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ATE506118T1 - SEPARABLE AGENT FOR OPTICAL ISOMER - Google Patents

SEPARABLE AGENT FOR OPTICAL ISOMER

Info

Publication number
ATE506118T1
ATE506118T1 AT04728898T AT04728898T ATE506118T1 AT E506118 T1 ATE506118 T1 AT E506118T1 AT 04728898 T AT04728898 T AT 04728898T AT 04728898 T AT04728898 T AT 04728898T AT E506118 T1 ATE506118 T1 AT E506118T1
Authority
AT
Austria
Prior art keywords
derivative
optical isomer
provides
porous carrier
separating agent
Prior art date
Application number
AT04728898T
Other languages
German (de)
Inventor
Yoshio Okamoto
Chiyo Yamamoto
Original Assignee
Daicel Chem
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daicel Chem filed Critical Daicel Chem
Application granted granted Critical
Publication of ATE506118T1 publication Critical patent/ATE506118T1/en

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/282—Porous sorbents
    • B01J20/285—Porous sorbents based on polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242—Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • B01J20/3268—Macromolecular compounds
    • B01J20/3272—Polymers obtained by reactions otherwise than involving only carbon to carbon unsaturated bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/38—Selective adsorption, e.g. chromatography characterised by the separation mechanism involving specific interaction not covered by one or more of groups B01D15/265 and B01D15/30 - B01D15/36, e.g. affinity, ligand exchange or chiral chromatography
    • B01D15/3833—Chiral chromatography
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/291—Gel sorbents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3242—Layers with a functional group, e.g. an affinity material, a ligand, a reactant or a complexing group
    • B01J20/3268—Macromolecular compounds
    • B01J20/328—Polymers on the carrier being further modified
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86

Landscapes

  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

The present invention provides a separating agent for enantiomeric isomers which exhibits high optical resolving power together with solvent resistance. That is, the present invention provides a separating agent for enantiomeric isomers including a polysaccharide derivative such as a carbamate derivative or ester derivative of cellulose or amylose carried on a porous carrier such as silica gel, in which the porous carrier having an epoxy group and part of hydroxyl groups of the polysaccharide derivative are chemically bonded.
AT04728898T 2003-04-24 2004-04-22 SEPARABLE AGENT FOR OPTICAL ISOMER ATE506118T1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2003119326 2003-04-24
PCT/JP2004/005757 WO2004095018A1 (en) 2003-04-24 2004-04-22 Separating agent for optical isomer

Publications (1)

Publication Number Publication Date
ATE506118T1 true ATE506118T1 (en) 2011-05-15

Family

ID=33308098

Family Applications (1)

Application Number Title Priority Date Filing Date
AT04728898T ATE506118T1 (en) 2003-04-24 2004-04-22 SEPARABLE AGENT FOR OPTICAL ISOMER

Country Status (8)

Country Link
US (1) US7772153B2 (en)
EP (1) EP1632286B1 (en)
JP (1) JP4294028B2 (en)
KR (1) KR101011784B1 (en)
CN (1) CN100391593C (en)
AT (1) ATE506118T1 (en)
DE (1) DE602004032335D1 (en)
WO (1) WO2004095018A1 (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006150214A (en) * 2004-11-29 2006-06-15 Daicel Chem Ind Ltd Separation agent for optical isomers and separation column for optical isomers
EP2031388B1 (en) * 2006-05-09 2012-11-14 National University Corporation Nagoya University Filler for optical isomer separation
WO2007129658A1 (en) * 2006-05-09 2007-11-15 National University Corporation Nagoya University Filler for optical isomer separation
WO2007148834A1 (en) * 2006-06-23 2007-12-27 Daicel Chemical Industries, Ltd Method of analyzing optical isomers or method of resolving the same
JP5741858B2 (en) * 2009-08-26 2015-07-01 株式会社ダイセル Separating agent for optical isomers
JP6016631B2 (en) * 2010-06-18 2016-10-26 株式会社ダイセル Separating agent for optical isomers
CN102060995B (en) * 2010-11-19 2012-06-06 中南大学 Method for preparing silica gel supported dithiocarbamate heavy metal chelating resin
EP2522647B1 (en) 2011-05-10 2014-04-30 DSM IP Assets B.V. Process of separating chiral isomers of chroman compounds and their derivatives and precursors
EP2573063A1 (en) 2011-09-23 2013-03-27 DSM IP Assets B.V. Process for preparing chiral quinone
CN104028253B (en) * 2014-06-23 2015-10-28 镇江出入境检验检疫局检验检疫综合技术中心 A kind of gold nano grain-polysaccharide bonded silica gel stationary phase and preparation method thereof
CN106268657A (en) * 2015-05-14 2017-01-04 株式会社大赛璐 Agent for separating optical isomers
WO2023208514A1 (en) 2022-04-28 2023-11-02 F. Hoffmann-La Roche Ag Chiral separation of n-phthaloyl-d/l-glutamic acid

