AU2005293039A1 - Method for producing metal by molten salt electrolysis and method for producing metal titanium - Google Patents
Method for producing metal by molten salt electrolysis and method for producing metal titanium Download PDFInfo
- Publication number
- AU2005293039A1 AU2005293039A1 AU2005293039A AU2005293039A AU2005293039A1 AU 2005293039 A1 AU2005293039 A1 AU 2005293039A1 AU 2005293039 A AU2005293039 A AU 2005293039A AU 2005293039 A AU2005293039 A AU 2005293039A AU 2005293039 A1 AU2005293039 A1 AU 2005293039A1
- Authority
- AU
- Australia
- Prior art keywords
- metal
- calcium
- electrolysis
- chloride
- molten
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- 229910052751 metal Inorganic materials 0.000 title claims description 147
- 239000002184 metal Substances 0.000 title claims description 147
- 238000005868 electrolysis reaction Methods 0.000 title claims description 137
- 150000003839 salts Chemical class 0.000 title claims description 39
- 238000004519 manufacturing process Methods 0.000 title claims description 23
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 title claims description 17
- 239000010936 titanium Substances 0.000 title claims description 17
- 229910052719 titanium Inorganic materials 0.000 title claims description 17
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 102
- 239000011575 calcium Substances 0.000 claims description 102
- 229910052791 calcium Inorganic materials 0.000 claims description 102
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 59
- 239000001110 calcium chloride Substances 0.000 claims description 59
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 59
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 54
- 239000001103 potassium chloride Substances 0.000 claims description 27
- 235000011164 potassium chloride Nutrition 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 26
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 13
- 230000005496 eutectics Effects 0.000 claims description 12
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 11
- 229910001634 calcium fluoride Inorganic materials 0.000 claims description 11
- 239000011780 sodium chloride Substances 0.000 claims description 11
- 239000003638 chemical reducing agent Substances 0.000 claims description 6
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 claims description 5
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 3
- 229910001510 metal chloride Inorganic materials 0.000 claims description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 230000008018 melting Effects 0.000 description 22
- 238000002844 melting Methods 0.000 description 22
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 13
- 238000011084 recovery Methods 0.000 description 13
- 239000007787 solid Substances 0.000 description 13
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 description 9
- 239000010439 graphite Substances 0.000 description 8
- 229910002804 graphite Inorganic materials 0.000 description 8
- 238000000354 decomposition reaction Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 5
- 229910052799 carbon Inorganic materials 0.000 description 5
- 150000001805 chlorine compounds Chemical class 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 229910000975 Carbon steel Inorganic materials 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 239000010962 carbon steel Substances 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 238000006722 reduction reaction Methods 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 4
- 230000003247 decreasing effect Effects 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
- 238000004090 dissolution Methods 0.000 description 3
- 229910001209 Low-carbon steel Inorganic materials 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 230000000149 penetrating effect Effects 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000013519 translation Methods 0.000 description 2
- 229910004261 CaF 2 Inorganic materials 0.000 description 1
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 229910010293 ceramic material Inorganic materials 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 239000002923 metal particle Substances 0.000 description 1
