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AU2001238109A1 - Sol-gel monolithic column with optical window and method of making - Google Patents

Sol-gel monolithic column with optical window and method of making

Info

Publication number
AU2001238109A1
AU2001238109A1 AU2001238109A AU3810901A AU2001238109A1 AU 2001238109 A1 AU2001238109 A1 AU 2001238109A1 AU 2001238109 A AU2001238109 A AU 2001238109A AU 3810901 A AU3810901 A AU 3810901A AU 2001238109 A1 AU2001238109 A1 AU 2001238109A1
Authority
AU
Australia
Prior art keywords
sol
making
optical window
monolithic column
gel monolithic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001238109A
Inventor
James D. Hayes
Abdul Malik
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
University of South Florida St Petersburg
Original Assignee
University of South Florida
University of South Florida St Petersburg
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by University of South Florida, University of South Florida St Petersburg filed Critical University of South Florida
Publication of AU2001238109A1 publication Critical patent/AU2001238109A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/291—Gel sorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28042—Shaped bodies; Monolithic structures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282—Porous sorbents
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/416—Systems
    • G01N27/447—Systems using electrophoresis
    • G01N27/44704—Details; Accessories
    • G01N27/44717—Arrangements for investigating the separated zones, e.g. localising zones
    • G01N27/44721—Arrangements for investigating the separated zones, e.g. localising zones by optical means
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/26—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating electrochemical variables; by using electrolysis or electrophoresis
    • G01N27/416—Systems
    • G01N27/447—Systems using electrophoresis
    • G01N27/44704—Details; Accessories
    • G01N27/44747—Composition of gel or of carrier mixture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
    • B01D15/20—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the sorbent material
    • B01D15/206—Packing or coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/52—Sorbents specially adapted for preparative chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/50—Aspects relating to the use of sorbent or filter aid materials
    • B01J2220/54—Sorbents specially adapted for analytical or investigative chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2220/00—Aspects relating to sorbent materials
    • B01J2220/80—Aspects related to sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J2220/82—Shaped bodies, e.g. monoliths, plugs, tubes, continuous beds
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid
    • G01N30/52—Physical parameters
    • G01N2030/524—Physical parameters structural properties
    • G01N2030/528—Monolithic sorbent material
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/60—Construction of the column
    • G01N30/6052—Construction of the column body
    • G01N30/6082—Construction of the column body transparent to radiation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
AU2001238109A 2000-02-09 2001-02-09 Sol-gel monolithic column with optical window and method of making Abandoned AU2001238109A1 (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US18137100P 2000-02-09 2000-02-09
US60181371 2000-02-09
US18164200P 2000-02-10 2000-02-10
US60181642 2000-02-10
PCT/US2001/004271 WO2001058562A1 (en) 2000-02-09 2001-02-09 Sol-gel monolithic column with optical window and method of making

Publications (1)

Publication Number Publication Date
AU2001238109A1 true AU2001238109A1 (en) 2001-08-20

Family

ID=26877128

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001238109A Abandoned AU2001238109A1 (en) 2000-02-09 2001-02-09 Sol-gel monolithic column with optical window and method of making

Country Status (3)

