MX2013013144A - Metodo para la produccion de un dimero mdi. - Google Patents
Metodo para la produccion de un dimero mdi.Info
- Publication number
- MX2013013144A MX2013013144A MX2013013144A MX2013013144A MX2013013144A MX 2013013144 A MX2013013144 A MX 2013013144A MX 2013013144 A MX2013013144 A MX 2013013144A MX 2013013144 A MX2013013144 A MX 2013013144A MX 2013013144 A MX2013013144 A MX 2013013144A
- Authority
- MX
- Mexico
- Prior art keywords
- mdi
- dimer
- phenylisocyanate
- methylenebis
- solvent
- Prior art date
Links
- 239000000539 dimer Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- UPMLOUAZCHDJJD-UHFFFAOYSA-N 4,4'-Diphenylmethane Diisocyanate Chemical compound C1=CC(N=C=O)=CC=C1CC1=CC=C(N=C=O)C=C1 UPMLOUAZCHDJJD-UHFFFAOYSA-N 0.000 abstract 9
- 239000002904 solvent Substances 0.000 abstract 3
- 238000003756 stirring Methods 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/18—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D229/00—Heterocyclic compounds containing rings of less than five members having two nitrogen atoms as the only ring hetero atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/84—Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
- C07C265/12—Derivatives of isocyanic acid having isocyanate groups bound to carbon atoms of six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/82—Post-polymerisation treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
La invención se refiere a un método para la producción del dímero 4,4'-metilenbis (fenilisocianato) (dímero MDI) que se distingue por un dímero MDI obtenido que está presente con alta pureza. El dímero MDI que se produce de conformidad con el método de conformidad con la invención se distingue por estar esencialmente libre de MDI y también de derivados de urea. Además, la invención se refiere a un dímero MDI correspondiente y también a su uso como un entrelazador para poliuretanos.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12192416.1A EP2730563B1 (de) | 2012-11-13 | 2012-11-13 | Verfahren zur Herstellung von MDI-Dimer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2013013144A true MX2013013144A (es) | 2014-06-10 |
Family
ID=47172532
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2013013144A MX2013013144A (es) | 2012-11-13 | 2013-11-11 | Metodo para la produccion de un dimero mdi. |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US10047054B2 (es) |
| EP (2) | EP3150583B1 (es) |
| JP (1) | JP6173176B2 (es) |
| KR (1) | KR102168372B1 (es) |
| CN (1) | CN103804297B (es) |
| BR (1) | BR102013029100B1 (es) |
| MX (1) | MX2013013144A (es) |
| RU (1) | RU2648047C2 (es) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2450389B1 (de) | 2010-11-08 | 2015-03-18 | EMS-Patent AG | Haftvermittler für textile Verstärkungseinlagen und dessen Verwendung |
| EP2837643B1 (de) | 2013-08-16 | 2018-10-10 | Ems-Patent Ag | Pulverförmiger, in wasser dispergierbarer haftvermittler |
| EP3184577B1 (de) | 2015-12-23 | 2025-08-20 | Ems-Chemie Ag | Verfahren und behälter für die lagerung und den transport von polyamidgranulaten und entsprechend gelagertes oder transportiertes polyamidgranulat sowie hieraus hergestellte formkörper |
| EP3312224B1 (en) | 2016-10-21 | 2018-12-26 | Ems-Patent Ag | Polyamide moulding composition and multi-layered structure made herefrom |
| US9929540B1 (en) * | 2017-08-01 | 2018-03-27 | Denso International America, Inc. | Spark plug ground electrode |
| EP3444112B1 (de) | 2017-08-18 | 2020-12-23 | Ems-Chemie Ag | Verstärkte polyamid-formmassen mit geringem haze und formkörper daraus |
| EP3444114B1 (de) | 2017-08-18 | 2023-10-25 | Ems-Chemie Ag | Verstärkte polyamid-formmassen mit geringem haze und formkörper daraus |
