionic surfactant)
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Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 370.0 74
Total 6332.1
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # D5
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N10 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N10: Teric N20 (5:10:85)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N10: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.7 900
Solvent used: Diethylene Glycol Monoethyl Ether 892.1 178
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 22.9 5
Nonyl phenol ethoxylated used: Teric N10 (non-ionic surfactant) 46.4 9
Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 395.7 79
Total 6327.9
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # D6
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N8 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N8: Teric N20 (10:10:80)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N8: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4972.9 901
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 890.7 178
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 44.3 9
used: Ninate 60E (anionic surfactant)
Nonyl phenol ethoxylated 44.3 9
used: Teric N8 (non-ionic surfactant)
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Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 370.7 74
Total 6322.9
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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-78 Trial # D7
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N8 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N8: Teric N20 (5:10:85)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N8: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 901
Solvent used: Diethylene Glycol Monoethyl Ether 891.4 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 21.4 4
Nonyl phenol ethoxylated used: Teric N8 (non-ionic surfactant) 45.0 9
Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 394.3 79
Total 6322.1
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # D8
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N2 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N2: Teric N20 (10:5:85)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N2: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4976.4 899
Solvent used: Diethylene Glycol Monoethyl Ether 895.0 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 47.9 10
Nonyl phenol ethoxylated used: Teric N2 (non-ionic surfactant) 22.9 5
397.9 79
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Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant)
Total 6340.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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-81 Trial # D9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N2 and Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N2: Teric N20 (5:5:90)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N2: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.7 900
Solvent used: Diethylene Glycol Monoethyl Ether 893.6 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 24.3 5
Nonyl phenol ethoxylated used: Teric N2 (non-ionic surfactant) 22.9 5
Nonyl phenol ethoxylated used: Teric N20 (non-ionic surfactant) 417.1 83
Total 6328.6
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # E1
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE62: Teric PE68 (40:28:32)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.9 902
Solvent used: Diethylene Glycol Monoethyl Ether 892.9 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 178.6 36
Block co-polymer used: Teric PE 62 (non-ionic surfactant) 125.0 25
Co block polymer used: Teric PE 68 (non-ionic surfactant) 145.0 29
Total 6314.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
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Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # E2
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E Ratio of N60E: Teric PE62: Teric PE68 (30:36:34)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4972.1 903
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 890.7 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 133.6 27
used: Ninate 60E (anionic surfactant)
161.4 32
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Block co-polymer used: Teric PE 62 (non-ionic surfactant
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 153.6 31
Total 6311.4
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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Trial # E3
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE62: Teric PE68 (20:45:35)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4971.4 902
Solvent used: Diethylene Glycol Monoethyl Ether 892.9 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 88.6 18
Block co-polymer used: Teric PE 62 (non-ionic surfactant 202.1 41
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 157.1 32
Total 6312.1
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # E4
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE62: Teric PE68 (10:53:37)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4971.4 903
Solvent used: Diethylene Glycol Monoethyl Ether 889.3 178
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 45.0 9
Block co-polymer used: Teric PE 62 (non-ionic surfactant 238.6 48
165.7 33
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Block co-polymer used: Teric PE 68 (non-ionic surfactant)
Total 6310.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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Trial # E5
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE64: Teric PE68 (40:45:15)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.9 902
Solvent used: Diethylene Glycol Monoethyl Ether 897.9 180
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 178.6 36
Block co-polymer used: Teric PE 64 (non-ionic surfactant 199.3 40
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 66.4 13
Total 6315.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2ml solid crystals & 2.5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # E6
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E Ratio of N60E: Teric PE64: Teric PE68 (30:57:13)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.1 903
Solvent used: Diethylene Glycol Monoethyl Ether 893.6 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 131.4 26
Block co-polymer used: Teric PE 64 (non-ionic surfactant 252.1 51
Block co-polymer 57.9 12
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used: Teric PE 68 (non-ionic surfactant)
Total 6307.1
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.5ml solid crystals & 2.5ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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Trial # E7
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE64: Teric PE68 (20:70:10)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.1 902
Solvent used: Diethylene Glycol Monoethyl Ether 899.3 180
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 88.6 18
Block co-polymer used: Teric PE 64 (non-ionic surfactant 309.3 62
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 45.0 9
Total 6314.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4.5ml solid crystals&oil & 0.5ml cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # E8
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE64: Teric PE68 (10:83:7)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4976.4 904
Solvent used: Diethylene Glycol Monoethyl Ether 895.0 180
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 42.9 9
Block co-polymer used: Teric PE 64 (non-ionic surfactant 362.9 73
30.0 6
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Block co-polymer used: Teric PE 68 (non-ionic surfactant)
Total 6307.1
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4.5ml oil &solid crystals & 0.5ml cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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Trial # F1
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE62: Teric PE68 (40:28:32)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: no solvents
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.9 900
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 544.3 109
Block co-polymer used: Teric PE 62 (non-ionic surfactant) 379.3 76
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 435.0 87
Total 6331.4
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
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Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # F2
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE62: Teric PE68 (30:36:34)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: no solvents
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4974.3 899
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 410.7 82
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used: Ninate 60E (anionic surfactant)
Block co-polymer used: Teric PE 62 (non-ionic surfactant 491.4 98
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 462.9 92
Total 6339.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 6ml cream&oil @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE62: Teric PE68 (20:45:35)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: no solvents
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.9 899
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 273.6 55
Block co-polymer used: Teric PE 62 (non-ionic surfactant 615.0 123
