MX2012003973A - Metodo para ailar metilglicinanitrilo-n, n-diacetonitrilo. - Google Patents
Metodo para ailar metilglicinanitrilo-n, n-diacetonitrilo.Info
- Publication number
- MX2012003973A MX2012003973A MX2012003973A MX2012003973A MX2012003973A MX 2012003973 A MX2012003973 A MX 2012003973A MX 2012003973 A MX2012003973 A MX 2012003973A MX 2012003973 A MX2012003973 A MX 2012003973A MX 2012003973 A MX2012003973 A MX 2012003973A
- Authority
- MX
- Mexico
- Prior art keywords
- diacetonitrile
- mgdn
- methylglycinenitrile
- isolating
- steps
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 239000000203 mixture Substances 0.000 abstract 3
- 238000001816 cooling Methods 0.000 abstract 2
- 238000007711 solidification Methods 0.000 abstract 2
- 230000008023 solidification Effects 0.000 abstract 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C253/00—Preparation of carboxylic acid nitriles
- C07C253/32—Separation; Purification; Stabilisation; Use of additives
- C07C253/34—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C255/00—Carboxylic acid nitriles
- C07C255/01—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
- C07C255/24—Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and singly-bound nitrogen atoms, not being further bound to other hetero atoms, bound to the same saturated acyclic carbon skeleton
- C07C255/25—Aminoacetonitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
Se provee un método para aislar metilglicinanitrilo-N,N-diacetonit rilo (MGDN) de una mezcla acuosa que comprende MGDN. El método comprende enfriar la mezcla acuosa en uno o más pasos. En uno de estos pasos, la mezcla se enfría a una velocidad de enfriamiento de por lo menos 20 K/h desde una temperatura arriba del punto de solidificación de MGDN a una temperatura debajo del punto de solidificación de MGDN. El método es implementado continuamente.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09172246A EP2308834A1 (de) | 2009-10-05 | 2009-10-05 | Verfahren zur Isolierung von Methylglycinnitril-N,N-diacetonitril |
| PCT/IB2010/054382 WO2011042836A1 (en) | 2009-10-05 | 2010-09-29 | Method for isolating methylglycinenitrile-n,n-diacetonitrile |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2012003973A true MX2012003973A (es) | 2012-05-08 |
Family
ID=41683091
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2012003973A MX2012003973A (es) | 2009-10-05 | 2010-09-29 | Metodo para ailar metilglicinanitrilo-n, n-diacetonitrilo. |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US20120184769A1 (es) |
| EP (2) | EP2308834A1 (es) |
| JP (1) | JP2013506652A (es) |
| KR (1) | KR20120093228A (es) |
| CN (1) | CN102725262A (es) |
| AU (1) | AU2010304779A1 (es) |
| BR (1) | BR112012007377A2 (es) |
| CA (1) | CA2774157A1 (es) |
| MX (1) | MX2012003973A (es) |
| RU (1) | RU2012118229A (es) |
| TW (1) | TW201121928A (es) |
| WO (1) | WO2011042836A1 (es) |
| ZA (1) | ZA201203155B (es) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9062278B2 (en) | 2010-02-19 | 2015-06-23 | Basf Se | Preparing ether carboxylates |
| US8802894B2 (en) | 2011-04-04 | 2014-08-12 | Basf Se | Process for the preparation of aqueous solutions of methylglycine-N,N-diacetic acid trialkali metal salts |
| US9227915B2 (en) | 2011-05-03 | 2016-01-05 | Basf Se | Process for the preparation of a crystalline L-MGDA trialkali metal salt |
| US8772527B2 (en) | 2012-04-27 | 2014-07-08 | Basf Se | Process for isomerization of cis-2-pentenenitrile to 3-pentenenitriles |
| CN107108476A (zh) | 2014-12-23 | 2017-08-29 | 阿克苏诺贝尔化学品国际有限公司 | 丙氨酸n‑乙酸前体的晶体、其制备方法及其应用 |
| WO2022006254A1 (en) * | 2020-06-30 | 2022-01-06 | Ascend Performance Materials Operations Llc | Production of nitrogen-containing chelators |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4319935A1 (de) | 1993-06-16 | 1994-12-22 | Basf Ag | Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen |
| DE19518986A1 (de) * | 1995-05-29 | 1996-12-05 | Basf Ag | Verfahren zur Herstellung von Glycin-N,N-diessigsäure-Derivaten durch Umsetzung von Glycinderivaten oder deren Vorstufen mit Formaldehyd und Cyanwasserstoff oder von Iminodiacetonitril oder Imindodiessigsäure mit entsprechenden Aldehyden und Cyanwasserstoff in wäßrig-saurem Medium |
| US7485747B2 (en) * | 2001-06-04 | 2009-02-03 | Eastman Chemical Company | Two stage oxidation process for the production of aromatic dicarboxylic acids |
| DE102005021056A1 (de) * | 2005-05-06 | 2006-11-09 | Basf Ag | Verfahren zur Isolierung von Methylglycinnitril-N,N-diacetonitrilen aus einem wässrigen Rohgemisch |
-
2009
- 2009-10-05 EP EP09172246A patent/EP2308834A1/de not_active Withdrawn
-
2010
- 2010-09-29 JP JP2012531535A patent/JP2013506652A/ja not_active Withdrawn
- 2010-09-29 KR KR1020127010250A patent/KR20120093228A/ko not_active Withdrawn
- 2010-09-29 CA CA2774157A patent/CA2774157A1/en not_active Abandoned
- 2010-09-29 US US13/498,825 patent/US20120184769A1/en not_active Abandoned
- 2010-09-29 EP EP10821654.0A patent/EP2486003A4/en not_active Withdrawn
- 2010-09-29 AU AU2010304779A patent/AU2010304779A1/en not_active Abandoned
- 2010-09-29 RU RU2012118229/04A patent/RU2012118229A/ru not_active Application Discontinuation
- 2010-09-29 CN CN2010800428828A patent/CN102725262A/zh active Pending
- 2010-09-29 WO PCT/IB2010/054382 patent/WO2011042836A1/en not_active Ceased
- 2010-09-29 MX MX2012003973A patent/MX2012003973A/es unknown
- 2010-09-29 BR BR112012007377A patent/BR112012007377A2/pt not_active IP Right Cessation
- 2010-10-04 TW TW099133737A patent/TW201121928A/zh unknown
-
2012
- 2012-05-02 ZA ZA2012/03155A patent/ZA201203155B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RU2012118229A (ru) | 2013-11-10 |
| EP2308834A1 (de) | 2011-04-13 |
| EP2486003A1 (en) | 2012-08-15 |
| ZA201203155B (en) | 2013-07-31 |
| EP2486003A4 (en) | 2013-12-11 |
| CA2774157A1 (en) | 2011-04-14 |
| JP2013506652A (ja) | 2013-02-28 |
| KR20120093228A (ko) | 2012-08-22 |
| US20120184769A1 (en) | 2012-07-19 |
| CN102725262A (zh) | 2012-10-10 |
| TW201121928A (en) | 2011-07-01 |
| BR112012007377A2 (pt) | 2016-04-19 |
| AU2010304779A1 (en) | 2012-04-12 |
| WO2011042836A1 (en) | 2011-04-14 |
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