Country Link
US (2) US7947174B2 (en)
AU (1) AU2001238109A1 (en)
WO (1) WO2001058562A1 (en)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU765881B2 (en) * 1998-08-21 2003-10-02 University Of South Florida Capillary column and method of making
US6998040B2 (en) * 2001-01-24 2006-02-14 University Of South Florida Sol-gel open tubular ODS columns with charged inner surface for capillary electrochromatography
US20040129141A1 (en) * 2002-03-08 2004-07-08 Abdul Malik High efficiency sol-gel gas chromatography column
US20030164297A1 (en) * 2002-03-04 2003-09-04 Corning Incorporated Electrophoretic inorganic porous material
EP1509533B1 (en) * 2002-05-31 2009-10-21 McMaster University Polyol-modified silanes as precursors for silica
WO2004018360A1 (en) * 2002-08-23 2004-03-04 Mcmaster University Methods and compounds for controlling the morphology and shrinkage of silica derived from polyol-modified silanes
US7407568B1 (en) * 2002-11-08 2008-08-05 University Of South Florida Method of using sol-gel coatings for on-line preconcentration of amino acids in capillary electrophoresis
DE112004000906T5 (en) * 2003-05-28 2006-10-19 Waters Investments Ltd., New Castle New nanocomposites and their application as monolithic columns
US20050106068A1 (en) * 2003-11-18 2005-05-19 Abdul Malik Sol-gel dendron separation and extraction capillary column
US20050127002A1 (en) * 2003-12-12 2005-06-16 Zare Richard N. Immobilized-enzyme microreactor devices for characterization of biomolecular analytes and associated methods
JP2008501961A (en) * 2004-06-09 2008-01-24 メルク　パテント　ゲゼルシャフト　ミット　ベシュレンクテル　ハフトング Open tubular capillary with connecting layer
US7439272B2 (en) * 2004-12-20 2008-10-21 Varian, Inc. Ultraporous sol gel monoliths
ES2593478T3 (en) * 2006-04-07 2016-12-09 Merck Patent Gmbh Manufacture of monolithic separation columns
EP1843154A1 (en) * 2006-04-07 2007-10-10 MERCK PATENT GmbH Preparation of monolithic separation columns
EP1843155B1 (en) * 2006-04-07 2016-06-29 Merck Patent GmbH Production of monolithic separating columns
EP2079665A4 (en) * 2006-11-07 2017-01-18 Waters Technologies Corporation Monolithic electrokinetic pump fabrication
US7651762B2 (en) * 2007-03-13 2010-01-26 Varian, Inc. Methods and devices using a shrinkable support for porous monolithic materials
JP4660563B2 (en) * 2008-02-28 2011-03-30 株式会社日立ハイテクノロジーズ Separation column and liquid chromatograph
CN101537344B (en) * 2009-04-23 2011-05-18 中国科学院化学研究所 Monolithic column, preparation method and application thereof
CN102489345B (en) * 2011-12-05 2013-08-28 福州大学 Hydrophilic strong anion exchange action hybrid silica gel capillary chromatographic column
CN103170161B (en) * 2011-12-22 2014-09-24 中国科学院大连化学物理研究所 A kind of preparation method of organic-inorganic hybrid monolithic column
CN102940979B (en) * 2012-10-22 2015-03-04 暨南大学 Method and application for preparing cyclodextrin organic polymer capillary monolithic column via one-step method
EP3118277B1 (en) * 2014-03-10 2019-10-23 Kyoto University Method for producing surface-modified substrate, method for producing conjugate, novel hydrosilane compound, surface treatment agent, surface treatment agent kit, and surface-modified substrate
CN105944700A (en) * 2016-05-25 2016-09-21 厦门华厦学院 A kind of preparation method of porous fibrous silicon sphere solid phase microextraction coating
US10618030B2 (en) * 2016-06-30 2020-04-14 University Of South Florida Metal oxide-based biocompatible hybrid sorbent for the extraction and enrichment of catecholamine neurotransmitters and related compounds, and method of synthesis
US11819822B2 (en) * 2019-01-31 2023-11-21 The Governors Of The University Of Alberta Silica composite monolith as a solid phase extraction material
CN114570064A (en) * 2020-11-30 2022-06-03 中国科学院大连化学物理研究所 Superfine inner diameter capillary monolithic column and preparation and application thereof

