MX394637B - Proceso de produccion y de purificacion del 2,3,3,3-tetrafluoropropeno. - Google Patents
Proceso de produccion y de purificacion del 2,3,3,3-tetrafluoropropeno.Info
- Publication number
- MX394637B MX394637B MX2018007594A MX2018007594A MX394637B MX 394637 B MX394637 B MX 394637B MX 2018007594 A MX2018007594 A MX 2018007594A MX 2018007594 A MX2018007594 A MX 2018007594A MX 394637 B MX394637 B MX 394637B
- Authority
- MX
- Mexico
- Prior art keywords
- tetrafluoropropene
- pentafluoropropane
- chloro
- trifluoropropene
- composition
- Prior art date
Links
- FXRLMCRCYDHQFW-UHFFFAOYSA-N 2,3,3,3-tetrafluoropropene Chemical compound FC(=C)C(F)(F)F FXRLMCRCYDHQFW-UHFFFAOYSA-N 0.000 title abstract 6
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- OQISUJXQFPPARX-UHFFFAOYSA-N 2-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)C(Cl)=C OQISUJXQFPPARX-UHFFFAOYSA-N 0.000 abstract 5
- FDOPVENYMZRARC-UHFFFAOYSA-N 1,1,1,2,2-pentafluoropropane Chemical compound CC(F)(F)C(F)(F)F FDOPVENYMZRARC-UHFFFAOYSA-N 0.000 abstract 4
- MSSNHSVIGIHOJA-UHFFFAOYSA-N pentafluoropropane Chemical compound FC(F)CC(F)(F)F MSSNHSVIGIHOJA-UHFFFAOYSA-N 0.000 abstract 2
- CDOOAUSHHFGWSA-OWOJBTEDSA-N (e)-1,3,3,3-tetrafluoroprop-1-ene Chemical compound F\C=C\C(F)(F)F CDOOAUSHHFGWSA-OWOJBTEDSA-N 0.000 abstract 1
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000013067 intermediate product Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/18—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds containing fluorine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
La invención se refiere a un proceso de producción del 2,3,3,3-tetrafluoropropeno puesto en operación a partir de una composición de partida que comprende las etapas de la puesta en contacto, en presencia de un catalizador, de la composición de partida con HF para producir una composición A que comprende 2,3,3, 3-tetrafluoropropeno (1234yf), los productos intermediarios B que consisten en 2-cloro-3,3,3-trifluoropropeno (1233xf), 1,1,1,2, 2-pentafluoropropano (245cb), y productos secundarios C que consisten en E-1-cloro-3,3,3-trifluoro-1-propeno (1233zd E), trans-1,3,3,3-tetrafluoro-1-propeno(1234ze E) y 1,1,1,3,3-pentafluoropropano (245fa); la recuperación de la composición A y la purificación de la misma para formar y recuperar una primera corriente que comprende 2,3,3,3-tetrafluoropropeno (1234yf) y uno o varios flujos que comprenden el 2-cloro-3,3,3-trifluoropropeno (1233xf) y/o el 1,1,1,2,2-pentafluoropropano (245cb); el reciclamiento hacia la etapa a) de uno o de varios flujos que comprenden 2-cloro-3,3,3-trifluoropropeno (1233xf) y/o 1,1,1,2, 2-pentafluoropropano (245cb).
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1563168A FR3046164B1 (fr) | 2015-12-23 | 2015-12-23 | Procede de production et de purification du 2,3,3,3-tetrafluoropropene. |
| PCT/EP2016/080949 WO2017108523A1 (fr) | 2015-12-23 | 2016-12-14 | Procede de production et de purification du 2,3,3,3-tetrafluoropropene |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MX2018007594A MX2018007594A (es) | 2018-09-21 |
| MX394637B true MX394637B (es) | 2025-03-24 |
Family
ID=55971114
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2018007594A MX394637B (es) | 2015-12-23 | 2016-12-14 | Proceso de produccion y de purificacion del 2,3,3,3-tetrafluoropropeno. |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US10407369B2 (es) |
| EP (1) | EP3394019B1 (es) |
| JP (1) | JP6964589B2 (es) |
| CN (1) | CN108368013A (es) |
| ES (1) | ES2777607T3 (es) |
| FR (1) | FR3046164B1 (es) |
| MX (1) | MX394637B (es) |