| EP3444113B1 (de) | 2017-08-18 | 2021-01-20 | Ems-Chemie Ag | Verstärkte polyamid-formmassen mit geringem haze und formkörper daraus |
| EP3450481B1 (de) | 2017-08-31 | 2020-10-21 | Ems-Chemie Ag | Polyamid-formmasse mit hohem glanz und hoher kerbschlagzähigkeit |
| EP3502164B1 (de) | 2017-12-22 | 2022-10-05 | Ems-Chemie Ag | Polyamid-formmasse |
| EP3502191B1 (de) | 2017-12-22 | 2021-02-17 | Ems-Chemie Ag | Polyamid-formmasse |
| PT3597816T (pt) | 2018-07-19 | 2021-07-05 | Ems Chemie Ag | Composições de banho de imersão para o tratamento de insertos de reforço |
| PL3597686T3 (pl) | 2018-07-19 | 2021-04-19 | Ems-Patent Ag | Kompozycja kąpieli zanurzeniowej do obróbki wkładek wzmacniających |
| EP3636406B1 (de) | 2018-10-09 | 2021-04-28 | Ems-Chemie Ag | Schlagzähmodifizierte polyamid-formmassen |
| EP3772521B1 (de) | 2019-08-09 | 2023-06-07 | Ems-Chemie Ag | Teilkristalline copolyamide, diese enthaltende formmassen und deren verwendung sowie daraus hergestellte formkörper |
| EP3772520B1 (de) | 2019-08-09 | 2023-07-12 | Ems-Chemie Ag | Polyamid-formmasse und deren verwendung sowie aus der formmasse hergestellte formkörper |
| EP3842470A1 (de) | 2019-12-23 | 2021-06-30 | Ems-Chemie Ag | Polyamid-formmassen für hypochlorit-beständige anwendungen |
| EP3842496A1 (de) | 2019-12-23 | 2021-06-30 | Ems-Chemie Ag | Polyamid-formmassen für hypochlorit-beständige anwendungen |
| EP4015575A1 (de) | 2020-12-17 | 2022-06-22 | Ems-Chemie Ag | Gefüllte polyamid-formmassen, hieraus hergestellte formkörper und verwendung der gefüllten polyamid-formmassen |
| EP4015562A1 (de) | 2020-12-17 | 2022-06-22 | Ems-Chemie Ag | Polyamid-formmassen, hieraus hergestellte formkörper und verwendung der polyamid-formmassen |
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| JPS422896Y1 (es) | 1965-02-24 | 1967-02-21 | ||
| US3489744A (en) * | 1966-07-18 | 1970-01-13 | Uniroyal Inc | Preparation of diisocyanate dimers in aqueous medium |
| DE3131779A1 (de) * | 1981-08-12 | 1983-02-24 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von niedermolekularen 4,4'-diphenylmethan-uretdion-diisocyanaten |
| US4381332A (en) | 1982-01-19 | 1983-04-26 | W. R. Grace & Co. | Adhesive and resulting nonwoven fabric |
| US4477619A (en) | 1982-10-08 | 1984-10-16 | The B. F. Goodrich Company | Preparation of fabric for bonding to rubber |
| JPS6013869A (ja) | 1983-07-05 | 1985-01-24 | Nippon Zeon Co Ltd | ゴムと繊維の接着剤組成物 |
| EP0137427B1 (de) | 1983-10-11 | 1990-05-16 | Bayer Ag | Schlichtemittel für Glasfasern |
| DE3506834A1 (de) * | 1985-02-27 | 1986-08-28 | Bayer Ag, 5090 Leverkusen | Verfahren zur herstellung von additionsverbindungen aus 1 mol dimerisiertem oder niedrig-oligodimerisiertem 4,4'-diisocyanatodiphenylmethan und 2 bis 3 mol 4,4'-diisocyanatodiphenylmethan, entsprechende additionsverbindungen und ihre verwendung zur polyurethanherstellung |
| US4742095A (en) | 1985-07-25 | 1988-05-03 | Mobay Corporation | Continuous process for the production of aqueous polyurethane-urea dispersions |
| US4740528A (en) | 1986-07-18 | 1988-04-26 | Kimberly-Clark Corporation | Superwicking crosslinked polyurethane foam composition containing amino acid |
| EP0367812B1 (en) | 1988-04-18 | 1995-03-01 | S.C. Johnson & Son, Inc. | Process for preparing water-dispersable polyurethane/acrylic polymer compositions |
| JPH02151619A (ja) | 1988-12-05 | 1990-06-11 | Toray Ind Inc | ブロックドポリイソシアネート分散液 |
| DE3930670A1 (de) * | 1989-09-14 | 1991-03-28 | Basf Ag | Verfahren zur herstellung von uretdiongruppen aufweisenden polyisocyanaten |
| DE4218540A1 (de) * | 1992-06-05 | 1993-12-09 | Basf Ag | Verfahren zur Herstellung von Uretdiongruppen aufweisenden Polyisocanaten |