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US4509964A (en) * 1984-01-04 1985-04-09 The Foxboro Company Fused silica capillary column
US4675300A (en) * 1985-09-18 1987-06-23 The Board Of Trustees Of The Leland Stanford Junior University Laser-excitation fluorescence detection electrokinetic separation
US4966785A (en) * 1989-07-03 1990-10-30 Associated Universities, Inc. Method for making a non-extractable stationary phase of polymer within a capillary column
US5308495A (en) * 1990-01-23 1994-05-03 Yissum, Research Development Company Of The Hebrew University Of Jerusalem Chromatography processes using doped sol gel glasses as chromatographic media
US5691206A (en) * 1990-04-02 1997-11-25 Pawliszyn; Janusz B. Method and device for solid phase microextraction and desorption
US5224972A (en) * 1990-09-11 1993-07-06 Frye Gregory C Coatings with controlled porosity and chemical properties
US5240577A (en) * 1990-11-13 1993-08-31 University Of North Carolina At Chapel Hill Two-dimensional high-performance liquid chromatography/capillary electrophoresis
US5128291A (en) * 1990-12-11 1992-07-07 Wax Michael J Porous titania or zirconia spheres
US5192406A (en) * 1991-01-09 1993-03-09 Supelco Deactivated capillary columns for use in capillary electrophoresis
IT1251937B (en) * 1991-10-17 1995-05-27 Donegani Guido Ist HIGH POROSITY SILICA XEROGELS AND PROCESS FOR THEIR PREPARATION.
US5262052A (en) * 1992-03-09 1993-11-16 Brigham Young University Polysiloxanes containing pendant cyano substituted biphenyls as stationary phases for chromatographic columns
US5624875A (en) * 1993-07-19 1997-04-29 Merck Patent Gesellschaft Mit Beschrankter Haftung Inorganic porous material and process for making same
US5522994A (en) * 1995-02-01 1996-06-04 Cornell Research Foundation, Inc. Single column chromatographic determination of small molecules in mixtures with large molecules
US5637135A (en) * 1995-06-26 1997-06-10 Capillary Technology Corporation Chromatographic stationary phases and adsorbents from hybrid organic-inorganic sol-gels
US5869152A (en) * 1996-03-01 1999-02-09 The Research Foundation Of State University Of New York Silica materials
US6136187A (en) * 1997-12-09 2000-10-24 The Board Of Trustees Of The Leland Stanford Junior University Separation column containing porous matrix and method of packing column
US6613234B2 (en) * 1998-04-06 2003-09-02 Ciphergen Biosystems, Inc. Large pore volume composite mineral oxide beads, their preparation and their applications for adsorption and chromatography
AU765881B2 (en) * 1998-08-21 2003-10-02 University Of South Florida Capillary column and method of making
US6759126B1 (en) * 1998-09-21 2004-07-06 University Of South Florida Solid phase microextraction fiber structure and method of making
US6344242B1 (en) * 1999-09-10 2002-02-05 Mcdonnell Douglas Corporation Sol-gel catalyst for electroless plating
WO2002055986A2 (en) * 2000-10-23 2002-07-18 Univ South Florida Sample preconcentration tubes with sol-gel surface coatings and/or sol-gel monolithic beds
US20060113231A1 (en) * 2000-10-23 2006-06-01 Abdul Malik Sample pre-concentration tubes with sol-gel surface coatings and/or sol-gel monolithic beds
US6998040B2 (en) * 2001-01-24 2006-02-14 University Of South Florida Sol-gel open tubular ODS columns with charged inner surface for capillary electrochromatography
WO2002072225A1 (en) 2001-03-09 2002-09-19 University Of South Florida High efficiency sol-gel gas chromatography column
US20040129141A1 (en) * 2002-03-08 2004-07-08 Abdul Malik High efficiency sol-gel gas chromatography column
WO2002094410A1 (en) 2001-05-18 2002-11-28 University Of South Florida Sol-gel dendron separation and extraction capillary column
US7407568B1 (en) * 2002-11-08 2008-08-05 University Of South Florida Method of using sol-gel coatings for on-line preconcentration of amino acids in capillary electrophoresis
US20050106068A1 (en) * 2003-11-18 2005-05-19 Abdul Malik Sol-gel dendron separation and extraction capillary column
US7622191B2 (en) * 2004-07-19 2009-11-24 University Of South Florida Titania-based coating for capillary microextraction
US20060013981A1 (en) * 2004-07-19 2006-01-19 University Of South Florida Polytetrahydrofuran-Based Coating for Capillary Microextraction

Also Published As

Publication number Publication date
US8597508B2 (en) 2013-12-03
US20120000850A1 (en) 2012-01-05
WO2001058562A1 (en) 2001-08-16
US20030213732A1 (en) 2003-11-20
US7947174B2 (en) 2011-05-24

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