ATE508T1 - PROCESS FOR THE PREPARATION OF ANHYDROUS MAGNESIUM CHLORIDE. - Google Patents
PROCESS FOR THE PREPARATION OF ANHYDROUS MAGNESIUM CHLORIDE.Info
- Publication number
- ATE508T1 ATE508T1 AT79301489T AT79301489T ATE508T1 AT E508 T1 ATE508 T1 AT E508T1 AT 79301489 T AT79301489 T AT 79301489T AT 79301489 T AT79301489 T AT 79301489T AT E508 T1 ATE508 T1 AT E508T1
- Authority
- AT
- Austria
- Prior art keywords
- magnesium chloride
- magnesium carbonate
- packed bed
- anhydrous magnesium
- preparation
- Prior art date
Links
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 title abstract 5
- 238000000034 method Methods 0.000 title abstract 4
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 abstract 5
- 239000001095 magnesium carbonate Substances 0.000 abstract 5
- 229910000021 magnesium carbonate Inorganic materials 0.000 abstract 5
- 235000014380 magnesium carbonate Nutrition 0.000 abstract 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract 1
- 239000001569 carbon dioxide Substances 0.000 abstract 1
- 229910002091 carbon monoxide Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 229910001629 magnesium chloride Inorganic materials 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/26—Magnesium halides
- C01F5/30—Chlorides
- C01F5/32—Preparation of anhydrous magnesium chloride by chlorinating magnesium compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Treating Waste Gases (AREA)
- Treatment Of Water By Oxidation Or Reduction (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Hybrid Cells (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention relates to a process for the preparation of anhydrous magnesium chloride from magnesium carbonate preferably magnesium carbonate ores such as magnesite. The process comprises reacting solid magnesium carbonate pieces preferably screened ore in a packed bed reactor comprising the magnesium carbonate pieces with gaseous chlorine in the presence of carbon monoxide at a temperature above the melting point of magnesium chloride and below 1200°C. The off-gas predominantly carbon dioxide is withdrawn from the above the packed bed and molten anhydrous magnesium chloride is withdrawn from below the packed bed. The invention provides a process having low energy requirements which can be applied industrially on a continuous basis using simple apparatus.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB7831427 | 1978-07-27 | ||
| EP79301489A EP0007803B1 (en) | 1978-07-27 | 1979-07-26 | Process for the preparation of anhydrous magnesium chloride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE508T1 true ATE508T1 (en) | 1982-01-15 |
Family
ID=10498720
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT79301489T ATE508T1 (en) | 1978-07-27 | 1979-07-26 | PROCESS FOR THE PREPARATION OF ANHYDROUS MAGNESIUM CHLORIDE. |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4269816A (en) |
| EP (1) | EP0007803B1 (en) |
| JP (1) | JPS603004B2 (en) |
| AT (1) | ATE508T1 (en) |
| AU (1) | AU522102B2 (en) |
| BR (1) | BR7904815A (en) |
| CA (1) | CA1128288A (en) |
| DE (1) | DE2961687D1 (en) |
| GR (1) | GR66831B (en) |
| NO (1) | NO152041C (en) |
| TR (1) | TR20901A (en) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5928526Y2 (en) * | 1975-10-09 | 1984-08-17 | アルプス電気株式会社 | Tape recorder operating device |
| US4943426A (en) * | 1988-06-20 | 1990-07-24 | Aluminum Company Of America | Method for regulating reaction temperature |
| US4981674A (en) * | 1988-12-13 | 1991-01-01 | Noranda, Inc. | Production of anhydrous magnesium chloride |
| US5565080A (en) * | 1994-05-17 | 1996-10-15 | Noranda Metallurgy Inc. | Preparation of anhydrous magnesium chloride-containing melts from hydrated magnesium chloride |
| RU2334829C1 (en) * | 2006-12-22 | 2008-09-27 | Открытое Акционерное Общество "Корпорация Всмпо-Ависма" | Method of dehydration of chlorine magnesium salts in multichamber furnace of boiling bed |
| RU2363657C2 (en) * | 2007-07-11 | 2009-08-10 | Государственное Учреждение Институт металлургии Уральского отделения Российской Академии Наук (ГУ ИМЕТ УрО РАН) | Method for preparation of anhydrous magnesium chloride |
