AT97104B - Process for the production of tungsten or molybdenum carbide. - Google Patents
Process for the production of tungsten or molybdenum carbide.Info
- Publication number
- AT97104B AT97104B AT97104DA AT97104B AT 97104 B AT97104 B AT 97104B AT 97104D A AT97104D A AT 97104DA AT 97104 B AT97104 B AT 97104B
- Authority
- AT
- Austria
- Prior art keywords
- tungsten
- production
- molybdenum carbide
- molybdenum
- carbon
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C1/00—Making non-ferrous alloys
- C22C1/10—Alloys containing non-metals
- C22C1/1036—Alloys containing non-metals starting from a melt
- C22C1/1068—Making hard metals based on borides, carbides, nitrides, oxides or silicides
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/90—Carbides
- C01B32/914—Carbides of single elements
- C01B32/949—Tungsten or molybdenum carbides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Inorganic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
Description
<Desc/Clms Page number 1>
Verfahren zur Herstellung von Wolfram- oder Molybd nkarbid.
EMI1.1
<Desc/Clms Page number 2>
EMI2.1
vollkommen homogen zusammengesetzter Stücke aus Wolframkarbid und Molybdänkarbids in denkbar wirtschaftlichster und vollkommenster Weise dadurch, dass das mit einem entsprechenden Kohlenstoffzusatz versehene pulverförmige Schmelzgut (Wolfram bzw. Wolframoxyd, Molybdän bzw. Molybdänoxyd) einer durchaus gleichmässigen, konzentrischen Erwärmung unterworfen, und die Erwärmung selbst so hoch getrieben wird, dass ein durch die ganze Masse vollständig gleichmässig temperierter Schmelzfluss erzielt wird.
Das Verfahren selbst wird so ausgeübt, dass das mit den erforderlichen Kohlenstoffmengen vermischte pulverförmige Wolfram bzw. Wolframoxyd, Molybdän bzw. Molybdänoxyd der konzentrischen Wärmeeinwirkung eines Kohlerohrwiderstandsofens ausgesetzt wird, dessen Leistungsfähigkeit bis über
EMI2.2
mässig verteilte Temperatur innerhalb des Ofenraum aufrecht zu erhalten, die zur Verflüssigung des Wolframs ausreicht.
Zu diesem Zweck wird ein elektrischer Ofen verwendet, der in seiner Anordnung dem an sich bekannten Kohlerohrwiderstandsofen entspricht, jedoch an Stelle von Metallklemmen mit solchen aus Kohlenstoff versehen ist. Es hat sich herausgestellt, dass erst durch die Verwendung dieser Klemmen aus Kohlenstoff die praktische Lösung der vorliegenden Aufgabe in wirtschaftlicher und einwandfreier Weise möglich wird.
<Desc / Clms Page number 1>
Process for the production of tungsten or molybdenum carbide.
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<Desc / Clms Page number 2>
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perfectly homogeneous pieces of tungsten carbide and molybdenum carbide in the most economical and perfect way imaginable, in that the powdered melt material (tungsten or tungsten oxide, molybdenum or molybdenum oxide) is subjected to a thoroughly uniform, concentric heating, and the heating itself is so high is driven so that a melt flow that is completely uniformly tempered through the entire mass is achieved.
The process itself is carried out in such a way that the powdery tungsten or tungsten oxide, molybdenum or molybdenum oxide mixed with the required amounts of carbon is exposed to the concentric heat effects of a carbon tube resistance furnace, the efficiency of which is up to over
EMI2.2
Maintain a moderately distributed temperature within the furnace chamber that is sufficient to liquefy the tungsten.
For this purpose, an electric furnace is used, the arrangement of which corresponds to the carbon tube resistance furnace known per se, but is provided with carbon clamps instead of metal clamps. It has been found that only through the use of these clamps made of carbon is the practical solution of the present problem possible in an economical and flawless manner.
Claims (1)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE533062X | 1914-04-16 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AT97104B true AT97104B (en) | 1924-06-10 |
Family
ID=6555829
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT97104D AT97104B (en) | 1914-04-16 | 1920-10-30 | Process for the production of tungsten or molybdenum carbide. |
Country Status (4)
| Country | Link |
|---|---|
| AT (1) | AT97104B (en) |
| CH (1) | CH88775A (en) |
| FR (1) | FR533062A (en) |
| GB (1) | GB157750A (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110422846B (en) * | 2019-08-13 | 2022-06-07 | 哈尔滨工业大学 | Synthesis method of molybdenum carbide nano material |
-
1919
- 1919-12-23 CH CH88775D patent/CH88775A/en unknown
-
1920
- 1920-10-30 AT AT97104D patent/AT97104B/en active
-
1921
- 1921-01-10 GB GB1453/21A patent/GB157750A/en not_active Expired
- 1921-03-30 FR FR533062D patent/FR533062A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| FR533062A (en) | 1922-02-18 |
| CH88775A (en) | 1921-03-16 |
| GB157750A (en) | 1922-05-10 |
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