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 477.9 95
Total 6339.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml cream&oil @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # F4
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE62 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE62: Teric PE68 (10:53:37)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE62: Teric PE68: no solvents FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.9 898
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 136.4 27
Block co-polymer used: Teric PE 62 (non-ionic surfactant 727.1 145
Block co-polymer 507.1 101
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used: Teric PE 68 (non-ionic surfactant)
Total 6343.6
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 6ml oil&cream @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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Trial # F5
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE64: Teric PE68 (40:45:15)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: no solvents
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.1 897
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 551.4 110
Block co-polymer used: Teric PE 64 (non-ionic surfactant 618.6 123
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 205.7 41
Total 6347.9
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml cream&oil @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # F6
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E Ratio of N60E: Teric PE64: Teric PE68 (30:57:13)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: no solvents
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.6 898
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 410.7 82
Block co-polymer used: Teric PE 64 (non-ionic surfactant 781.4 156
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 177.9 35
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6343.6
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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Trial # F7
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE64: Teric PE68 (20:70:10)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: no solvent
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4975.0 900
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 271.4 54
Block co-polymer used: Teric PE 64 (non-ionic surfactant 953.6 191
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 135.0 27
Total 6335.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 3.5ml cream&oil @bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # F8
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Teric PE64 and Teric PE68 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric PE64: Teric PE68 (10:83:7)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric PE64: Teric PE68: no solvents
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.6 898
Solvent used: Diethylene Glycol Monoethyl Ether 0.0 0
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 139.3 28
Block co-polymer used: Teric PE 64 (non-ionic surfactant 1135.7 227
Block co-polymer used: Teric PE 68 (non-ionic surfactant) 94.3 19
Total 6342.9
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil @bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, solidify Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING, BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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APPENDIX 5
Trial # F1
HALOXYFOP 900 TRIALS
Haloxyfop active present at 950g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 5249.4 950
Solvent used: Diethylene Glycol Monoethyl Ether 701.9 140
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 132.5 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 307.1 61
Total 6390.9
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 950g/L Passed
pH at 1%aq. Solution 6 to 8 7.42 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.278 Above the required result
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Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, no cream@bottom Passed
Persistent Foaming <60mL after 1 min 12ml in 1min Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 4350cps Failed
Viscosity (temperature at 20C) 0 to 2000cPs 477cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: FAILED THE VISCOSITY TEST @ 5°C
Trial # F2
HALOXYFOP 900 TRIALS
Haloxyfop active present at 10OOg/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 5525.2 1000
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 508.2 102
Calcium C10-16 alkyl benzenesulfonic acid 131.1 26
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in 2-ethyl hexanol used: Ninate 60E (anionic surfactant)
Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.5 61
Total 6470.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 1000g/L Passed
pH at 1 % aq. Solution 6 to 8 7.43 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.294 Above the required result
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.1ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 12ml in 1min Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 10100cps Failed
Viscosity (temperature at 20C) 0 to 2000cPs 912cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: FAILED THE VISCOSITY TEST @ 5°C
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Trial # F3
HALOXYFOP 900 TRIALS
Haloxyfop active present at 1050g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 5801.5 1050
Solvent used: Diethylene Glycol Monoethyl Ether 295.8 59
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 131.1 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 306.7 61
Total 6535.1
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 1050g/L Passed
pH at 1 % aq. Solution 6 to 8 7.66 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.307 Above the required result
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.1ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 4ml in 1min Passed
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 25000cps Failed
Viscosity (temperature at 20C) 0 to 2000cPs 1840cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: FAILED THE VISCOSITY TEST @ 5°C
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APPENDIX 6
Trial # H1
HALOXYFOP 900 TRIALS
Haloxyfop active present at 950g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: PGME
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 5249.9 950
Solvent used: Propylene Glycol Monomethyl Ether 631.5 126
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 131.3 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 306.2 61
Total 6318.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Red to brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 950g/L Passed
pH at 1 % aq. Solution 6 to 8 7.24 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.264 Passed
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Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h Milky emulsion, no separation, 0.2ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 2ml in 1min Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1850cps Passed
Viscosity (temperature at 20C) 0 to 2000cPs 350cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years.
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # H2
HALOXYFOP 900 TRIALS
Haloxyfop active present at 10OOg/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: PGME
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 5526.7 1000
eg. Haloxyfop Tech (94% purity)
Solvent used: Propylene Glycol Monomethyl Ether 439.1 88
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 131.9 26
used: Ninate 60E (anionic surfactant)
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Block Co-polymer used: Termul 203 (non-ionic surfactant) 306.8 61
Total 6404.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Red to brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 1000g/L Passed
pH at 1 % aq. Solution 6 to 8 7.56 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.281 Above Specs
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h Milky emulsion, no separation, 0.5ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 2ml in 1min Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 7100cps Failed
Viscosity (temperature at 20C) 0 to 2000cPs 635cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years.
General Remarks PASS or FAIL? PASS
Description: VISCOSITY AT 5°C FAILED THE TRIAL
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Trial # H3
HALOXYFOP 900 TRIALS
Haloxyfop active present at 1050g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: PGME
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 5806.6 1051
Solvent used: Propylene Glycol Monomethyl Ether 252.8 51
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 131.4 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 307.5 62
Total 6498.2
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Red to brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 1051 g/L Passed
pH at 1 % aq. Solution 6 to 8 7.63 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.300 Above Specs
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h Milky emulsion, no separation, 1.0ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 2ml in 1min Passed
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 57000cps Failed
Viscosity (temperature at 20C) 0 to 2000cPs 1660cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years.
