MY169486A - Process for producing hydrogen peroxide - Google Patents
Process for producing hydrogen peroxideInfo
- Publication number
- MY169486A MY169486A MYPI2014000987A MYPI2014000987A MY169486A MY 169486 A MY169486 A MY 169486A MY PI2014000987 A MYPI2014000987 A MY PI2014000987A MY PI2014000987 A MYPI2014000987 A MY PI2014000987A MY 169486 A MY169486 A MY 169486A
- Authority
- MY
- Malaysia
- Prior art keywords
- hydrogen peroxide
- oxidation
- hydrogenation
- working solution
- unit
- Prior art date
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title abstract 10
- 238000000034 method Methods 0.000 title abstract 3
- 230000003647 oxidation Effects 0.000 abstract 5
- 238000007254 oxidation reaction Methods 0.000 abstract 5
- 238000005984 hydrogenation reaction Methods 0.000 abstract 4
- 239000012224 working solution Substances 0.000 abstract 4
- 238000000605 extraction Methods 0.000 abstract 3
- 239000003054 catalyst Substances 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 238000004519 manufacturing process Methods 0.000 abstract 2
- 230000008929 regeneration Effects 0.000 abstract 2
- 238000011069 regeneration method Methods 0.000 abstract 2
- PYKYMHQGRFAEBM-UHFFFAOYSA-N anthraquinone Natural products CCC(=O)c1c(O)c2C(=O)C3C(C=CC=C3O)C(=O)c2cc1CC(=O)OC PYKYMHQGRFAEBM-UHFFFAOYSA-N 0.000 abstract 1
- 150000004056 anthraquinones Chemical class 0.000 abstract 1
- 238000006701 autoxidation reaction Methods 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 230000007420 reactivation Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/022—Preparation from organic compounds
- C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
A process for manufacturing hydrogen peroxide by an anthraquinone autoxidation process (AO-process) comprising two alternate essential steps of: (a) hydrogenation of a working solution in a hydrogenation unit in the presence of a catalyst, wherein the working solution contains at least one alkylanthraquinone dissolved in at least one organic solvent, to obtain at least one corresponding alkylanthrahydroquinonc compound; and (b) oxidation of the at least one alkylanthrahydroquinone compound to obtain hydrogen peroxide in an oxidation unit; and further comprising step (c): extracting the hydrogen peroxide formed in the oxidation step in an extraction unit wherein the hydrogenation, oxidation and extraction steps are performed in an reactor system which is designed as a compact modular system of a hydrogenation. an oxidation and an extraction unit. and wherein the reactor system is configured to operate without a reversion (regeneration) unit for continuous reversion of the working solution as a small to medium scale AO-process with a production capacity of hydrogen peroxide of up to 20 kilo tons per year. wherein the working solution and/or the catalyst are replaced and/or treated for regeneration or reactivation only intermittently or periodically, e.g., with a low frequency.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11184576 | 2011-10-11 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MY169486A true MY169486A (en) | 2019-04-15 |
Family
ID=46963742
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MYPI2014000987A MY169486A (en) | 2011-10-11 | 2012-10-02 | Process for producing hydrogen peroxide |
Country Status (17)
| Country | Link |
|---|---|
| US (1) | US9617153B2 (en) |
