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NZ740037B2 - New effective aminoglycoside antibiotic for multidrug-resistant bacteria - Google Patents

New effective aminoglycoside antibiotic for multidrug-resistant bacteria Download PDF

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Publication number
NZ740037B2
NZ740037B2 NZ740037A NZ74003716A NZ740037B2 NZ 740037 B2 NZ740037 B2 NZ 740037B2 NZ 740037 A NZ740037 A NZ 740037A NZ 74003716 A NZ74003716 A NZ 74003716A NZ 740037 B2 NZ740037 B2 NZ 740037B2
Authority
NZ
New Zealand
Prior art keywords
group
hydrogen atom
amino
hydroxyl
solvate
Prior art date
Application number
NZ740037A
Other versions
NZ740037A (en
Inventor
Takashi Ida
Masayuki Igarashi
Yoshiaki Takahashi
Eijiro Umemura
Original Assignee
Meiji Seika Pharma Co Ltd
Microbial Chemistry Research Foundation
Filing date
Publication date
Application filed by Meiji Seika Pharma Co Ltd, Microbial Chemistry Research Foundation filed Critical Meiji Seika Pharma Co Ltd
Priority claimed from PCT/JP2016/072400 external-priority patent/WO2017018528A1/en
Publication of NZ740037A publication Critical patent/NZ740037A/en
Publication of NZ740037B2 publication Critical patent/NZ740037B2/en

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/70Carbohydrates; Sugars; Derivatives thereof
    • A61K31/7028Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages
    • A61K31/7034Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages attached to a carbocyclic compound, e.g. phloridzin
    • A61K31/7036Compounds having saccharide radicals attached to non-saccharide compounds by glycosidic linkages attached to a carbocyclic compound, e.g. phloridzin having at least one amino group directly attached to the carbocyclic ring, e.g. streptomycin, gentamycin, amikacin, validamycin, fortimicins
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/04Antibacterial agents
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/02Acyclic radicals, not substituted by cyclic structures
    • C07H15/12Acyclic radicals, not substituted by cyclic structures attached to a nitrogen atom of the saccharide radical
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20Carbocyclic rings
    • C07H15/22Cyclohexane rings, substituted by nitrogen atoms
    • C07H15/222Cyclohexane rings substituted by at least two nitrogen atoms
    • C07H15/224Cyclohexane rings substituted by at least two nitrogen atoms with only one saccharide radical directly attached to the cyclohexyl radical, e.g. destomycin, fortimicin, neamine
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20Carbocyclic rings
    • C07H15/22Cyclohexane rings, substituted by nitrogen atoms
    • C07H15/222Cyclohexane rings substituted by at least two nitrogen atoms
    • C07H15/226Cyclohexane rings substituted by at least two nitrogen atoms with at least two saccharide radicals directly attached to the cyclohexane rings
    • C07H15/234Cyclohexane rings substituted by at least two nitrogen atoms with at least two saccharide radicals directly attached to the cyclohexane rings attached to non-adjacent ring carbon atoms of the cyclohexane rings, e.g. kanamycins, tobramycin, nebramycin, gentamicin A2
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

Disclosed are: a compound represented by general formula (I), or a pharmaceutically acceptable salt of the compound, or a solvate of the compound or the pharmaceutically acceptable salt; a pharmaceutical composition containing the compound, the pharmaceutically acceptable salt or the solvate; a use of the compound, the pharmaceutically acceptable salt or the solvate for the prevention or treatment of infectious diseases; and a method for preventing or treating infectious diseases using the compound, the pharmaceutically acceptable salt or the solvate. The compound represented by general formula (I) has an antibacterial activity against both gram-positive bacteria and gram-negative bacteria, and is therefore useful for the prevention or treatment of infectious diseases induced by these bacteria.

Claims (14)

