MY184018A - Continuous process for dry fractionation of glyceride oils - Google Patents
Continuous process for dry fractionation of glyceride oilsInfo
- Publication number
- MY184018A MY184018A MYPI2014703630A MYPI2014703630A MY184018A MY 184018 A MY184018 A MY 184018A MY PI2014703630 A MYPI2014703630 A MY PI2014703630A MY PI2014703630 A MYPI2014703630 A MY PI2014703630A MY 184018 A MY184018 A MY 184018A
- Authority
- MY
- Malaysia
- Prior art keywords
- glyceride oil
- temperature
- sop
- oil
- glyceride
- Prior art date
Links
- 125000005456 glyceride group Chemical group 0.000 title abstract 18
- 238000005194 fractionation Methods 0.000 title abstract 3
- 238000010924 continuous production Methods 0.000 title 1
- 239000003921 oil Substances 0.000 title 1
- 239000007788 liquid Substances 0.000 abstract 3
- 239000013078 crystal Substances 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- PHYFQTYBJUILEZ-IUPFWZBJSA-N triolein Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CCCCCCCC)COC(=O)CCCCCCC\C=C/CCCCCCCC PHYFQTYBJUILEZ-IUPFWZBJSA-N 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000007711 solidification Methods 0.000 abstract 1
- 230000008023 solidification Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B7/00—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils
- C11B7/0075—Separation of mixtures of fats or fatty oils into their constituents, e.g. saturated oils from unsaturated oils by differences of melting or solidifying points
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provide a continuous dry fractionation process comprising the successive step of: (a) providing a liquid glyceride oil having a temperature that is at least 5?C higher than the solidification onset point (SOP) of the glyceride oil, the SOP of the glyceride oil being the minimum temperature at which the glyceride oil has a N-value of 0%; (b) precooling the liquid glyceride oil at a cooling rate of at least 1 ?C/min by passing the glyceride oil through a heat exchanger to reduce the temperature of the liquid glyceride oil with at least 5?C to a temperature that is not lower than 10?C below the SOP and not higher than 5?C above the SOP; (c) homogenizing the precooled glyceride oil to produce a prenucleated glyceride oil by passing the precooled glyceride oil through a homogenizer in which the temperature of the glyceride oil is kept a temperature within 1?C of the prenucleation temperature Tp for at least 0.5 hour, said Tp being 0.5-10?C below the SOP; (d) crystallizing the prenucleated glyceride oil to produce a crystallized glyceride oil containing separable fat crystals by passing the prenucleated glyeride oil through one or more crystallizers to reduce the temperature of the prenucleated glyceride oil with at least 10?C to a crystallization temperature Tc and keeping the glyceride oil at a temperature within 1?C of Tc for at least 1 hour; and (e) removing separable fat crystals from the crystallized glyceride oil and recovering an olein fraction of the glyceride oil. This continuous fractionation process enables the manufacture of a high quality olein fraction in high yield and in a relatively short period of time.
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MYPI2014703630A MY184018A (en) | 2014-12-03 | 2014-12-03 | Continuous process for dry fractionation of glyceride oils |
| PT157666686T PT3227418T (en) | 2014-12-03 | 2015-07-16 | Continuous process for dry fractionation of glyceride oils |
| ES15766668T ES2753402T3 (en) | 2014-12-03 | 2015-07-16 | Continuous process for the dry fractionation of glyceride oils |
| PCT/MY2015/000059 WO2016089196A1 (en) | 2014-12-03 | 2015-07-16 | Continuous process for dry fractionation of glyceride oils |
| EP15766668.6A EP3227418B1 (en) | 2014-12-03 | 2015-07-16 | Continuous process for dry fractionation of glyceride oils |
| PL15766668T PL3227418T3 (en) | 2014-12-03 | 2015-07-16 | Continuous process for dry fractionation of glyceride oils |
| DK15766668T DK3227418T3 (en) | 2014-12-03 | 2015-07-16 | CONTINUOUS PROCEDURE FOR DRY FRACTIONING GLYCERID OILS |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MYPI2014703630A MY184018A (en) | 2014-12-03 | 2014-12-03 | Continuous process for dry fractionation of glyceride oils |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY184018A true MY184018A (en) | 2021-03-17 |
Family
ID=54148603
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI2014703630A MY184018A (en) | 2014-12-03 | 2014-12-03 | Continuous process for dry fractionation of glyceride oils |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP3227418B1 (en) |
| DK (1) | DK3227418T3 (en) |
| ES (1) | ES2753402T3 (en) |
| MY (1) | MY184018A (en) |
| PL (1) | PL3227418T3 (en) |
| PT (1) | PT3227418T (en) |
| WO (1) | WO2016089196A1 (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108837551B (en) * | 2018-07-28 | 2024-04-02 | 湖南懋天世纪新材料有限公司 | Superfine ammonium paratungstate evaporation crystallization device and crystallization method |
| CN110257169A (en) * | 2019-06-12 | 2019-09-20 | 深圳精益油脂技术有限公司 | A method of preparing the palm oil of low ethylene oxidic ester and low 3-MCPD ester content |
| MY203841A (en) * | 2020-03-10 | 2024-07-20 | Liew Heng Wen | Dry fractionation of edible oil |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1120456A (en) * | 1964-12-14 | 1968-07-17 | Ranchers Cotton Oil | Method of separating components of oleaginous mixtures by fractional crystallization |
| DE2901328C2 (en) * | 1979-01-15 | 1985-07-25 | Walter Rau Lebensmittelwerke GmbH & Co. KG, 4517 Hilter | Process for the selective extraction of triglycerides or mixtures of triglycerides of higher fatty acids in crystalline form from natural fats |
| CA1301775C (en) * | 1986-06-04 | 1992-05-26 | Karel Petrus Agnes Maria Van Putte | Fractionation of fat blends |
| DE4132892A1 (en) * | 1991-10-04 | 1993-04-22 | Krupp Maschinentechnik | SUBSTANCE MIXING FACTIONING |
| AU742221B2 (en) * | 1997-05-12 | 2001-12-20 | Wisconsin Alumni Research Foundation | Continuous crystallization system with controlled nucleation for milk fat fractionation |
| EP1281749B1 (en) * | 2001-07-31 | 2009-10-14 | De Smet Engineering N.V. | Process and installation for dry fractionation |
| EP1818088A1 (en) * | 2006-01-20 | 2007-08-15 | De Smet Engineering N.V. | Crystallisers useful in fractionation processes for oils and fats |
| GB2496606B (en) * | 2011-11-15 | 2014-01-22 | Desmet Ballestra Engineering S A Nv | Continuous fractionation of triglyceride oils |
-
2014
- 2014-12-03 MY MYPI2014703630A patent/MY184018A/en unknown
-
2015
- 2015-07-16 EP EP15766668.6A patent/EP3227418B1/en active Active
- 2015-07-16 DK DK15766668T patent/DK3227418T3/en active
- 2015-07-16 WO PCT/MY2015/000059 patent/WO2016089196A1/en not_active Ceased
- 2015-07-16 ES ES15766668T patent/ES2753402T3/en active Active
- 2015-07-16 PL PL15766668T patent/PL3227418T3/en unknown
- 2015-07-16 PT PT157666686T patent/PT3227418T/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP3227418A1 (en) | 2017-10-11 |
| PL3227418T3 (en) | 2020-06-15 |
| ES2753402T3 (en) | 2020-04-08 |
| DK3227418T3 (en) | 2019-11-11 |
| PT3227418T (en) | 2019-11-05 |
| WO2016089196A1 (en) | 2016-06-09 |
| EP3227418B1 (en) | 2019-09-04 |
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