General Remarks PASS or FAIL? PASS
Description: VISCOSITY AT 5OC FAILED THE TRIAL
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APPENDIX 7
Trial # IA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4978.3 899
Solvent used: Diethylene Glycol Monoethyl Ether 917.5 183
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 136.7 27
Block Co-polymer used: Termul 203 (non-ionic surfactant) 313.3 63
Total 6345.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 899g/L Passed
pH at 1 % aq. Solution 6 to 8 7.35 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.266 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.3ml cream@bottom Passed
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Persistent Foaming <60mL after 1 min 25ml Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1212cps Passed
Viscosity (temperature at 20C) 0 to 2000cPs 315cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # IB9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Rhodacal 60/BE-C as anionic surfactants against Termul 203 Ratio of Rhodacal 60/BE-C : Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Rhodacal 60/BE-C: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.5 898
Solvent used: Diethylene Glycol Monoethyl Ether 938.3 187
Calcium Dodecylbenzene Sulphonate in 2ethylhexanol used: Rhodacal 60/BE-C (anionic surfactant) 133.3 27
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Block Co-polymer used: Termul 203 (non-ionic surfactant) 302.5 60
Total 6346.7
RESULTS OF FORMULATION
Parameter Method Required Results Remarks
Appearance Visual Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay Validated chromatographic method (Accuracy: 98-102%) (Linearity: R > 0.99) (Precision: s/average < 2%) 875 to 925g/L Haloxyfop 898g/L Passed
pH at 1 % aq. Solution MT 75.3 6 to 8 n/a
Specific gravity (temperature at 20C) CIPAC MT 3.1 1.25 to 1.27 n/a
Emulsion characteristics CIPAC MT 36.1 <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, traces of cream@bottom Passed
Persistent Foaming CIPAC MT 47.2 <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) MT75.3 Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) MT 192 0 to 2000cPs n/a
Viscosity (temperature at 20C) MT 192 0 to 2000cPs n/a
Long Term Performance Various as per above Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
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Trial # IC9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Kemmat HF60 as anionic surfactants against Termul 203
Ratio of Kemmat HF60 : Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Kemmat HF60: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4976.7 896
Solvent used: Diethylene Glycol Monoethyl Ether 938.3 187
Calcium Dodecylbenzene Sulphonate in 2ethylhexanol used: Kemmat HF60 (anionic surfactant) 138.3 28
Block Co-polymer used: Termul 203 (non-ionic surfactant) 306.7 61
Total 6360.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 896g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, traces of cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
Trial # ID9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Nansa EVM 70/2E as anionic surfactants against Termul 203
Ratio of Nansa EVM 70/2E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Nansa EVM 70/2E: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4971.7 899
Solvent used: Diethylene Glycol Monoethyl Ether 920.0 184
Calcium Dodecylbenzene Sulphonate in butanol used: Nansa EVM 70/2E (anionic surfactant) 135.0 27
Block Co-polymer 309.2 62
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used: Termul 203 (non-ionic surfactant)
Total 6335.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 899g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, traces of cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
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HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Rhodacal 70 as anionic surfactants against Termul 203
Ratio of Rhodacal 70: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Rhodacal 70: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4980.8 896
Solvent used: Diethylene Glycol Monoethyl Ether 939.2 187
Calcium Dodecylbenzene Sulphonate in butanol used: Rhodacal 70 (anionic surfactant) 139.2 28
Block Co-polymer used: Termul 203 (non-ionic surfactant) 310.0 62
Total 6369.2
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 896g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, traces of cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
Trial # IF9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Rhodacal 70B as anionic surfactants against Termul 203
Ratio of Rhodacal 70B: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Rhodacal 70B: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4981.7 897
Solvent used: Diethylene Glycol Monoethyl Ether 933.3 186
Calcium Dodecylbenzene Sulphonate in butanol used: Rhodacal 70B (anionic surfactant) 132.5 26
Block Co-polymer 311.7 62
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used: Termul 203 (non-ionic surfactant)
Total 6359.2
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 897g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, traces of cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
Trial # IG9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul TANS 5 as ionic surfactants against Termul 203 Ratio of Toximul TANS 5: Termul 203 (30:70) lonic/Non-ionic surfactant/ Solvent used: Toximul TANS 5: Termul 203: Diethylene Glycol monoethyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4968.3 897
Solvent used: Diethylene Glycol Monoethyl Ether 933.3 186
Alkylphenol ether sulfate/tallow amines ethoxylated used: Toximul TANS 5 (anionic surfactant) 135.0 27
Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.8 61
Total 6342.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 897g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 1ml cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
Trial # IH9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul TANS 6 as ionic surfactants against Termul 203 Ratio of Toximul TANS 6: Termul 203 (30:70) lonic/Non-ionic surfactant/ Solvent used: Toximul TANS 6: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4965.0 896
Solvent used: Diethylene Glycol Monoethyl Ether 930.0 185
Alkylphenol ether sulfate/tallow amines ethoxylated used: Toximul TANS 6 (anionic surfactant) 145.0 29
Block Co-polymer used: Termul 203 (non-ionic surfactant) 310.0 62
Total 6350.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 896g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
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Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.9ml cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
Trial # 119
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul TANS 8 as ionic surfactants against Termul 203
Ratio of Toximul TANS 8: Termul 203 (30:70) lonic/Non-ionic surfactant/ Solvent used: Toximul TANS 8: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4980.0 901
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 916.7 183
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Alkylphenol ether sulfate/tallow amines ethoxylated used: Toximul TANS 8 (anionic surfactant) 130.8 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 303.3 61
Total 6330.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 901 g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, traces of cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
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Trial # IJ9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul TAABS 5 as ionic surfactants against Termul 203
Ratio of Toximul TAABS 5: Termul 203 (30:70) lonic/Non-ionic surfactant/ Solvent used: Toximul TAABS 5: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 897
Solvent used: Diethylene Glycol Monoethyl Ether 940.0 187
branched alcohol ether sulfate/tallow amines ethoxylated used: Toximul TAABS 5 (anionic surfactant) 130.0 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 309.2 62
Total 6349.2
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 897g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, traces of cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
Trial # IK9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul TAABS 8 as ionic surfactants against Termul 203 Ratio of Toximul TAABS 8: Termul 203 (30:70) lonic/Non-ionic surfactant/ Solvent used: Toximul TAABS 8: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 899
Solvent used: Diethylene Glycol Monoethyl Ether 933.3 186
branched alcohol ether sulfate/tallow amines ethoxylated used: Toximul TAABS 8 (anionic surfactant) 129.2 26
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Block Co-polymer used: Termul 203 (non-ionic surfactant) 303.3 61
Total 6335.8
RESULTS OF FORMULAT ON
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1% aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2ml cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
3472646vl
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APPENDIX 8
Trial # IA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4978.3 899
Solvent used: Diethylene Glycol Monoethyl Ether 917.5 183
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 136.7 27
Block Co-polymer used: Termul 203 (non-ionic surfactant) 313.3 63
Total 6345.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 899g/L Passed
pH at 1 % aq. Solution 6 to 8 7.35 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.266 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.3ml cream@bottom Passed
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Persistent Foaming <60mL after 1 min 25ml Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1212cps Passed
Viscosity (temperature at 20C) 0 to 2000cPs 315cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # IIA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Recosol 150
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4977.5 900
Solvent used: Recosol 150 923.3 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 129.2 26
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Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.8 61
Total 6335.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
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Trial # III A9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Recosol 200