| KR100929187B1 (en) * | 2007-12-24 | 2009-12-01 | 재단법인 포항산업과학연구원 | Method for preparing magnesium chloride compound using magnesium waste |
| CN102586805B (en) * | 2012-03-29 | 2014-09-17 | 北京科技大学 | Preparation method of metal magnesium by magnesium-containing mineral and equipment adopted by preparation method |
| DE102014202593A1 (en) * | 2014-02-13 | 2015-08-13 | Siemens Aktiengesellschaft | Transformation of metal carbonate into metal chloride |
| DE102014202591A1 (en) | 2014-02-13 | 2015-08-13 | Siemens Aktiengesellschaft | Transformation of metal carbonate into metal chloride |
| JP6355184B1 (en) * | 2018-01-31 | 2018-07-11 | 富田製薬株式会社 | Method for producing purified magnesium salt |
| JP7744018B2 (en) * | 2022-09-08 | 2025-09-25 | 株式会社エスイー | Method for producing anhydrous metal chlorides |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2384479A (en) * | 1945-09-11 | Process fob the production of | ||
| US1331257A (en) * | 1918-08-26 | 1920-02-17 | Heap William | Manufacture of metallic chlorids |
| DE379203C (en) * | 1919-08-06 | 1923-08-17 | Norske Saltverker As De | Process for the production of anhydrous magnesium chloride |
| DE502646C (en) * | 1926-01-16 | 1930-11-05 | I G Farbenindustrie Akt Ges | Process for the preparation of anhydrous magnesium chloride or mixtures consisting of anhydrous magnesium chloride and other salts |
| US1933499A (en) * | 1928-10-04 | 1933-10-31 | Magnesium Dev Corp | Process for producing anhydrous magnesium chloride |
| GB333741A (en) * | 1928-10-04 | 1930-08-21 | Ig Farbenindustrie Ag | Process for the preparation of anhydrous magnesium chloride practically free from oxide |
| DE506276C (en) * | 1928-10-05 | 1930-09-01 | I G Farbenindustrie Akt Ges | Process for the extraction of anhydrous and oxide-free chlorine magnesium from magnesite or rocks containing magnesite |
| US2355367A (en) * | 1941-06-28 | 1944-08-08 | Frank H Wilson | Method of producing anhydrous mgcl2 |
| GB582332A (en) | 1944-01-11 | 1946-11-13 | Magnesium Elektron Ltd | Improvements in or relating to the production of anhydrous magnesium chloride |
| GB582333A (en) * | 1944-01-11 | 1946-11-13 | Magnesium Elektron Ltd | Improvements in or relating to the production of anhydrous magnesium chloride |
| GB582357A (en) * | 1944-09-07 | 1946-11-13 | Magnesium Elektron Ltd | Improvements in or relating to the production of anhydrous magnesium chloride |
| FR928521A (en) * | 1944-09-07 | 1947-12-01 | Magnesium Elektron Ltd | Improvements in the production of anhydrous magnesium chloride |
| US2567419A (en) * | 1948-06-05 | 1951-09-11 | Kermit B Bengtson | Recovery of magnesium from siliceous magnesium minerals |
| US3411880A (en) * | 1965-08-23 | 1968-11-19 | Canadian Patents Dev | Recovery of high purity magnesium oxide and calcium oxide from magnesite and calciteores |
-
1979
- 1979-07-24 CA CA332,417A patent/CA1128288A/en not_active Expired
- 1979-07-24 JP JP54093332A patent/JPS603004B2/en not_active Expired
- 1979-07-26 AT AT79301489T patent/ATE508T1/en not_active IP Right Cessation
- 1979-07-26 BR BR7904815A patent/BR7904815A/en not_active IP Right Cessation
- 1979-07-26 DE DE7979301489T patent/DE2961687D1/en not_active Expired
- 1979-07-26 NO NO792472A patent/NO152041C/en unknown
- 1979-07-26 GR GR59702A patent/GR66831B/el unknown
- 1979-07-26 AU AU49269/79A patent/AU522102B2/en not_active Ceased
- 1979-07-26 EP EP79301489A patent/EP0007803B1/en not_active Expired
- 1979-07-27 TR TR20901A patent/TR20901A/en unknown
- 1979-07-27 US US06/061,416 patent/US4269816A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| GR66831B (en) | 1981-05-04 |
| JPS603004B2 (en) | 1985-01-25 |
| CA1128288A (en) | 1982-07-27 |
| AU522102B2 (en) | 1982-05-13 |
| AU4926979A (en) | 1980-01-31 |
| JPS5520296A (en) | 1980-02-13 |
| DE2961687D1 (en) | 1982-02-18 |
| EP0007803A1 (en) | 1980-02-06 |
| EP0007803B1 (en) | 1981-12-30 |
| BR7904815A (en) | 1980-04-22 |
| NO792472L (en) | 1980-01-29 |
| US4269816A (en) | 1981-05-26 |
| NO152041B (en) | 1985-04-15 |
| NO152041C (en) | 1985-07-24 |
| TR20901A (en) | 1982-12-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| UEP | Publication of translation of european patent specification | ||
| REN | Ceased due to non-payment of the annual fee |