| PL (1) | PL3394019T3 (es) |
| WO (1) | WO2017108523A1 (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108383679B (zh) * | 2018-04-13 | 2021-04-13 | 淄博飞源化工有限公司 | 一种反式-1-氯-3,3,3-三氟丙烯和2,3,3,3-四氟丙烯的联产方法 |
| CN109384640B (zh) * | 2018-12-30 | 2022-02-15 | 山东华安新材料有限公司 | 一种2,3,3,3-四氟丙烯的制备装置及制备方法 |
| FR3100461B1 (fr) | 2019-09-06 | 2021-09-03 | Arkema France | Procédé de purification d’hydrofluorocarbures |
| CN113527049B (zh) * | 2020-04-22 | 2024-08-23 | 陕西中蓝化工科技新材料有限公司 | 一种反式/顺式-HFO-1234ze和HFO-1234yf的联产制备工艺 |
| CN116199560B (zh) * | 2023-04-28 | 2023-07-14 | 山东澳帆新材料有限公司 | 一种反式-1-氯-3,3,3-三氟丙烯与1,1,1,3,3-五氟丙烷混合物的分离方法 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5874657A (en) | 1996-11-01 | 1999-02-23 | E. I. Du Pont De Nemours And Company | Process for the purification of 1,1-difluoroethane |
| EP0864554B1 (en) | 1997-03-11 | 2002-09-18 | Central Glass Company, Limited | Method for purifying crude 1,1,1,3,3-pentafluoropropane |
| DE69909860T2 (de) | 1998-02-26 | 2004-05-27 | Central Glass Co., Ltd., Ube | Verfahren zur Herstellung von fluorierten Propanen |
| US7060165B2 (en) | 2002-02-14 | 2006-06-13 | Pcbu Services, Inc. | Processes for purification and production of fluorocarbons |
| EP2546225B1 (en) | 2006-01-03 | 2017-12-20 | Honeywell International Inc. | Method for producing fluorinated organic compounds |
| JP5416587B2 (ja) | 2006-10-03 | 2014-02-12 | メキシケム、アマンコ、ホールディング、ソシエダッド、アノニマ、デ、カピタル、バリアブレ | プロセス |
| CN103483140B (zh) | 2006-10-31 | 2015-09-09 | 纳幕尔杜邦公司 | 氟丙烷、卤代丙烯以及2-氯-3,3,3-三氟-1-丙烯与hf的共沸组合物和1,1,1,2,2-五氟丙烷与hf的共沸组合物的制备方法 |
| RU2474569C2 (ru) * | 2008-02-21 | 2013-02-10 | Е.И.Дюпон Де Немур Энд Компани | Способ отделения 1,3,3,3-тетрафторпропена от фтороводорода азеотропной дистилляцией |
| CN102686542A (zh) * | 2009-12-23 | 2012-09-19 | 阿克马法国公司 | 1233xf到1234yf的催化气相氟化 |
| US8900417B2 (en) * | 2010-07-23 | 2014-12-02 | Daikin Industries, Ltd. | Purification method of 2,3,3,3-tetrafluoropropene |
| ES2773202T3 (es) * | 2010-10-22 | 2020-07-09 | Arkema France | Proceso para la preparación de 2,3,3,3-tetrafluoropropeno |
| CN107814685A (zh) * | 2011-01-21 | 2018-03-20 | 阿克马法国公司 | 通过五氯丙烷的气相氟化制造2,3,3,3‑四氟丙烯的方法 |
| US9340473B2 (en) * | 2011-01-21 | 2016-05-17 | Arkema France | Catalytic gas phase fluorination |
| FR2977584B1 (fr) * | 2011-07-08 | 2014-12-05 | Arkema France | Procede de separation et recuperation du 2,3,3,3-tetrafluoropropene et de l'acide fluorhydrique |
| JP5992532B2 (ja) * | 2011-12-14 | 2016-09-14 | アルケマ フランス | 2,3,3,3−テトラフルオロプロペンを調製する方法 |
| US9334206B2 (en) * | 2013-03-15 | 2016-05-10 | Honeywell International Inc. | Integrated process to produce 2,3,3,3-tetrafluoropropene |
| CN104710274B (zh) * | 2013-12-13 | 2017-05-03 | 中化近代环保化工(西安)有限公司 | 联产制备1,3,3,3‑四氟丙烯和/或2,3,3,3‑四氟丙烯的工艺 |
| CN104744210A (zh) * | 2013-12-25 | 2015-07-01 | 中化近代环保化工(西安)有限公司 | 一种2,3,3,3-四氟丙烯的制备工艺 |
-
2015
- 2015-12-23 FR FR1563168A patent/FR3046164B1/fr not_active Expired - Fee Related
-
2016
- 2016-12-14 MX MX2018007594A patent/MX394637B/es unknown
- 2016-12-14 US US16/063,302 patent/US10407369B2/en active Active
- 2016-12-14 JP JP2018532114A patent/JP6964589B2/ja not_active Expired - Fee Related
- 2016-12-14 EP EP16809821.8A patent/EP3394019B1/fr active Active
- 2016-12-14 PL PL16809821T patent/PL3394019T3/pl unknown
- 2016-12-14 ES ES16809821T patent/ES2777607T3/es active Active
- 2016-12-14 CN CN201680071474.2A patent/CN108368013A/zh active Pending
- 2016-12-14 WO PCT/EP2016/080949 patent/WO2017108523A1/fr not_active Ceased
-
2019
- 2019-07-24 US US16/521,031 patent/US10730813B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| ES2777607T3 (es) | 2020-08-05 |