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 899
Solvent used: Recosol 200 926.7 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 129.2 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 304.2 61
Total 6330.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # IVA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Xylene
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.3 900
Solvent used: Xylene 926.7 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 127.5 25
Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.0 61
Total 6332.5
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial #VA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Toluene
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4978.3 901
eg. Haloxyfop Tech (94% purity)
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Solvent used: Toluene 922.5 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 128.3 26
used: Ninate 60E (anionic surfactant)
Block Co-polymer used: Termul 203 (non-ionic surfactant) 304.2 61
Total 6333.3
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml cream&oil@botto m Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # VIA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Acetone
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4974.2 900
Solvent used: Acetone 925.0 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 130.8 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 304.2 61
Total 6334.2
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
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Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 3ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # VIIA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Dimethyl adipate
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4975.0 900
eg. Haloxyfop Tech (94% purity)
Solvent used: Dimethyl adipate 924.2 185
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Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 127.5 25
Block Co-polymer used: Termul 203 (non-ionic surfactant) 308.3 62
Total 6335.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 3ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, formed lumps Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
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Trial # VIIIA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Dimethyl succinate
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4976.7 899
Solvent used: Dimethyl succinate 935.0 187
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 128.3 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.0 61
Total 6345.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, formed lumps Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial # IXA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: NMP
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4971.7 898
Solvent used: NMP 927.5 185
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 131.7 26
Block Co-polymer 310.0 62
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used: Termul 203 (non-ionic surfactant)
Total 6340.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, formed lumps Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS AND COLD STAB FAILED
Trial #XA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: Ethylene glycol monobutyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifIuoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4971.7 899
Solvent used: Ethylene glycol monobutyl ether 923.3 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 130.0 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 313.3 63
Total 6338.3
RESULTS OF FORMULAT ON
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1% aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 2ml cream&oil@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
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Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial #XIA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: propylene glycol monomethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.3 900
Solvent used: propylene glycol monomethyl ether 922.5 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 131.7 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.0 61
Total 6332.5
RESULTS OF FORMULATION
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.2ml cream&oil@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASSED
Description: AWAITS FURTHER ANALYSIS
Trial # XIIA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: propylene glycol
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2- 4970.8 900
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pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity)
Solvent used: propylene glycol 920.0 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 132.5 27
Block Co-polymer used: Termul 203 (non-ionic surfactant) 306.7 61
Total 6330.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h n/a
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Yellow to brown solid Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE COLD STAB FAILED
Trial # XIIIA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: diethylene glycol
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 900
Solvent used: diethylene glycol 920.8 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 130.0 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.0 61
Total 6325.8
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h n/a
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Yellow to brown solid Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE COLD STAB FAILED
Trial #XIVA9
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Trial using Termul 203 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Termul 203: dipropylene glycol
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- 152FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.5 900
Solvent used: dipropylene glycol 920.8 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 132.5 26
Block Co-polymer used: Termul 203 (non-ionic surfactant) 305.0 61
Total 6330.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h Milky white emulsion, no separation, 5ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, phase separation@top Failed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTIC FAILED
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APPENDIX 9
Trial # J1
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Decrease in surfactant loading to 80% from the original formulation with constant surfactant ratio
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E : Termul 203 : Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L HLB
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.8 901
Solvent used: Diethylene Glycol Monoethyl Ether 978.9 196
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 105.1 21 3.31
Block Co-polymer used: Termul 203 (non-ionic surfactant) 244.4 49 12.24
Total 6301.2 15.55
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 901 g/L Passed
pH at 1%aq. Solution 6 to 8 6.92 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.261 Passed
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Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, traces of cream@ bottom of cylinder Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: AWAITS FURTHER ANALYSIS
Trial # J2
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Decrease in surfactant loading to 60% from the original formulation with constant surfactant ratio
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E : Termul 203 : Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L HLB
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.6 900
Solvent used: Diethylene Glycol Monoethyl Ether 1063.1 213
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 78.8 16 3.30
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used: Ninate 60E (anionic surfactant)
Block Co-polymer used: Termul 203 (non-ionic surfactant) 183.6 37 12.24
. Total 6298.1 15.55
RESULTS OF FORMULAT ON
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L Passed
pH at 1% aq. Solution 6 to 8 7.09 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.259 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, 1mi mixture of cream & oil @ bottom of cylinder Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
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Trial # J3
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Decrease in surfactant loading to 40% from the original formulation with constant surfactant ratio
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E : Termul 203 : Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L HLB
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.5 900
Solvent used: Diethylene Glycol Monoethyl Ether 1157.3 231
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 52.1 10 3.29
Block Co-polymer used: Termul 203 (non-ionic surfactant) 122.2 24 12.27
Total 6305.1 15.56
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L Passed
pH at 1 % aq. Solution 6 to 8 7.26 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.261 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 5ml mixture of cream&oil@bottom Failed
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Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER ANALYSIS BECAUSE EMULSION CHARACTERISTICS FAIL
Trial # J3
HALOXYFOP 900 TRIALS
Haloxyfop active present at 900g/L
Trial details: Decrease in surfactant loading to 20% from the original formulation with constant surfactant ratio
Ratio of N60E: Termul 203 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E : Termul 203 : Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L HLB
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.5 900
Solvent used: Diethylene Glycol Monoethyl Ether 1236.1 247
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 26 5 3.26
61.8 12 12.32
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Block Co-polymer used: Termul 203 (non-ionic surfactant)
Total 6296.4 15.58
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L Passed
pH at 1 % aq. Solution 6 to 8 7.32 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.259 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4.5ml mixture of cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER ANALYSIS BECAUSE EMULSION CHARACTERISTICS FAIL