| EP (1) | EP2766300B1 (en) |
| CN (1) | CN103974899B (en) |
| AP (1) | AP3843A (en) |
| AR (1) | AR088292A1 (en) |
| BR (1) | BR112014008478B1 (en) |
| CA (1) | CA2850214C (en) |
| CL (1) | CL2014000810A1 (en) |
| ES (1) | ES2808336T3 (en) |
| IN (1) | IN2014CN03354A (en) |
| MY (1) | MY169486A (en) |
| PE (1) | PE20141490A1 (en) |
| PT (1) | PT2766300T (en) |
| RU (1) | RU2609474C2 (en) |
| UY (1) | UY34377A (en) |
| WO (1) | WO2013053617A1 (en) |
| ZA (1) | ZA201402448B (en) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013053616A1 (en) | 2011-10-11 | 2013-04-18 | Solvay Sa | Process for producing hydrogen peroxide |
| CN105540551B (en) * | 2014-11-03 | 2017-07-28 | 中国石油化工股份有限公司 | A kind of efficient hydrogenation process in Hydrogen Peroxide Production |
| US9890397B1 (en) | 2015-07-15 | 2018-02-13 | Gaurab Chakrabarti | Hydrogen peroxide production method, system, and apparatus |
| WO2017028911A1 (en) * | 2015-08-19 | 2017-02-23 | Solvay Sa | Process for manufacturing hydrogen peroxide |
| US11203769B1 (en) | 2017-02-13 | 2021-12-21 | Solugen, Inc. | Hydrogen peroxide and gluconic acid production |
| CN108862205B (en) * | 2018-08-29 | 2023-09-12 | 江苏德邦工程有限公司 | Hydrogen peroxide preparation device |
| WO2021048365A1 (en) * | 2019-09-11 | 2021-03-18 | Solvay Sa | Process for manufacturing an alkyl substituted cyclohexanecarbonitrile |
| BR112022004135A2 (en) * | 2019-09-11 | 2022-05-31 | Solvay | Process for making an aqueous solution of hydrogen peroxide |
| CN114702012B (en) * | 2022-04-06 | 2024-05-03 | 山东华鲁恒升化工股份有限公司 | Working solution, preparation method thereof and application thereof in producing hydrogen peroxide by anthraquinone process |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2158525A (en) | 1935-10-10 | 1939-05-16 | Ig Farbenindustrie Ag | Production of hydrogen peroxide |
| IT360853A (en) | 1937-04-07 | |||
| US2739875A (en) * | 1951-12-06 | 1956-03-27 | Du Pont | Regeneration of degraded alkylanthraquinone solutions for the production of hydrogen peroxide |
| GB798237A (en) | 1956-01-27 | 1958-07-16 | Du Pont | Improvements in or relating to the production of hydrogen peroxide |
| US3330625A (en) * | 1963-10-22 | 1967-07-11 | Pittsburgh Plate Glass Co | Hydrogen peroxide manufacture |
| US4061598A (en) | 1976-06-25 | 1977-12-06 | E. I. Du Pont De Nemours And Company | Catalyst for hydrogenating anthraquinones |
| US4428922A (en) | 1982-05-14 | 1984-01-31 | Fmc Corporation | Process for manufacturing hydrogen peroxide |
| JPS604121A (en) | 1983-06-23 | 1985-01-10 | Taisho Pharmaceut Co Ltd | Suppository |
| US5488024A (en) * | 1994-07-01 | 1996-01-30 | Phillips Petroleum Company | Selective acetylene hydrogenation |
| FI97465C (en) | 1995-02-10 | 1996-12-27 | Kemira Chemicals Oy | Process for producing hydrogen peroxide |
| FR2730985B1 (en) | 1995-02-28 | 1997-08-01 | Chemoxal Sa | PROCESS AND PLANT FOR PRODUCING HYDROGEN PEROXIDE |
| US5662878A (en) * | 1996-04-25 | 1997-09-02 | University Of Chicago | Process for the production of hydrogen peroxide |
| BR9712193A (en) | 1996-10-04 | 1999-08-31 | . | Hydrogenation catalysts based on palladium, platinum or rhodium, on a support of zirconium and silicon oxides, manufacturing process and use of them, and hydrogen peroxide manufacturing process. |
| GB2334028A (en) * | 1998-02-04 | 1999-08-11 | Solvay | Making hydrogen peroxide by the anthraquinone process |