- 239000013528 metallic particle Substances 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 230000010287 polarization Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003609 titanium compounds Chemical class 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
- C25C3/02—Electrolytic production, recovery or refining of metals by electrolysis of melts of alkali or alkaline earth metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/129—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/26—Chlorine; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C3/00—Electrolytic production, recovery or refining of metals by electrolysis of melts
- C25C3/26—Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium
- C25C3/28—Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium of titanium
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inorganic Chemistry (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Electrolytic Production Of Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2004297873 | 2004-10-12 | ||
| JP2004-297873 | 2004-10-12 | ||
| PCT/JP2005/018452 WO2006040979A1 (ja) | 2004-10-12 | 2005-10-05 | 溶融塩電解による金属の製造方法および金属チタンの製造方法 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU2005293039A1 true AU2005293039A1 (en) | 2006-04-20 |
Family
ID=36148274
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2005293039A Abandoned AU2005293039A1 (en) | 2004-10-12 | 2005-10-05 | Method for producing metal by molten salt electrolysis and method for producing metal titanium |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20080053838A1 (ja) |
| EP (1) | EP1808513A4 (ja) |
| JP (1) | JP4602986B2 (ja) |
| CN (1) | CN101040064A (ja) |
| AU (1) | AU2005293039A1 (ja) |
| CA (1) | CA2582039A1 (ja) |
| EA (1) | EA011110B1 (ja) |
| NO (1) | NO20072149L (ja) |
| WO (1) | WO2006040979A1 (ja) |
Families Citing this family (34)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB0714021D0 (en) * | 2007-07-18 | 2007-08-29 | Green Metals Ltd | Improvements in anode materials |
| GB0801791D0 (en) * | 2008-01-31 | 2008-03-05 | Univ Leeds | Process |
| JP5138465B2 (ja) * | 2008-05-27 | 2013-02-06 | 東邦チタニウム株式会社 | 金属カルシウムの製造方法および製造装置 |
| CN101519789A (zh) * | 2009-03-30 | 2009-09-02 | 攀钢集团研究院有限公司 | 一种钛循环熔盐电解制取金属钛的方法 |
| US9076996B2 (en) | 2009-07-20 | 2015-07-07 | Massachusetts Institute Of Technology | Liquid metal alloy energy storage device |
| WO2012018379A1 (en) | 2010-08-06 | 2012-02-09 | Massachusetts Institute Of Technology | Electrolytic recycling of compounds |
| US9000713B2 (en) | 2010-09-20 | 2015-04-07 | Massachussetts Institute Of Technology | Alkali metal ion battery with bimetallic electrode |
| JP6286438B2 (ja) | 2012-10-16 | 2018-02-28 | アンブリ・インコーポレイテッド | 電気化学エネルギー蓄積デバイスおよびハウジング |
| US11211641B2 (en) | 2012-10-18 | 2021-12-28 | Ambri Inc. | Electrochemical energy storage devices |
| US9312522B2 (en) | 2012-10-18 | 2016-04-12 | Ambri Inc. | Electrochemical energy storage devices |
| US11387497B2 (en) | 2012-10-18 | 2022-07-12 | Ambri Inc. | Electrochemical energy storage devices |
| US10541451B2 (en) | 2012-10-18 | 2020-01-21 | Ambri Inc. | Electrochemical energy storage devices |
| US9520618B2 (en) | 2013-02-12 | 2016-12-13 | Ambri Inc. | Electrochemical energy storage devices |
| US11721841B2 (en) | 2012-10-18 | 2023-08-08 | Ambri Inc. | Electrochemical energy storage devices |
| US9735450B2 (en) | 2012-10-18 | 2017-08-15 | Ambri Inc. | Electrochemical energy storage devices |
| US10270139B1 (en) | 2013-03-14 | 2019-04-23 | Ambri Inc. | Systems and methods for recycling electrochemical energy storage devices |
| US9502737B2 (en) | 2013-05-23 | 2016-11-22 | Ambri Inc. | Voltage-enhanced energy storage devices |
| US12347832B2 (en) | 2013-09-18 | 2025-07-01 | Ambri, LLC | Electrochemical energy storage devices |
| EP3058605B1 (en) | 2013-10-16 | 2023-12-06 | Ambri Inc. | Seals for high temperature reactive material devices |
| WO2015058165A1 (en) | 2013-10-17 | 2015-04-23 | Ambri Inc. | Battery management systems for energy storage devices |
| US12142735B1 (en) | 2013-11-01 | 2024-11-12 | Ambri, Inc. | Thermal management of liquid metal batteries |
| CN103898553B (zh) * | 2014-03-25 | 2016-06-22 | 中国科学院过程工程研究所 | 一种电积和精炼同步进行生产金属钙的方法 |
| CN105531401B (zh) * | 2014-06-30 | 2018-09-04 | 东邦钛株式会社 | 制造金属的方法以及制造高熔点金属的方法 |
| US10170799B2 (en) | 2014-12-15 | 2019-01-01 | Massachusetts Institute Of Technology | Multi-element liquid metal battery |