| US5565527A (en) * | 1992-06-05 | 1996-10-15 | Basf Aktiengesellschaft | Polymeric, catalytically active compounds, their preparation, and their use as catalysts in the preparation of polyisocyanates containing uretdione groups |
| ATE213257T1 (de) | 1993-03-31 | 2002-02-15 | Rhodia Chimie Sa | Verfahren zur herstellung von wässrigen emulsionen von ölen und/oder gummi und/oder vorzugsweise maskierten (poly)isocyanatharzen, und resultierende emulsionen |
| FR2733506B1 (fr) | 1995-04-28 | 1997-06-06 | Rhone Poulenc Chimie | Dispersions de latex a fonction hydroxyle et a fonction carboxylique et leur utilisation pour fabrication des revetements |
| JPH0912556A (ja) * | 1995-06-23 | 1997-01-14 | Nippon Polyurethane Ind Co Ltd | 低融点のジフェニルメタンジイソシアネート二量体の製造方法 |
| JPH09328474A (ja) | 1996-06-07 | 1997-12-22 | Nippon Polyurethane Ind Co Ltd | ジフェニルメタンジイソシアネート二量体の製造方法 |
| US5998539A (en) | 1996-10-08 | 1999-12-07 | Nippon Polyurethane Industry Co., Ltd. | Water-dispersible blocked isocyanate composition, and water-base paint composition and water-base adhesive composition using same |
| DE19644309A1 (de) | 1996-10-24 | 1998-04-30 | Basf Ag | Pulverförmiger Klebstoff |
| ZA981836B (en) | 1997-03-17 | 1999-09-06 | Dow Chemical Co | Continuous process for preparing a polyurethane latex. |
| DE19913042C2 (de) | 1999-03-23 | 2001-05-03 | Inventa Ag | Haftvermittler für textile Verstärkungseinlagen, Verfahren zur Herstellung und dessen Verwendung |
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| DE102004038784A1 (de) * | 2004-08-09 | 2006-02-23 | Basf Ag | Monomerarme Polyisocyanate |
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| MY148143A (en) | 2006-03-03 | 2013-03-15 | Indspec Chemical Corp | Resorcinol-blocked isocyanate compositions and their applications |
| DE102007058487A1 (de) * | 2007-12-04 | 2009-06-10 | Bayer Materialscience Ag | Herstellung von Uretdion-Polyisocyanaten |
| CN101250251A (zh) | 2008-03-21 | 2008-08-27 | 华南理工大学 | 一种高稳定性己内酰胺封端异氰酸酯粘合剂乳液的制备方法 |
| US8410213B2 (en) | 2009-01-26 | 2013-04-02 | Michael James Barker | Primerless two-part polyurethane adhesive |
| ATE510869T1 (de) | 2009-04-09 | 2011-06-15 | Isochem Kautschuk Gmbh | Verfahren zur herstellung von oligomeren diphenylmethan-4,4'- und/oder diphenylmethan-2,4'-diisocyanat-uretdionen |
| EP2450389B1 (de) | 2010-11-08 | 2015-03-18 | EMS-Patent AG | Haftvermittler für textile Verstärkungseinlagen und dessen Verwendung |
| EP2837643B1 (de) | 2013-08-16 | 2018-10-10 | Ems-Patent Ag | Pulverförmiger, in wasser dispergierbarer haftvermittler |
-
2012
- 2012-11-13 EP EP16197899.4A patent/EP3150583B1/de active Active
- 2012-11-13 EP EP12192416.1A patent/EP2730563B1/de active Active
-
2013
- 2013-11-01 RU RU2013148660A patent/RU2648047C2/ru active
- 2013-11-11 MX MX2013013144A patent/MX2013013144A/es unknown
- 2013-11-12 BR BR102013029100-5A patent/BR102013029100B1/pt active IP Right Grant
- 2013-11-12 JP JP2013234184A patent/JP6173176B2/ja active Active
- 2013-11-12 CN CN201310561355.3A patent/CN103804297B/zh active Active
- 2013-11-12 US US14/078,134 patent/US10047054B2/en active Active
- 2013-11-13 KR KR1020130137421A patent/KR102168372B1/ko active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP3150583A1 (de) | 2017-04-05 |
| JP2014097983A (ja) | 2014-05-29 |
| CN103804297A (zh) | 2014-05-21 |
| CN103804297B (zh) | 2018-04-27 |
| KR102168372B1 (ko) | 2020-10-22 |
| JP6173176B2 (ja) | 2017-08-02 |
| BR102013029100B1 (pt) | 2021-09-08 |
| US20140135458A1 (en) | 2014-05-15 |
| BR102013029100A2 (pt) | 2014-10-29 |
| EP2730563B1 (de) | 2017-01-11 |
| EP2730563A1 (de) | 2014-05-14 |
| RU2648047C2 (ru) | 2018-03-22 |
| KR20140061280A (ko) | 2014-05-21 |
| EP3150583B1 (de) | 2019-05-22 |
| US10047054B2 (en) | 2018-08-14 |
| RU2013148660A (ru) | 2015-05-10 |
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