NO20006219L - Fremgangsmåte for fremstilling av alkoksyaminer fra nitroksyder - Google Patents
Fremgangsmåte for fremstilling av alkoksyaminer fra nitroksyderInfo
- Publication number
- NO20006219L NO20006219L NO20006219A NO20006219A NO20006219L NO 20006219 L NO20006219 L NO 20006219L NO 20006219 A NO20006219 A NO 20006219A NO 20006219 A NO20006219 A NO 20006219A NO 20006219 L NO20006219 L NO 20006219L
- Authority
- NO
- Norway
- Prior art keywords
- alkoxyamines
- preparation
- nitroxide
- nitroxides
- organic solvent
- Prior art date
Links
- 125000005262 alkoxyamine group Chemical group 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- -1 nitroxides Chemical class 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical class ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- 239000012074 organic phase Substances 0.000 abstract 2
- 239000003960 organic solvent Substances 0.000 abstract 2
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 239000003446 ligand Substances 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C239/00—Compounds containing nitrogen-to-halogen bonds; Hydroxylamino compounds or ethers or esters thereof
- C07C239/08—Hydroxylamino compounds or their ethers or esters
- C07C239/20—Hydroxylamino compounds or their ethers or esters having oxygen atoms of hydroxylamino groups etherified
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/22—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms with hetero atoms directly attached to ring nitrogen atoms
- C07D295/24—Oxygen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/40—Esters thereof
- C07F9/4003—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
- C07F9/4006—Esters of acyclic acids which can have further substituents on alkyl
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Hydrogenated Pyridines (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
FFremgangsmåte for fremstilling av alkoksyaminer omfattende blanding, i et organisk oppløsningsmiddel, av et metallsalt, en metall-ligand, en halogenkarbonforbindelse ZX og et nitroksyd idet reaksjonsmediet holdes omrørt ved en temperatur mellom 20°C og 90°C, inntil nitroksydet blir borte, gjenvinning av den organiske fase, vasking av den organiske fase med vann og derefter isolering av alkoksyaminet ved fordamping av det organiske oppløsningsmiddel under redusert trykk.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9904405A FR2791979B1 (fr) | 1999-04-08 | 1999-04-08 | Procede de preparation d'alcoxyamines a partir de nitroxydes |
| PCT/FR2000/000750 WO2000061544A1 (fr) | 1999-04-08 | 2000-03-24 | Procede de preparation d'alcoxyamines a partir de nitroxydes |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO20006219D0 NO20006219D0 (no) | 2000-12-07 |
| NO20006219L true NO20006219L (no) | 2001-01-29 |
Family
ID=9544180
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20006219A NO20006219L (no) | 1999-04-08 | 2000-12-07 | Fremgangsmåte for fremstilling av alkoksyaminer fra nitroksyder |
Country Status (21)
| Country | Link |
|---|---|
| US (1) | US6495720B1 (no) |
| EP (1) | EP1086073B1 (no) |
| JP (1) | JP4705248B2 (no) |
| KR (1) | KR100698002B1 (no) |
| CN (1) | CN1298699C (no) |
| AT (1) | ATE234275T1 (no) |
| AU (1) | AU3564700A (no) |