| AU2016225020A1 (en) | 2015-02-27 | 2017-09-14 | Massachusetts Institute Of Technology | Electrochemical cell with bipolar faradaic membrane |
| US10181800B1 (en) | 2015-03-02 | 2019-01-15 | Ambri Inc. | Power conversion systems for energy storage devices |
| WO2016141354A2 (en) | 2015-03-05 | 2016-09-09 | Ambri Inc. | Ceramic materials and seals for high temperature reactive material devices |
| US9893385B1 (en) | 2015-04-23 | 2018-02-13 | Ambri Inc. | Battery management systems for energy storage devices |
| US11929466B2 (en) | 2016-09-07 | 2024-03-12 | Ambri Inc. | Electrochemical energy storage devices |
| EP3607603A4 (en) | 2017-04-07 | 2021-01-13 | Ambri Inc. | MOLTEN SALT BATTERY WITH SOLID METAL CATHODE |
| CN107475539B (zh) * | 2017-08-18 | 2019-05-17 | 中南大学 | 一种气态电化学制备金属钛的方法 |
| AU2019405440A1 (en) | 2018-12-17 | 2021-08-12 | Ambri, LLC | High temperature energy storage systems and methods |
| CN113279022B (zh) * | 2021-05-14 | 2022-04-19 | 奥勇新材料科技（上海）有限公司 | 一种还原性熔盐介质及其制备方法 |
| CN114672850B (zh) * | 2022-05-07 | 2023-08-29 | 华北理工大学 | 一种利用熔盐电解脱氧分离钛铝合金制取金属钛的方法 |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US806006A (en) * | 1903-01-20 | 1905-11-28 | Otto Ruff | Process of manufacturing calcium. |
| US2043756A (en) * | 1933-09-06 | 1936-06-09 | Lalancette Joseph Ovila | Free vision windshield |
| US2921890A (en) * | 1950-03-27 | 1960-01-19 | Chicago Dev Corp | Electrolytic method for the production of pure titanium |
| US2951021A (en) * | 1952-03-28 | 1960-08-30 | Nat Res Corp | Electrolytic production of titanium |
| US3043756A (en) * | 1958-07-31 | 1962-07-10 | Dow Chemical Co | Calcium metal production |
| ES257371A1 (es) * | 1959-05-13 | 1960-11-16 | Solvay | Procedimiento para la preparaciën de un metal alcalino-terreo por electrëlisis de banos de cloruros fundidos |
| GB950889A (en) * | 1961-10-25 | 1964-02-26 | Atomic Energy Authority Uk | Improvements in or relating to the production of alkaline earth metals |
| BE624084A (ja) * | 1961-10-25 | |||
| JPS4970808A (ja) * | 1972-11-10 | 1974-07-09 | ||
| US4032328A (en) * | 1975-10-23 | 1977-06-28 | University Of Minnesota, Inc. | Metal reduction process |
| FR2582019B1 (fr) * | 1985-05-17 | 1987-06-26 | Extramet Sa | Procede pour la production de metaux par reduction de sels metalliques, metaux ainsi obtenus et dispositif pour sa mise en oeuvre |
| CA2012009C (en) * | 1989-03-16 | 1999-01-19 | Tadashi Ogasawara | Process for the electrolytic production of magnesium |
| ITTO970080A1 (it) * | 1997-02-04 | 1998-08-04 | Marco Vincenzo Ginatta | Procedimento per la produzione elettrolitica di metalli |
| AUPR602901A0 (en) * | 2001-06-29 | 2001-07-26 | Bhp Innovation Pty Ltd | Removal of oxygen from metals oxides and solid metal solutions |
| JP3718691B2 (ja) * | 2002-04-18 | 2005-11-24 | 財団法人生産技術研究奨励会 | チタンの製造方法、純金属の製造方法、及び純金属の製造装置 |
| JP4395386B2 (ja) * | 2003-10-10 | 2010-01-06 | 株式会社大阪チタニウムテクノロジーズ | Ｃａ源の循環によるＴｉ又はＴｉ合金の製造方法 |
| JP2005264320A (ja) * | 2004-02-20 | 2005-09-29 | Sumitomo Titanium Corp | Ｃａ還元によるＴｉ又はＴｉ合金の製造方法 |
-
2005
- 2005-10-05 CA CA002582039A patent/CA2582039A1/en not_active Abandoned
- 2005-10-05 AU AU2005293039A patent/AU2005293039A1/en not_active Abandoned
- 2005-10-05 EA EA200700839A patent/EA011110B1/ru not_active IP Right Cessation
- 2005-10-05 WO PCT/JP2005/018452 patent/WO2006040979A1/ja not_active Ceased
- 2005-10-05 CN CNA2005800349295A patent/CN101040064A/zh active Pending
- 2005-10-05 JP JP2006540892A patent/JP4602986B2/ja not_active Expired - Fee Related
- 2005-10-05 EP EP05790446A patent/EP1808513A4/en not_active Withdrawn
- 2005-10-05 US US11/576,891 patent/US20080053838A1/en not_active Abandoned
-
2007
- 2007-04-25 NO NO20072149A patent/NO20072149L/no not_active Application Discontinuation
Also Published As
| Publication number | Publication date |
|---|---|
| JPWO2006040979A1 (ja) | 2008-05-15 |
| JP4602986B2 (ja) | 2010-12-22 |
| EA200700839A1 (ru) | 2007-08-31 |
| CN101040064A (zh) | 2007-09-19 |
| EA011110B1 (ru) | 2008-12-30 |
| EP1808513A1 (en) | 2007-07-18 |
| WO2006040979A1 (ja) | 2006-04-20 |
| NO20072149L (no) | 2007-04-25 |
| US20080053838A1 (en) | 2008-03-06 |
| EP1808513A4 (en) | 2009-07-29 |
| CA2582039A1 (en) | 2006-04-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK4 | Application lapsed section 142(2)(d) - no continuation fee paid for the application |