| FR2803783B1 (en) | 2000-01-13 | 2002-04-26 | Valfond Argentan S A | BIMETALLIC PIECE IN ALUMINUM ALLOY COMPRISING A SOLID TITANIUM OR TITANIUM ALLOY INSERT |
| DE10336852A1 (en) * | 2003-08-11 | 2005-03-10 | Degussa | Process for the preparation of hydrogen peroxide by the anthraquinone cyclic process |
| US8366796B2 (en) | 2007-07-09 | 2013-02-05 | Range Fuels, Inc. | Modular and distributed methods and systems to convert biomass to syngas |
| FR2930772B1 (en) | 2008-04-30 | 2010-04-30 | Arkema France | DIRECT OXYGENED WATER SYNTHESIS ON A PAPER SITE |
| KR100998082B1 (en) * | 2008-07-22 | 2010-12-03 | 오씨아이 주식회사 | Hydrogen peroxide production method with improved productivity and composition for same |
| US9903027B2 (en) | 2008-12-17 | 2018-02-27 | Thyssenkrupp Uhde Chlorine Engineers (Italia) S.R. | Process for producing chlorine, caustic soda, and hydrogen |
| US8558043B2 (en) | 2009-03-04 | 2013-10-15 | Kior, Inc. | Modular biomass treatment unit |
| CN102395527A (en) | 2009-03-27 | 2012-03-28 | 索尔维公司 | Method for the production of hydrogen peroxide |
| WO2013053616A1 (en) | 2011-10-11 | 2013-04-18 | Solvay Sa | Process for producing hydrogen peroxide |
| EP2639200A1 (en) | 2012-03-13 | 2013-09-18 | Solvay Sa | Plant for hydrogen peroxide production and a process using it |
-
2012
- 2012-10-02 PE PE2014000526A patent/PE20141490A1/en active IP Right Grant
- 2012-10-02 IN IN3354CHN2014 patent/IN2014CN03354A/en unknown
- 2012-10-02 PT PT127666741T patent/PT2766300T/en unknown
- 2012-10-02 MY MYPI2014000987A patent/MY169486A/en unknown
- 2012-10-02 EP EP12766674.1A patent/EP2766300B1/en not_active Revoked
- 2012-10-02 RU RU2014118565A patent/RU2609474C2/en active
- 2012-10-02 US US14/350,825 patent/US9617153B2/en not_active Expired - Fee Related
- 2012-10-02 BR BR112014008478-5A patent/BR112014008478B1/en not_active IP Right Cessation
- 2012-10-02 WO PCT/EP2012/069414 patent/WO2013053617A1/en not_active Ceased
- 2012-10-02 ES ES12766674T patent/ES2808336T3/en active Active
- 2012-10-02 CA CA2850214A patent/CA2850214C/en active Active
- 2012-10-02 AP AP2014007562A patent/AP3843A/en active
- 2012-10-02 CN CN201280056747.8A patent/CN103974899B/en not_active Expired - Fee Related
- 2012-10-09 UY UY0001034377A patent/UY34377A/en active IP Right Grant
- 2012-10-10 AR ARP120103775A patent/AR088292A1/en active IP Right Grant
-
2014
- 2014-04-02 CL CL2014000810A patent/CL2014000810A1/en unknown
- 2014-04-02 ZA ZA2014/02448A patent/ZA201402448B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| ES2808336T3 (en) | 2021-02-26 |
| CL2014000810A1 (en) | 2014-06-20 |
| WO2013053617A1 (en) | 2013-04-18 |
| ZA201402448B (en) | 2016-03-30 |
| AR088292A1 (en) | 2014-05-21 |
| EP2766300B1 (en) | 2020-05-20 |
| CN103974899A (en) | 2014-08-06 |
| IN2014CN03354A (en) | 2015-07-03 |
| RU2609474C2 (en) | 2017-02-02 |
| CA2850214A1 (en) | 2013-04-18 |
| RU2014118565A (en) | 2015-11-20 |
| AP2014007562A0 (en) | 2014-04-30 |
| PE20141490A1 (en) | 2014-10-23 |
| UY34377A (en) | 2013-04-30 |
| US20140234202A1 (en) | 2014-08-21 |
| PT2766300T (en) | 2020-07-29 |
| US9617153B2 (en) | 2017-04-11 |
| CA2850214C (en) | 2020-08-25 |
| AP3843A (en) | 2016-09-30 |
| CN103974899B (en) | 2017-03-29 |
| BR112014008478A2 (en) | 2017-04-11 |
| BR112014008478B1 (en) | 2021-04-13 |
| EP2766300A1 (en) | 2014-08-20 |
| BR112014008478A8 (en) | 2020-05-19 |
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