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Trial# 4a
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Toximul 8320 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Toximul 8320: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.3 900
Solvent used: Diethylene Glycol Monoethyl Ether 920.8 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 143.3 29
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 310.0 62
Total 6347.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L Passed
pH at 1 % aq. Solution 6 to 8 7.60 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.266 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.5ml cream@bottom Passed
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Persistent Foaming <60mL after 1 min 6.0 mis Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format. Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1520 cps (LV3 @60rpm) Passed
Viscosity (temperature at 20C) 0 to 2000cPs 345 cps (LV2 @60rpm) Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. N/A n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # 4b
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N20 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4978.9 901
Solvent used: Diethylene Glycol Monoethyl Ether 929.4 186
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 150.6 30
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Nonyl Phenol Ethoxylates used: Teric N20 (non-ionic surfactant) 309.4 62
Total 6368.3
RESULTS OF FORMULAT ON
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1% aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.0ml cream&oil@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
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Trial# 4c
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N30 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N30 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N30: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 5000.3 905
Solvent used: Diethylene Glycol Monoethyl Ether 920.6 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 145.0 29
Nonyl Phenol Ethoxylates used: Teric N30 (non-ionic surfactant) 310.6 62
Total 6376.4
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml cream&oil@bottom Failed
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Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 4d
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N13 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N13 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N13: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.1 899
Solvent used: Diethylene Glycol Monoethyl Ether 931.1 186
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 149.6 30
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Nonyl Phenol Ethoxylates used: Teric N13 (non-ionic surfactant) 312.1 62
Total 6362.8
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1% aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2ml cream&oil@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
3472646v1
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Trial #4e
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N15 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N15 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N15: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4981.7 902
Solvent used: Diethylene Glycol Monoethyl Ether 920.6 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 151.7 30
Nonyl Phenol Ethoxylates used: Teric N15 (non-ionic surfactant) 324.8 65
Total 6378.7
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 3ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 4f
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N9 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N9 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N9: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4980.0 901
Solvent used: Diethylene Glycol Monoethyl Ether 938.3 188
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 151.4 30
Nonyl Phenol Ethoxylates 330.4 66
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used: Teric N9 (non-ionic surfactant)
Total 6400.2
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 1.5ml cream&oil@bottom. Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
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HALOXYFOP 800 TRIAL
Haloxyfop active present at 800g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Toximul 8320 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Toximul 8320: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (95% purity) 4433.2 802
Solvent used: Diethylene Glycol Monoethyl Ether 1371.0 274
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 127.0 25
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 320.0 64
Total 6251.2
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L Passed
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 1.270 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 1.0ml cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # 4h
HALOXYFOP 800 TRIAL
Haloxyfop active present at 800g/L
Trial details: Trial using Teric N30 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N30 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N30: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2- pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4420.0 800
Solvent used: Diethylene Glycol Monoethyl Ether 1419.0 284
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 127.5 26
Nonyl Phenol Ethoxylates used: Teric N30 (non-ionic surfactant) 303.0 61
Total 6269.5
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 4i
HALOXYFOP 800 TRIAL
Haloxyfop active present at 800g/L
Trial details: Trial using Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N20 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N20: Diethylene Glycol monoethyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4432.0 802
Solvent used: Diethylene Glycol Monoethyl Ether 1313.0 263
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 126.0 25
Nonyl Phenol Ethoxylates used: Teric N20 (non-ionic surfactant) 304.4 61
Total 6175.4
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4.0ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
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Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 4j
HALOXYFOP 800 TRIAL
Haloxyfop active present at 800g/L
Trial details: Trial using Teric N15 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N15 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N15: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4448.0 805
Solvent used: Diethylene Glycol Monoethyl Ether 1322.0 264
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 128.5 26
Nonyl Phenol Ethoxylates used: Teric N15 (non-ionic surfactant) 301.0 60
Total 6199.5
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 4k
HALOXYFOP 800 TRIAL
Haloxyfop active present at 800g/L
Trial details: Trial using Teric N13 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N13 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N13: Diethylene Glycol monoethyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4448.0 805
Solvent used: Diethylene Glycol Monoethyl Ether 1322.0 264
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 128.5 26
Nonyl Phenol Ethoxylates used: Teric N13 (non-ionic surfactant) 301.2 60
Total 6199.7
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 41
HALOXYFOP 800 TRIAL
Haloxyfop active present at 800g/L
Trial details: Trial using Teric N9 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N9 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N9: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4429.0 802
Solvent used: Diethylene Glycol Monoethyl Ether 1329.5 266
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 139.0 28
Nonyl Phenol Ethoxylates used: Teric N9 (non-ionic surfactant) 303.7 61
Total 6201.2
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1%aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2ml cream & trace of oil @ bottom Pass
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Pass
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial# 4m
HALOXYFOP 700 TRIAL
Haloxyfop active present at 700g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Toximul 8320 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Toximul 8320: Diethylene Glycol monoethyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 3882.5 703
Solvent used: Diethylene Glycol Monoethyl Ether 1689.5 338
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 139.5 28
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 322.5 65
Total 6034.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L Passed
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.3ml cream@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # 4n
HALOXYFOP 700 TRIAL
Haloxyfop active present at 700g/L
Trial details: Trial using Teric N30 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N30 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N30: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 3873.0 701
Solvent used: Diethylene Glycol Monoethyl Ether 1679.0 336
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 142.0 28
Nonyl Phenol Ethoxylates used: Teric N30 (non-ionic surfactant) 317.5 64
Total 6011.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
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Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, 4ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial #4o
HALOXYFOP 700 TRIAL
Haloxyfop active present at 700g/L
Trial details: Trial using Teric N20 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N20 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N20: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 3884.0 703
eg. Haloxyfop Tech (94% purity)
Solvent used: Diethylene Glycol Monoethyl Ether 1677.5 336
140.5 28
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Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant)
Nonyl Phenol Ethoxylates used: Teric N20 (non-ionic surfactant) 320.0 64
Total 6022.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion,, 3.0ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
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HALOXYFOP 700 TRIAL
Haloxyfop active present at 700g/L