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4539399A (en) 1984-07-27 1985-09-03 Advanced Separation Technologies Inc. Bonded phase material for chromatographic separations
EP0231515B1 (en) 1985-12-27 1990-09-26 Daicel Chemical Industries, Ltd. Utilisation of optically active carboalkylated amino alcohols in optical resolution
JPH0713030B2 (en) 1986-04-02 1995-02-15 エーザイ株式会社 Separation agent for optical isomers
JPH0730122B2 (en) 1986-05-19 1995-04-05 ダイセル化学工業株式会社 Method for producing polysaccharide derivative
JP2535446B2 (en) 1990-11-29 1996-09-18 ナカライテスク株式会社 Method for producing optical resolving agent
US5302633A (en) 1990-11-29 1994-04-12 Nacalai Tesque, Inc. Optical resolution agent and process for the preparation of the same
JP3848377B2 (en) * 1993-05-24 2006-11-22 ダイセル化学工業株式会社 Manufacturing method of separation agent
JP3190206B2 (en) 1993-06-22 2001-07-23 ダイセル化学工業株式会社 Separating agent for optical isomers and method for producing the same
JP2751004B2 (en) 1993-09-22 1998-05-18 ダイセル化学工業株式会社 Novel polysaccharide derivative, its production method and its use
US5679572A (en) 1993-09-22 1997-10-21 Daicel Chemical Industries, Ltd. Separation of chiral compounds on polysaccharide supports
KR100355335B1 (en) * 1994-02-25 2003-04-11 다이세루 가가꾸 고오교 가부시끼가이샤 Process for producing optically active mevalonolactone compound
JP3478595B2 (en) 1994-05-17 2003-12-15 ダイセル化学工業株式会社 Separating agent for optical isomers
JPH11255671A (en) 1998-03-11 1999-09-21 Daicel Chem Ind Ltd Chromatographic separation of optical isomer
JP2002350413A (en) 2001-05-24 2002-12-04 Daicel Chem Ind Ltd Separation column
US6736967B2 (en) * 2001-06-07 2004-05-18 Daicel Chemical Industries, Ltd. Separating agent for enantiomeric isomers
JP2005017268A (en) 2003-05-30 2005-01-20 Daicel Chem Ind Ltd Separation agent for optical isomers, method for producing the same, and separation column for optical isomers

Also Published As

Publication number Publication date
CN1758959A (en) 2006-04-12
KR101011784B1 (en) 2011-02-07
KR20070066815A (en) 2007-06-27
JP4294028B2 (en) 2009-07-08
EP1632286A1 (en) 2006-03-08
WO2004095018A1 (en) 2004-11-04
US7772153B2 (en) 2010-08-10
DE602004032335D1 (en) 2011-06-01
CN100391593C (en) 2008-06-04
JPWO2004095018A1 (en) 2006-07-13
US20060189796A1 (en) 2006-08-24
EP1632286A4 (en) 2007-09-12
EP1632286B1 (en) 2011-04-20

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