| CN108368013A (zh) | 2018-08-03 |
| EP3394019A1 (fr) | 2018-10-31 |
| PL3394019T3 (pl) | 2020-06-29 |
| WO2017108523A1 (fr) | 2017-06-29 |
| FR3046164B1 (fr) | 2021-01-08 |
| US10407369B2 (en) | 2019-09-10 |
| US10730813B2 (en) | 2020-08-04 |
| FR3046164A1 (fr) | 2017-06-30 |
| EP3394019B1 (fr) | 2020-01-29 |
| US20190345083A1 (en) | 2019-11-14 |
| US20180370879A1 (en) | 2018-12-27 |
| JP2019501166A (ja) | 2019-01-17 |
| JP6964589B2 (ja) | 2021-11-10 |
| MX2018007594A (es) | 2018-09-21 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| MX2014009265A (es) | Proceso mejorado para la fabricacion de 2, 3, 3, 3 - tetrafluoropropeno. | |
| MX344552B (es) | Proceso para producir 2, 3, 3, 3 - tetrafluoropropeno. | |
| MX394637B (es) | Proceso de produccion y de purificacion del 2,3,3,3-tetrafluoropropeno. | |
| MX2009003206A (es) | Composiciones semejantes a azeotropo de 2-cloro-3,3,3,-trifluoropr open (hcfc-1233xf y 2-cloro-1,1,1,2-tetrafluoropropano (hcfc-244bb). | |
| MX2009003492A (es) | Composiciones azeotropicas de 2-cloro-3,3,3-trifluoropropeno (hcfc-1233xf), 2-cloro-1,1,1,2-tetrafluoropropano (hcfc-244bb), y fluoruro de hidrogeno (hf). | |
| MX341276B (es) | Procedimiento para la fabricacion de 2,3,3,3-tetrafluoropropeno mediante fluoracion en fase gaseosa de pentacloropropano. | |
| SG10201509239XA (en) | Compositions comprising 2,3,3,3-tetrafluoropropene, 1,1,2,3-tetrachloropropene, 2-chloro-3,3,3-trifluoropropene, or 2-chloro-1,1,1,2-tetrafluoropropane | |
| MX2009008958A (es) | Metodo para separar halocarburos. | |
| MX2023009585A (es) | Isomerizacion catalitica de z-1,1,1,4,4,4-hexafluoro-2- buteno a e-1,1,1,4,4,4-hexafluoro-2-buteno. | |
| WO2012148695A3 (en) | INTEGRATED PROCESS TO CO-PRODUCE 1,1,1,3,3-PENTAFLUOROPROPANE, TRANS-1-CHLORO-3,3,3-TRIFLUOROPROPENE and TRANS-1,3,3,3-TETRAFLUOROPROPENE | |
| WO2012154227A3 (en) | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene, trans-1,3,3,3-tetrafluoropropene, and 1,1,1,3,3-pentafluoropropane | |
| EP3505504A4 (en) | METHOD FOR COPRODUCING 1-CHLORINE-3,3,3-TRIFLUORPROPEN, 2,3,3,3-TETRAFLUORPROPEN AND 1,3,3,3-TETRAFLUORPROPEN | |
| IN2014DN07744A (es) | ||
| MX2013005403A (es) | Composiciones similares a azeotropos que comprende 1 - cloro - 3, 3, 3 - trifluoropropeno. | |
| MX344948B (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno. | |
| PL2563750T3 (pl) | SPOSÓB WYTWARZANIA 2-CHLORO-3,3,3-TRIFLUOROPROPENU (HCFO 1233xf) PRZEZ FLUOROWANIE PENTACHLOROPROPANU W FAZIE CIEKŁEJ | |
| MX2016004735A (es) | Proceso para producir 1-cloro-3,3,3-trifluropropeno en un liquido ionico. | |
| MX367470B (es) | Proceso para la preparacion de 1-cloro-3,3,3-trifluoropropeno utilizando un catalizador de transferencia de fase. | |
| EP3202882A4 (en) | Azeotropic like composition containing 2-chloro-1,3,3,3-tetrafluoropropene and 1-chloro-3,3,3-trifluoropropene | |
| MX2013004414A (es) | Proceso para la fabricacion de 2-cloro-1,1,1,2-tetrafluoropropano por fluoracion en fase liquida de 2-cloro-3,3,3-trifluoropropeno. | |
| MX2015010962A (es) | Proceso para producir 2,3,3,3-tetrafluoropropeno. | |
| MX2014003659A (es) | Proceso para producir 2,3,3,3 - tetrafluoropropeno. | |
| MX389335B (es) | Procedimiento de produccion de e-1-cloro-3,3,3-trifluoropropeno a partir de 1,1,3,3-tetracloropropeno. | |
| GB2540427B (en) | Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf) | |
| MX2013005459A (es) | Proceso para la fabricacion de 2-cloro-3,3,3-trifluoropropeno (hcfo 1233xf) por fluoracion en bas liquida de pentacloropropano. |