Trial details: Trial using Teric N15 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N15 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N15: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 3870.0 700
Solvent used: Diethylene Glycol Monoethyl Ether 1710.0 342
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 140.0 28
Nonyl Phenol Ethoxylates used: Teric N15 (non-ionic surfactant) 321.0 64
Total 6041.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion,, 3ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial #4q
HALOXYFOP 700 TRIAL
Haloxyfop active present at 700g/L
Trial details: Trial using Teric N13 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N13 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N13: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 3873.0 701
Solvent used: Diethylene Glycol Monoethyl Ether 1673.0 335
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 136.0 27
Nonyl Phenol Ethoxylates 338.0 68
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used: Teric N13 (non-ionic surfactant)
Total 6020.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, 2.5ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 4r
HALOXYFOP 700 TRIAL
Haloxyfop active present at 700g/L
Trial details: Trial using Teric N9 as non-ionic surfactants against Ninate 60E
Ratio of N60E: Teric N9 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Ninate 60E: Teric N9: Diethylene Glycol monoethyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 3877.0 702
Solvent used: Diethylene Glycol Monoethyl Ether 1670.0 334
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 140.0 28
Nonyl Phenol Ethoxylates used: Teric N9 (non-ionic surfactant) 332.5 67
Total 6019.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, 2.5ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
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Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
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APPENDIX 11
Trial# 4s
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Kemmat HF60
Ratio of Kemmat HF60: Toximul 8320 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Kemmat HF 60: Toximul 8320: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4975.1 900
Solvent used: Diethylene Glycol Monoethyl Ether 876.1 175
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Kemmat HF 60 (anionic surfactant) 130.8 26
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 334.7 67
Total 6316.7
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900g/L Passed
pH at 1 % aq. Solution 6 to 8 7.15 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.263 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.3ml cream@bottom Passed
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Persistent Foaming <60mL after 1 min 10 mis Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1760 cps Passed
Viscosity (temperature at 20C) 0 to 2000cPs 465 cps Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # 4t
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Nanssa 70 EVM
Ratio of Nansa 70 EVM: Toximul 8320 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Nansa 70 EVM: Toximul 8320: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.3 900
Solvent used: Diethylene Glycol Monoethyl Ether 880.6 176
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Nansa 70 EVM (anionic surfactant) 131.4 26
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Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 340.9 68
Total 6326.1 900
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900 n/a
pH at 1 % aq. Solution 6 to 8 7.55 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 1.265 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 0.3ml cream&oil@bottom Pass
Persistent Foaming <60mL after 1 min 8 mis n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1640 cps n/a
Viscosity (temperature at 20C) 0 to 2000cPs 440 cps n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial #4u
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Rhodacal 70
Ratio of Rhodacal 70: Toximul 8320 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Rhodacal 70: Toximul 8320: Diethylene Glycol monoethyl ether
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Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4974.0 900
Solvent used: Diethylene Glycol Monoethyl Ether 907.0 181
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Rhodacal 70 (anionic surfactant) 139.5 28
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 320.0 64
Total 6340.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3.0ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
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Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial #4v
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Rhodacal 70B Ratio of Rhodacal 70B: Toximul 8320 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Rhodacal 70B: Toximul 8320: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4983.5 902
Solvent used: Diethylene Glycol Monoethyl Ether 837.5 168
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Rhodacal 70B (anionic surfactant) 162.5 33
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 320.0 64
Total 6303.5
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial#4w
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N13 as non-ionic surfactants against Kemmat HF 60
Ratio of Kemmat HF 60: Teric N9 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Kemmat HF60: Teric N9: Diethylene Glycol monoethyl ether
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4977.0 901
Solvent used: Diethylene Glycol Monoethyl Ether 894.0 179
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Kemmat HF 60 (anionic surfactant) 132.5 27
Nonyl Phenol Ethoxylates used: Teric N9 (non-ionic surfactant) 321.0 64
Total 6324.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1 % aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.5ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial #4x
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N9 as non-ionic surfactants against Nansa 70 EVM
Ratio of N60E: Teric N9 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Nanasa 70 EVM : Teric N9: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4977.0 901
Solvent used: Diethylene Glycol Monoethyl Ether 910.5 182
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Nansa 70 EVM (anionic surfactant) 146.5 29
Nonyl Phenol Ethoxylates used: Teric N9 (non-ionic surfactant) 313.0 63
Total 6347.0
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1% aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.0ml cream&oil@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial #4y
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N9 as non-ionic surfactants against Rhodacal 70
Ratio of N60E: Teric N9 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Rhodacal 70: Teric N9: Diethylene Glycol monoethyl ether
FORMULATION
3472646vl
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Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4983.5 902
Solvent used: Diethylene Glycol Monoethyl Ether 902.0 180
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Rhodacal 70 (anionic surfactant) 136.0 27
Nonyl Phenol Ethoxylates used: Teric N9 (non-ionic surfactant) 307.0 61
Total 6328.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1% aq. Solution 6 to 8 n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.0ml cream&oil@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
3472646v 1
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General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial #4z
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Teric N9 as non-ionic surfactants against Rhodacal 70B Ratio of N60E: Teric N9 (30:70)
Anionic/Non-ionic surfactant/ Solvent used: Rhodacal 70B: Teric N9: Diethylene Glycol monoethyl ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4976.5 901
Solvent used: Diethylene Glycol Monoethyl Ether 907.0 181
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Rhodacal 70B (anionic surfactant) 142.0 28
Nonyl Phenol Ethoxylates used: Teric N9 (non-ionic surfactant) 313.0 63
Total 6338.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous orange liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop n/a
pH at 1% aq. Solution 6 to 8 n/a
3472646vl
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Specific gravity (temperature at 20C) 1.25 to 1.27 n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.0ml cream&oil@bottom Passed
Persistent Foaming <60mL after 1 min n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Dark yellow to brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
3472646vl
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APPENDIX 12
Trial #4ae
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Recosol 200
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4972.5 900
Solvent used: Recosol 200 920.0 184
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 135.5 27
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 302.5 61
Total 6330.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop - n/a
pH at 1 % aq. Solution 6 to 8 - n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 - n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 3.0ml cream&oil@bottom Failed
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Persistent Foaming <60mL after 1 min - n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs - n/a
Viscosity (temperature at 20C) 0 to 2000cPs - n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial # 4af
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Butyl Glysolv
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4974.0 900
Solvent used: Butyl Glysolv 831.5 166
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 134.5 27
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Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 321.5 64
Total 6261.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 900 g/L Passed
pH at 1 % aq. Solution 6 to 8 7.30 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.252 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, Traces of cream at the bottom Passed
Persistent Foaming <60mL after 1 min 14 mis of foam after 1 min. Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1140cPs Passed
Viscosity (temperature at 20C) 0 to 2000cPs 300cPs Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial #4ag
