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NO20075092L - Process for producing Ti or Ti alloys, and process for winding electrolysis application for the process - Google Patents

Process for producing Ti or Ti alloys, and process for winding electrolysis application for the process

Info

Publication number
NO20075092L
NO20075092L NO20075092A NO20075092A NO20075092L NO 20075092 L NO20075092 L NO 20075092L NO 20075092 A NO20075092 A NO 20075092A NO 20075092 A NO20075092 A NO 20075092A NO 20075092 L NO20075092 L NO 20075092L
Authority
NO
Norway
Prior art keywords
electrolytic bath
alloy
solid
reduction
reduction process
Prior art date
Application number
NO20075092A
Other languages
Norwegian (no)
Inventor
Tadashi Ogasawara
Makoto Yamaguchi
Masahiko Hori
Kazuo Takemura
Original Assignee
Osaka Titanium Technology Co L
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP2005094205A external-priority patent/JP2006274340A/en
Priority claimed from JP2005096690A external-priority patent/JP4227113B2/en
Application filed by Osaka Titanium Technology Co L filed Critical Osaka Titanium Technology Co L
Publication of NO20075092L publication Critical patent/NO20075092L/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/26Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium
    • C25C3/28Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium of titanium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/1263Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
    • C22B34/1268Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00Obtaining refractory metals
    • C22B34/10Obtaining titanium, zirconium or hafnium
    • C22B34/12Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
    • C22B34/129Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B5/00General methods of reducing to metals
    • C22B5/02Dry methods smelting of sulfides or formation of mattes
    • C22B5/04Dry methods smelting of sulfides or formation of mattes by aluminium, other metals or silicon
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/02Electrolytic production, recovery or refining of metals by electrolysis of melts of alkali or alkaline earth metals
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C3/00Electrolytic production, recovery or refining of metals by electrolysis of melts
    • C25C3/26Electrolytic production, recovery or refining of metals by electrolysis of melts of titanium, zirconium, hafnium, tantalum or vanadium
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C5/00Electrolytic production, recovery or refining of metal powders or porous metal masses
    • C25C5/04Electrolytic production, recovery or refining of metal powders or porous metal masses from melts
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25CPROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
    • C25C7/00Constructional parts, or assemblies thereof, of cells; Servicing or operating of cells

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Electrolytic Production Of Metals (AREA)

Abstract

Ved fremstilling av Ti eller en Ti-legering gjennom reduksjon med Ca blir et elektrolyttisk badsalt tatt ut fra en reduksjonsprosess elektrolysert for å utvinne Ca og det elektrolyttiske badsaltet som en fast substans, og utvunnet Ca og elektrolyttisk badsalt leveres til reduksjonsprosessen. Derfor blir varmegenerering undertrykt i reduksjonsprosessen ved anvendelse av latent fusjonsvarme frembrakt av den faste substansen som derved i stor grad forbedrer fremstillingseffektiviteten og den termiske effektiviteten. Ytterligere er reaksjonstemperaturen enkel å kontrollere, og råmaterialtilsetningshastigheten kan økes for effektivt å fremstille Ti eller Ti-legering. Således, ved anvendelse av en opptrekkelektrolysemetode ifølge oppfinnelsen kan faststoff-Ca og elektrolyttisk badsalt oppnås ved lav spenning og høy strømeffektivitet, dvs. med relativt lav kraftkonsumpsjon. Når faststoff-Ca og elektrolyttisk badsalt anvendes som en Ca-kilde ved fremstilling av Ti eller Ti-legering gjennom reduksjon med Ca kan Ti eller Ti-legering effektivt produseres.In the preparation of Ti or a Ti alloy by reduction with Ca, an electrolytic bath salt is taken out of a reduction process to be electrolysed to recover Ca and the electrolytic bath salt as a solid, and recovered Ca and electrolytic bath salt are delivered to the reduction process. Therefore, heat generation is suppressed in the reduction process by using latent fusion heat generated by the solid which thereby greatly improves the manufacturing efficiency and the thermal efficiency. Further, the reaction temperature is easy to control, and the raw material addition rate can be increased to efficiently prepare Ti or Ti alloy. Thus, by using a pull-up electrolysis method according to the invention, solid-Ca and electrolytic bath salts can be obtained at low voltage and high current efficiency, i.e. with relatively low power consumption. When solid Ca and electrolytic bath salts are used as a Ca source in the preparation of Ti or Ti alloy through reduction with Ca, Ti or Ti alloy can be effectively produced.

NO20075092A 2005-03-29 2007-10-09 Process for producing Ti or Ti alloys, and process for winding electrolysis application for the process NO20075092L (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2005094205A JP2006274340A (en) 2005-03-29 2005-03-29 METHOD FOR PRODUCING Ti OR Ti ALLOY
JP2005096690A JP4227113B2 (en) 2005-03-30 2005-03-30 Pull-up electrolysis method
PCT/JP2006/305227 WO2006103944A1 (en) 2005-03-29 2006-03-16 PROCESS FOR PRODUCING Ti OR Ti ALLOY, AND PULL-UP ELECTROLYSIS METHOD APPLICABLE TO SAID PROCESS

Publications (1)

Publication Number Publication Date
NO20075092L true NO20075092L (en) 2007-12-19

Family

ID=37053205

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20075092A NO20075092L (en) 2005-03-29 2007-10-09 Process for producing Ti or Ti alloys, and process for winding electrolysis application for the process

Country Status (7)

Country Link
US (1) US20090101517A1 (en)
EP (1) EP1876248A1 (en)
AU (1) AU2006229128A1 (en)
CA (1) CA2602801A1 (en)
EA (1) EA200702096A1 (en)
NO (1) NO20075092L (en)
WO (1) WO2006103944A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR076863A1 (en) 2009-05-12 2011-07-13 Metalysis Ltd APPARATUS AND METHOD FOR REDUCTION OF SOLID RAW MATERIAL.
MY180279A (en) 2010-11-18 2020-11-26 Metalysis Ltd Electrolysis apparatus

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2205854A (en) * 1937-07-10 1940-06-25 Kroll Wilhelm Method for manufacturing titanium and alloys thereof
US2845386A (en) * 1954-03-16 1958-07-29 Du Pont Production of metals
GB2111531A (en) * 1981-07-11 1983-07-06 Toho Titanium Co Ltd Method for manufacturing titanium metal
JPS6447823A (en) * 1987-08-17 1989-02-22 Toho Titanium Co Ltd Production of metallic titanium
JP2002129250A (en) * 2000-10-30 2002-05-09 Katsutoshi Ono Method for producing metallic titanium
JP4198434B2 (en) * 2002-10-09 2008-12-17 勝敏 小野 Method for smelting titanium metal
JP4193985B2 (en) * 2003-08-28 2008-12-10 株式会社大阪チタニウムテクノロジーズ Metal production method and apparatus by Ca reduction
JP4193984B2 (en) * 2003-08-28 2008-12-10 株式会社大阪チタニウムテクノロジーズ Metal manufacturing equipment
JP4975244B2 (en) * 2004-08-20 2012-07-11 東邦チタニウム株式会社 Method and apparatus for producing metal by molten salt electrolysis

Also Published As

Publication number Publication date
US20090101517A1 (en) 2009-04-23
EP1876248A1 (en) 2008-01-09
AU2006229128A1 (en) 2006-10-05
EA200702096A1 (en) 2008-04-28
WO2006103944A1 (en) 2006-10-05
CA2602801A1 (en) 2006-10-05

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