| BG (1) | BG105035A (no) |
| BR (1) | BR0006023A (no) |
| CA (1) | CA2334845A1 (no) |
| DE (1) | DE60001611T2 (no) |
| DK (1) | DK1086073T3 (no) |
| ES (1) | ES2193946T3 (no) |
| FR (1) | FR2791979B1 (no) |
| HU (1) | HUP0103835A3 (no) |
| IL (1) | IL140166A0 (no) |
| MX (1) | MXPA00012135A (no) |
| NO (1) | NO20006219L (no) |
| PL (1) | PL344693A1 (no) |
| SK (1) | SK18672000A3 (no) |
| WO (1) | WO2000061544A1 (no) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2807439B1 (fr) | 2000-04-07 | 2003-06-13 | Atofina | Polymeres multimodaux par polymerisation radicalaire controlee en presence d'alcoxyamines |
| FR2812639B1 (fr) * | 2000-08-04 | 2002-09-27 | Atofina | Procede de preparation d'alcoxyamines a partir de nitroxydes |
| US20030045461A1 (en) * | 2001-09-06 | 2003-03-06 | Jen-Chang Hsia | Composition and methods of esterified nitroxides gated with carboxylic acids |
| EP1375457A1 (en) | 2002-06-25 | 2004-01-02 | Bayer Aktiengesellschaft | One-pot process for the preparation of functionalized alkoxyamines |
| EP1375476A1 (en) * | 2002-06-25 | 2004-01-02 | Bayer Aktiengesellschaft | A new process for the synthesis of alkoxyamines active in controlled radical polymerization |
| FR2843393B1 (fr) * | 2002-08-07 | 2005-12-30 | Atofina | Alcoxyamines issues de nitroxydes b-phosphore, leur utilisation en polymerisation radicalaire |
| FR2843394B1 (fr) * | 2002-08-07 | 2005-12-30 | Atofina | Alcoxyamines issues de nitroxydes b-phosphore, leur utilisation en polymerisation radicalaire |
| CN100558755C (zh) * | 2002-09-23 | 2009-11-11 | 西巴特殊化学品控股有限公司 | 通过原子转换自由基加成反应(atra)制备的聚合烷氧基胺 |
| FR2852963A1 (fr) * | 2003-03-26 | 2004-10-01 | Atofina | Nouveau procede de synthese/fabrication de films acryliques |
| WO2007078819A2 (en) * | 2005-12-16 | 2007-07-12 | Arkema Inc. | Low surface energy block co-polymer preparation methods and applications |
| US7498398B2 (en) * | 2006-03-21 | 2009-03-03 | Sabic Innovative Plastics Ip B.V. | Thermoplastic composition, method of making, and articles formed therefrom |
| EP2013240B1 (en) * | 2006-04-07 | 2017-05-31 | Piotrek Co., Ltd. | Process for the preparation of crosslinked nitroxide polymers |
| FR2918668B1 (fr) * | 2007-07-09 | 2009-08-21 | Arkema France | Procede ameliore de preparation d'alcoxyamines issues de nitroxydes beta-phosphores. |
| CN103073545B (zh) * | 2013-01-21 | 2015-04-15 | 清华大学 | N-(2-苯酚基)-β-咔啉和N-(5-溴-2-苯酚基)-β-咔啉的合成方法 |
| FR3030526B1 (fr) | 2014-12-18 | 2018-06-15 | Arkema France | Polymerisation radicalaire d'alcoxyamines a basse temperature |
| US10131735B2 (en) | 2014-12-18 | 2018-11-20 | Arkema France | Low-temperature radical polymerisation of alkoxyamines |
| FR3030525B1 (fr) * | 2014-12-18 | 2018-05-11 | Arkema France | Polymerisation radicalaire d'alcoxyamines a basse temperature |
| FR3075212B1 (fr) | 2017-12-18 | 2020-11-20 | Arkema France | Composition de polymere (meth)acrylique, son procede de preparation et utilisation |
| FR3075211B1 (fr) | 2017-12-18 | 2020-11-20 | Arkema France | Composition de polymere (meth)acrylique, son procede de preparation et utilisation |
| CN108218740A (zh) * | 2017-12-22 | 2018-06-29 | 中山市小榄企业服务有限公司 | 一种n-烷氧基胺的合成方法 |