1. A compound represented by a general formula (I) or a pharmaceutically acceptable salt or solvate thereof: [Chem. 1] 5 (I) wherein, R is a hydrogen atom or a hydroxyl group, R is a hydrogen atom or an amino group, R is a hydrogen atom, a halogen atom, a hydroxyl group or an amino 10 group, R is a hydrogen atom, a halogen atom or an amino group, wherein R and R may form a double bond together, R is a hydrogen atom, a hydroxyl group or an amino group, R is a hydrogen atom, a hydroxyl group or an amino group, 15 R is a hydrogen atom, a hydroxyl group or an amino group, R is a hydrogen atom, a hydroxyl group or an amino group, R and R are each independently a hydrogen atom, a C alkyl group, an amino-C alkyl group, a guanidino-C alkyl group, an 1-6 1-6 amino-C cycloalkyl group, an amino-C cycloalkyl-C alkyl group, 3-7 3-7 1-6 20 an amidino group, an azetidino group optionally substituted with a C alkyl group, a glycyl group, a sarcosyl group, an L- alanyl group, a D-alanyl group, an L-seryl group, a D-seryl group, a ß-alanyl group, an L-isoseryl group or a D-isoseryl group; and R is a hydrogen atom, a hydroxyl group or a fluorine atom, 25 except when 5 8 11 1 2 3 4 6 7 9 (i) R , R , and R are hydroxyl groups, R , R , R , R , R , R , R , and R are hydrogen atoms, 1 5 8 11 2 3 4 6 7 9 (ii) R , R , R , and R are hydroxyl groups, R , R , R , R , R , R , and R are hydrogen atoms, 5 8 11 2 3 6 7 9 10 30 (iii) R , R and R are hydroxyl groups, R , R , R , R , R and R are hydrogen atoms, R and R form a double bond together.
2. The compound according to Claim 1 represented by formula (I-1) or a pharmaceutically acceptable salt or solvate thereof: [Chem. 2] (I-1) 5 wherein, R is a hydrogen atom or a hydroxyl group, R is a hydrogen atom or an amino group, R is a hydrogen atom, a halogen atom, a hydroxyl group or an amino group, 10 R is a hydrogen atom, a halogen atom or an amino group, wherein R and R may form a double bond together, R is a hydrogen atom, a hydroxyl group or an amino group, R is a hydrogen atom, a hydroxyl group or an amino group, R is a hydrogen atom, a hydroxyl group or an amino group, 15 R is a hydrogen atom, a hydroxyl group or an amino group; and R is a hydrogen atom, a hydroxyl group or a fluorine atom, except when 5 8 11 1 2 3 4 6 7 (i) R , R , and R are hydroxyl groups, R , R , R , R , R , and R are hydrogen atoms, 1 5 8 11 2 3 4 6 7 20 (ii) R , R , R , and R are hydroxyl groups, R , R , R , R , and R are hydrogen atoms, 5 8 11 2 3 6 7 (iii) R , R and R are hydroxyl groups, R , R , R and R are hydrogen atoms, R and R form a double bond together.
3. The compound according to Claim 1 represented by a general 25 formula (I-2) or a pharmaceutically acceptable salt or solvate thereof: [Chem. 3] (I-2) wherein, R is a hydrogen atom or a hydroxyl group, R is a hydrogen atom or an amino group, 5 R is a hydrogen atom, a halogen atom, a hydroxyl group or an amino group, R is a hydrogen atom, a halogen atom or an amino group, wherein R and R may form a double bond together, R is a hydrogen atom, a hydroxyl group or an amino group, 10 R is a hydrogen atom, a hydroxyl group or an amino group, R is a hydrogen atom, a C alkyl group or an amino-C alkyl 1-6 1-6 group, R is a C alkyl group, an amino-C alkyl group, a guanidino-C 1-6 1-6 1-6 alkyl group, an amino-C cycloalkyl group, an amino-C 3-7 3-7 15 cycloalkyl-C alkyl group, an amidino group, an azetidino group optionally substituted with a C alkyl group, a glycyl group, a sarcosyl group, an L- alanyl group, a D-alanyl group, an L-seryl group, a D-seryl group, a ß-alanyl group, an L-isoseryl group or a D-isoseryl group; and 20 R is a hydrogen atom or a hydroxyl group.
4. The compound according to Claim 1 represented by a general formula (I-4) or a pharmaceutically acceptable salt or solvate thereof: [Chem. 5] 25 (I-4) wherein, R is a hydrogen atom or a hydroxyl group, R is a hydrogen atom or an amino group, R is a hydrogen atom, a halogen atom, a hydroxyl group or an amino group, 5 R is a hydrogen atom, a halogen atom or an amino group; and wherein R and R may form a double bond together, except when 1 2 3 4 (i) R , R , R , and R are hydrogen atoms, 1 2 3 4 (ii) R is a hydroxyl group, and R , R , and R are hydrogen atoms, 2 3 1 4 10 (iii) R and R are hydrogen atoms, R and R form a double bond together.