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Recosol 150
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FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4974.0 900
Solvent used: Recosol 150 815.0 163
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 140.0 28
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 309.5 62
Total 6238.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop - n/a
pH at 1 % aq. Solution 6 to 8 - n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 - n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.0ml cream&oil@bottom Failed
Persistent Foaming <60mL after 1 min - n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs - n/a
Viscosity (temperature at 20C) 0 to 2000cPs - n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial #4ah
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Ethylene Glycol Monobutyl Ether
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4976.5 901
Solvent used: Ethylene Glycol Monobutyl Ether 850.0 170
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 129.0 26
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 299.0 60
Total 6254.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 901 g/L Passed
pH at 1 % aq. Solution 6 to 8 7.13 Passed
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Specific gravity (temperature at 20C) 1.25 to 1.27 1.251 Passed
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, Traces of cream@bottom Passed
Persistent Foaming <60mL after 1 min 18mls of foam after 1 min. Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 1120 cPs Passed
Viscosity (temperature at 20C) 0 to 2000cPs 310 cPs Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # 4ai
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Dimethyl Succinate
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4982.5 902
eg. Haloxyfop Tech (94% purity)
Solvent used: Dimethyl Succinate 992.0 198
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol 134.0 27
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used: Ninate 60E (anionic surfactant)
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 312.0 62
Total 6420.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Formulation is not stable -
Assay 875 to 925g/L Haloxyfop - n/a
pH at 1 % aq. Solution 6 to 8 - n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 - n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h - n/a
Persistent Foaming <60mL after 1 min - n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format - n/a
Viscosity (temperature at 5C) 0 to 2000cPs - n/a
Viscosity (temperature at 20C) 0 to 2000cPs - n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE FORMULATION IS NOT STABLE
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Trial # 4aj
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Toluene
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 899
Solvent used: Toluene 816.5 163
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 130.5 26
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 304.5 61
Total 6221.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 899 g/L Passed
pH at 1%aq. Solution 6 to 8 7.69 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.244 -
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 1.0ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 12 mis of foam Passed
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-207 -
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 690 cPs Passed
Viscosity (temperature at 20C) 0 to 2000cPs 135 cPs Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial #4ak
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Acetone
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4970.0 899
Solvent used: Acetone 730.0 146
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 143.0 29
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 318.5 64
Total 6161.5
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RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop 899 g/L Passed
pH at 1%aq. Solution 6 to 8 7.69 Passed
Specific gravity (temperature at 20C) 1.25 to 1.27 1.232 -
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 0.2ml cream@bottom Passed
Persistent Foaming <60mL after 1 min 12mlsoffoam Passed
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs 260 cPs Passed
Viscosity (temperature at 20C) 0 to 2000cPs 73 cPs Passed
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? PASS
Description: SOLUTION MEETS ALL CRITERIA
Trial # 4al
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Dimethyl Adipate
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4973.0 900
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eg. Haloxyfop Tech (94% purity)
Solvent used: Dimethyl Adipate 933.5 187
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 144.5 29
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 309.5 62
Total 6360.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Formulation is not stable -
Assay 875 to 925g/L Haloxyfop - n/a
pH at 1 % aq. Solution 6 to 8 - n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 - n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h - n/a
Persistent Foaming <60mL after 1 min - n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format - n/a
Viscosity (temperature at 5C) 0 to 2000cPs n/a
Viscosity (temperature at 20C) 0 to 2000cPs - n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
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General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE FORMULATION IS NOT STABLE
Trial#4am
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: Xylene
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4975.0 900
Solvent used: Xylene 795.0 159
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 128.5 26
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 313.0 63
Total 6211.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop - n/a
pH at 1 % aq. Solution 6 to 8 - n/a
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Specific gravity (temperature at 20C) 1.25 to 1.27 - n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.5ml cream Failed
Persistent Foaming <60mL after 1 min - n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs - n/a
Viscosity (temperature at 20C) 0 to 2000cPs - n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
Trial #4an
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E Ratio of Ninate 60E: Toximul 8320 (30:70)
Solvent: N-methylpyrrolidone
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate 4971.0 900
eg. Haloxyfop Tech (94% purity)
Solvent used: N-methylpyrrolidone 924.5 185
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Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 140.0 28
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 306.5 61
Total 6342.0
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop - n/a
pH at 1 % aq. Solution 6 to 8 - n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 - n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete reemulsion after 24h milky emulsion, no separation, 2.5ml cream@bottom Failed
Persistent Foaming <60mL after 1 min - n/a
Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs - n/a
Viscosity (temperature at 20C) 0 to 2000cPs - n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
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2014203147 11 Jun2014
-213 Trial #4ao
HALOXYFOP 900 TRIAL
Haloxyfop active present at 900g/L
Trial details: Trial using Toximul 8320 as non-ionic surfactants against Ninate 60E
Ratioof Ninate 60E: Toximul 8320 (30:70)
Solvent: Exxate 700
FORMULATION
Component (Chemical name) Amount, g Loading, g/L
methyl (R) -2-[4-(3-chloro-5-trifluoromethyl-2pyridyloxy)phenoxy]propanoate eg. Haloxyfop Tech (94% purity) 4973.0 900
Solvent used: Exxate 700 812.5 163
Calcium C10-16 alkyl benzenesulfonic acid in 2-ethyl hexanol used: Ninate 60E (anionic surfactant) 126.5 25
Block Co-polymer used: Toximul 8320 (non-ionic surfactant) 301.5 60
Total 6213.5
RESULTS OF FORMULATION
Parameter Required Results Remarks
Appearance Red to brown liquid, homogeneous Brown liquid, homogeneous Passed
Assay 875 to 925g/L Haloxyfop - n/a
pH at 1 % aq. Solution 6 to 8 - n/a
Specific gravity (temperature at 20C) 1.25 to 1.27 - n/a
Emulsion characteristics <2mL cream after 30 min, trace of oil after 30 min and complete re-emulsion after 24h milky emulsion, no separation, 2.5ml cream@bottom Failed
Persistent Foaming <60mL after 1 min - n/a
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Cold temp, stability (Accelerated Ageing) Dark yellow to brown liquid, homogeneous, free from phase separation in any format Brown liquid, homogeneous, free from phase separation in any format Passed
Viscosity (temperature at 5C) 0 to 2000cPs - n/a
Viscosity (temperature at 20C) 0 to 2000cPs - n/a
Long Term Performance Test parameter maintained within required range after accelerated aging to approximate 2 years. - n/a
General Remarks PASS or FAIL? FAIL
Description: DID NOT CONTINUE ANY FURTHER TESTING BECAUSE EMULSION CHARACTERISTICS FAILED
215
2014203147 29 Jan 2018

Claims (23)

1. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of at least 825 g/L; an agriculturally acceptable surfactant selected from the group consisting of an alkylbenzene sulfonate, a tallow amine ethoxylate, an ether sulfate, an alcohol alkoxylate, a nonylphenol-9-ethylene oxide, a nonylphenol-20-ethylene oxide, a butyl alkylene oxide block copolymer and any combination thereof; and an agriculturally acceptable solvent comprising a monoalkyl ether.
2. The emulsifiable concentrate formulation of Claim 1, wherein the agriculturally acceptable surfactant is present at a concentration of at least about 45 g/L.
3. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of at least about 825 g/L; an agriculturally acceptable ionic surfactant;
an agriculturally acceptable non-ionic surfactant selected from the group consisting of an alcohol alkoxylate, a nonylphenol-9-ethylene oxide, a nonylphenol20-ethylene oxide, a butyl alkylene oxide block copolymer and any combination thereof; and an agriculturally acceptable solvent comprising a monoalkyl ether.
4. The emulsifiable concentrate formulation of Claim 3, wherein the ionic surfactant is selected from the group consisting of an alkylbenzene sulfonate, an alkylphenol ether sulfate, a tallow amine ethoxylate, an ether sulfate and any combination thereof.