| FR3086294A1 (fr) | 2018-09-25 | 2020-03-27 | Arkema France | Composition polymere pour vehicules nautiques, son utilisation et vehicule nautique comprenant celui-ci |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0157738B1 (de) * | 1984-03-22 | 1989-04-19 | Ciba-Geigy Ag | Verfahren zur Herstellung von Nitroxylen sterisch gehinderter Amine |
| US5077329A (en) * | 1990-04-06 | 1991-12-31 | Ciba-Geigy Corporation | Hydroxyaminomethylphosphonates and stabilized compositions |
| TW593347B (en) * | 1997-03-11 | 2004-06-21 | Univ Carnegie Mellon | Improvements in atom or group transfer radical polymerization |
-
1999
- 1999-04-08 FR FR9904405A patent/FR2791979B1/fr not_active Expired - Fee Related
-
2000
- 2000-03-24 AT AT00914251T patent/ATE234275T1/de not_active IP Right Cessation
- 2000-03-24 MX MXPA00012135A patent/MXPA00012135A/es active IP Right Grant
- 2000-03-24 AU AU35647/00A patent/AU3564700A/en not_active Abandoned
- 2000-03-24 PL PL00344693A patent/PL344693A1/xx unknown
- 2000-03-24 IL IL14016600A patent/IL140166A0/xx unknown
- 2000-03-24 CN CNB008010420A patent/CN1298699C/zh not_active Expired - Fee Related
- 2000-03-24 ES ES00914251T patent/ES2193946T3/es not_active Expired - Lifetime
- 2000-03-24 HU HU0103835A patent/HUP0103835A3/hu unknown
- 2000-03-24 CA CA002334845A patent/CA2334845A1/fr not_active Abandoned
- 2000-03-24 WO PCT/FR2000/000750 patent/WO2000061544A1/fr not_active Ceased
- 2000-03-24 DK DK00914251T patent/DK1086073T3/da active
- 2000-03-24 US US09/719,042 patent/US6495720B1/en not_active Expired - Fee Related
- 2000-03-24 EP EP00914251A patent/EP1086073B1/fr not_active Expired - Lifetime
- 2000-03-24 SK SK1867-2000A patent/SK18672000A3/sk unknown
- 2000-03-24 KR KR1020007013918A patent/KR100698002B1/ko not_active Expired - Fee Related
- 2000-03-24 DE DE60001611T patent/DE60001611T2/de not_active Expired - Lifetime
- 2000-03-24 JP JP2000610821A patent/JP4705248B2/ja not_active Expired - Fee Related
- 2000-03-24 BR BR0006023-2A patent/BR0006023A/pt not_active Application Discontinuation
- 2000-12-07 NO NO20006219A patent/NO20006219L/no not_active Application Discontinuation
- 2000-12-08 BG BG105035A patent/BG105035A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| HUP0103835A2 (hu) | 2002-01-28 |
| JP4705248B2 (ja) | 2011-06-22 |
| CN1298699C (zh) | 2007-02-07 |
| DK1086073T3 (da) | 2003-07-14 |
| WO2000061544A1 (fr) | 2000-10-19 |
| HUP0103835A3 (en) | 2002-04-29 |
| MXPA00012135A (es) | 2003-05-19 |
| ES2193946T3 (es) | 2003-11-16 |
| CN1313847A (zh) | 2001-09-19 |
| EP1086073A1 (fr) | 2001-03-28 |
| KR20010072588A (ko) | 2001-07-31 |
| DE60001611T2 (de) | 2003-12-04 |
| FR2791979A1 (fr) | 2000-10-13 |
| JP2002541239A (ja) | 2002-12-03 |
| NO20006219D0 (no) | 2000-12-07 |
| PL344693A1 (en) | 2001-11-19 |
| IL140166A0 (en) | 2002-02-10 |
| US6495720B1 (en) | 2002-12-17 |
| CA2334845A1 (fr) | 2000-10-19 |
| DE60001611D1 (de) | 2003-04-17 |
| FR2791979B1 (fr) | 2003-05-16 |
| BG105035A (en) | 2001-07-31 |
| EP1086073B1 (fr) | 2003-03-12 |
| AU3564700A (en) | 2000-11-14 |
| ATE234275T1 (de) | 2003-03-15 |
| SK18672000A3 (sk) | 2001-08-06 |
| BR0006023A (pt) | 2001-03-13 |
| KR100698002B1 (ko) | 2007-03-23 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FC2A | Withdrawal, rejection or dismissal of laid open patent application |