5. A compound according to claim 1 or a pharmaceutically acceptable salt or solvate thereof, wherein the compound is: 5-epiapramycin, 15 5-deoxyepifluoroapramycin, 6-deoxyepiapramycin, 5,6-dideoxyfluoroapramycin, 5-aminodeoxyepiapramycin, 5-aminodeoxyapramycin, 20 6-amino-5,6-dideoxy-5,6-diepifluoroapramycin, 5-amino-5,6-dideoxyapramycin, 5,6"-dideoxyapramycin, 5,3"-dideoxyapramycin, 3"-deoxyepiapramycin, 25 5,3"-dideoxyepifluoroapramycin, 6,3"-dideoxyepiapramycin, 5,6,3"-trideoxyapramycin, 5-amino-5,3"-dideoxyepiapramycin, 5,2"-dideoxy-5,3"-diepifluoroapramycin, 30 5,3"-diepiapramycin, 6,6"-dideoxyepiapramycin, 5-eno-5,6,6"-trideoxyapramycin, 5,6,6"-trideoxyapramycin, 5-deoxy-4"-N-methylapramycin, 35 4"-N-(2-aminoethyl)deoxyapramycin, 4"-N-(3-aminopropyl)deoxyapramycin, 5-deoxy-4"-N-(1,3-diaminopropanyl)apramycin, 4"-deaminodeoxy-4"-guanidinoapramycin, 5-epi-4"-N-methylapramycin, 4"-N-(2-aminoethyl)epiapramycin, 5 4"-N-(3-aminopropyl)epiapramycin, 4"-N-(1,3-diaminopropanyl)epiapramycin, 4"-deaminoepi-4"-guanidinoapramycin, 4"-deaminodeoxyepifluoro-4"-guanidinoapramycin, 5,6-dideoxy-4"-N-methylapramycin, 10 4"-N-(2-aminoethyl)-5,6-dideoxyapramycin, 4"-N-(3-aminopropyl)-5,6-dideoxyapramycin, 4"-N-(1,3-diaminopropanyl)-5,6-dideoxyapramycin, 4"-deamino-5,6-dideoxy-4"-guanidinoapramycin, 6-deoxyepi-4"-N-methylapramycin, 15 4"-N-(2-aminoethyl)deoxyepiapramycin, 4"-N-(3-aminopropyl)deoxyepiapramycin, 4"-deaminodeoxyepi-4"-guanidinoapramycin, 4"-N-(1,3-diaminopropanyl)-5,6"-dideoxyapramycin, 4"-deamino-5,6"-dideoxy-4"-guanidinoapramycin, 20 4"-deamino-5,3"-dideoxy-4"-guanidinoapramycin, 5-epi-4"-N-glycylapramycin, 5-epi-4"-N-sarcosylapramycin, 4"-N-(L-alanyl)epiapramycin, 5-epi-4"-N-(L-seryl)apramycin, 25 4"-N-(ß-alanyl)epiapramycin, 5-epi-4"-N-(L-isoseryl)apramycin, 5-epi-4"-N-(D-isoseryl)apramycin, 6-deoxyepi-4"-N-glycylapramycin, 6-deoxyepi-4"-N-sarcosylapramycin, 30 4"-N-(ß-alanyl)deoxyepiapramycin, 6-deoxyepi-4"-N-(L-isoseryl)apramycin, 5-amino-4"-deaminodeoxyepi-4"-guanidinoapramycin, 5-aminodeoxyepi-4"-N-glycylapramycin, 5-aminodeoxyepi-4"-N-(L-isoseryl)apramycin, 35 4"-deamino-3"-deoxyepi-4"-guanidinoapramycin, 4"-deamino-5,3"-dideoxyepifluoro-4"-guanidinoapramycin 2"-deoxy-5,3"-diepiapramycin.
6. A pharmaceutical composition comprising the compound according to any one of Claims 1 to 5 or a pharmaceutically 5 acceptable salt or solvate thereof.
7. The pharmaceutical composition according to Claim 6 for use in the prevention or treatment of infectious disease.
8. The pharmaceutical composition according to Claim 7, wherein the infectious disease is sepsis, infectious endocarditis, dermatological 10 infections, surgical site infections, orthopedic surgical site infections, respiratory infections, urinary tract infections, enteral infections, peritonitis, meningitis, ophthalmological infections or otolaryngological infections.
9. The pharmaceutical composition according to any one of Claims 7 15 or 8, wherein the infectious disease is caused by methicillin-resistant Staphylococcus aureus (MRSA), Staphylococcus aureus, Escherichia coli, Klebsiella pneumoniae or Pseudomonas aeruginosa.
10. The compound according to any one of Claims 1 to 5 or a pharmaceutically acceptable salt or solvate thereof for use in 20 therapy.
11. The compound according to any one of Claims 1 to 5 or a pharmaceutically acceptable salt or solvate thereof for use in the prevention or treatment of infectious disease.
12. Use of the compound according to any one of Claims 1 to 5 or a 25 pharmaceutically acceptable salt or solvate thereof in the manufacture of a medicament for the prevention or treatment of infectious disease.
13. An antimicrobial agent comprising the compound of any one of Claims 1 to 5 or a pharmaceutically acceptable salt or solvate thereof. 30
14. The compound according to claim 1, substantially as herein described with reference to any one of the Examples thereof.
NZ740037A 2016-07-29 New effective aminoglycoside antibiotic for multidrug-resistant bacteria NZ740037B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2015151250 2015-07-30
PCT/JP2016/072400 WO2017018528A1 (en) 2015-07-30 2016-07-29 Novel aminoglycoside antibiotic effective against multidrug-resistant bacteria

Publications (2)

Publication Number Publication Date
NZ740037A NZ740037A (en) 2024-08-30
NZ740037B2 true NZ740037B2 (en) 2024-12-03

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