5. The emulsifiable concentrate fonnulation of Claim 3 or Claim 4, wherein the ionic surfactant is present at a concentration of at least about 9 g/L.
6. The emulsifiable concentrate formulation of Claim 5, wherein the ionic surfactant is present at a concentration of at least about 12.5 g/L.
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2014203147 29 Jan 2018
7. The emulsifiable concentrate formulation of any one of Claims 3 to 6, wherein the non-ionic surfactant is present at a concentration of at least about 36 g/L.
8. The emulsifiable concentrate formulation of Claim 7, wherein the non-ionic surfactant is present at a concentration of at least about 57.5 g/L.
9. The emulsifiable concentrate formulation of any one of Claims 3 to 8, wherein the ionic surfactant is or comprises an anionic surfactant.
10. The emulsifiable concentrate formulation of any one of the preceding claims, wherein the alcohol alkoxylate is or comprises polypropylene glycol alkoxylate.
11. The emulsifiable concentrate formulation of any one of the preceding claims, wherein the solvent is or comprises a monomethyl ether, a monoethyl ether, a monobutyl ether or any combination thereof.
12. The emulsifiable concentrate formulation of any one of the preceding claims, wherein the solvent is present at a concentration of at least about 180 g/L.
13. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of at least about 650 g/L; a first agriculturally acceptable surfactant comprising an ionic surfactant; a second agriculturally acceptable surfactant selected from the group consisting of:
an alcohol alkoxylate; and a butyl alkylene oxide block copolymer; and an agriculturally acceptable solvent present at a concentration of at least about 187 g/L, wherein the solvent is or comprises a pyrrolidone.
14. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of at least about 650 g/L; a first agriculturally acceptable surfactant comprising an ionic surfactant; a second agriculturally acceptable surfactant comprising a butyl alkylene oxide block copolymer; and
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2014203147 29 Jan 2018 an agriculturally acceptable solvent selected from the group consisting of an alkyl ether, a mono-substituted benzene, a ketone and any combination thereof.
15. The emulsifiable concentrate formulation of Claim 13 or Claim 14, wherein the first agriculturally acceptable surfactant is present at a concentration of at least about 12.5 g/L.
16. The emulsifiable concentrate formulation of any one of Claims 13 to 15, wherein the second agriculturally acceptable surfactant is present at a concentration of at least about 57.5 g/L.
17. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of at least about 850 g/L; an agriculturally acceptable ionic surfactant;
an agriculturally acceptable non-ionic surfactant selected from the group consisting of:
a nonylphenol-13-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is at least about 0.3:1;
a nonylphenol-15-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is less than about 0.15:1; and an agriculturally acceptable solvent comprising a monoalkyl ether.
18. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of about 750 g/L to about
850 g/L;
an agriculturally acceptable ionic surfactant;
an agriculturally acceptable non-ionic surfactant selected from the group consisting of:
a butyl alkylene oxide block copolymer;
a nonylphenol-20-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is less than about 0.15:1;
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2014203147 29 Jan 2018 a nonylphenol-30-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is less than about 0.26:1; and a nonylphenol-15-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is at least about 0.4:1; and an agriculturally acceptable solvent comprising a monoalkyl ether.
19. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of about 650 g/L to about
750 g/L;
an agriculturally acceptable ionic surfactant;
an agriculturally acceptable non-ionic surfactant selected from the group consisting of:
a butyl alkylene oxide block copolymer;
a nonylphenol-20-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is less than about 0.26:1;
a nonylphenol-13-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is less than about 0.26:1;
a nonylphenol-15-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is at least about 0.4:1; and a nonylphenol-9-ethylene oxide present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is less than about 0.26:1; and an agriculturally acceptable solvent comprising a monoalkyl ether.
20. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of at least about 850 g/L; an agriculturally acceptable ionic surfactant;
an agriculturally acceptable non-ionic surfactant comprising a butyl alkylene oxide block copolymer, wherein the non-ionic surfactant is present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is at least about 0.4:1; and an agriculturally acceptable solvent comprising xylene.
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21. An emulsifiable concentrate formulation comprising:
haloxyfop or a derivative thereof at a concentration of at least about 850 g/L; an agriculturally acceptable ionic surfactant;
an agriculturally acceptable non-ionic surfactant comprising a butyl alkylene oxide block copolymer, wherein the non-ionic surfactant is present at a concentration such that the ratio of the ionic surfactant to the non-ionic surfactant is less than about 0.15:1;
an agriculturally acceptable solvent comprising a pyrrolidone.
22. The emulsifiable concentrate formulation of any one of Claims 13 to 21, wherein the ionic surfactant is or comprises an alkylbenzene sulfonate.
23. A method of selectively killing or suppressing weeds such as barley grass, brome grass, paradoxa grass, volunteer cereals, wild oats, musky or ferny leaf Storksbill, common crowsfoot, common storksbill, long or shiny leaf storksbill, couch grass, Rhodes grass, Australian millet, barnyard grass, green panic, Johnson grass, liverseed grass, Mossman river grass, summer grass, slender rats tail grass, Buffel grass, kikuyu, paspalum spp, starai spp, annual ryegrass, lesser canary grass, Rope twitch, Erodium spp which comprises adding an emulsifiable concentrate fonnulation as claimed in any one of claims 1 to 22 to an amount of spray water in a spray tank sufficient to make up a diluted liquor of generally accepted strength and spraying the resultant diluted liquor onto weeds or ground.
3517940vl
AU2014203147A 2013-06-28 2014-06-11 High level haloxyfop emulsifiable concentrate formulation Active AU2014203147B2 (en)

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AU2013902397A AU2013902397A0 (en) 2013-06-28 High level haloxyfop emulsifiable concentrate formulation
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US20230232829A1 (en) * 2018-01-04 2023-07-27 Dow Argo Sciences LLC High-load haloxyfop ester compositions
AU2021107371B4 (en) * 2021-08-25 2022-07-14 Adama Australia Pty Limited Highly Loaded Haloxyfop Formulations

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6444618B1 (en) * 1999-01-29 2002-09-03 Basf Aktiengesellschaft Crop protection emulsifiable concentrate containing defoaming agents

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6444618B1 (en) * 1999-01-29 2002-09-03 Basf Aktiengesellschaft Crop protection emulsifiable concentrate containing defoaming agents

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