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CN109537262A - 一种染色假发低损伤漂洗工艺 - Google Patents

一种染色假发低损伤漂洗工艺 Download PDF

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CN109537262A
CN109537262A CN201811228949.1A CN201811228949A CN109537262A CN 109537262 A CN109537262 A CN 109537262A CN 201811228949 A CN201811228949 A CN 201811228949A CN 109537262 A CN109537262 A CN 109537262A
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张建
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Taihe Ruisiyuan Hair Products Co Ltd
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Abstract

本发明公布了一种染色假发低损伤漂洗工艺，包括以下步骤：（1）向去离子水中加入无水乙醇等混合，将染色假发悬空至密闭老化室中，把混合溶液雾化后通入老化室老化处理，取出后紫外光照射，得老化假发；（2）向去离子水中加入草酸等混合，将老化假发浸入振荡处理，取出后木兰花碱溶液浸泡，得酸碱化假发；再悬挂于反应釜中通入臭氧升温处理，得氧化假发；（3）将假发浸入汽油清洗，得清洗假发；（4）将清洗假发浸入植物漂洗液置于变温箱变温处理，得漂洗假发；（5）使用50%的乙醇溶液对漂洗假发清洗，得复原假发。

Description

一种染色假发低损伤漂洗工艺
技术领域
本发明属于染色假发漂洗加工技术领域，具体涉及一种染色假发低损伤漂洗工艺。
背景技术
以真人发为原料的假发，由于其发质真实性和可变性，受到时尚界和影视界的欢迎，并且假发可根据不同场合和演艺需求进行染色处理，效果自然、美观，染色持久保持性好。真人发在染色后随着发质增长，会出现自然褪色，或采取裁剪等方式改变原有发质颜色，假发由于其不可再生性，虽然染色性持久，但是由于场合和需求不同，其并不能快速改变原有颜色，原有染色假发由于自然褪色和颜色不适应，就会造成废弃现象，造成资源和成本的浪费；并且现有技术对染色假发重新漂洗工艺，多使用强酸强碱、有毒有害溶剂等化学处理方法，可降低原有色泽，但是并不能完全消除原有颜色，对假发也造成不同程度的损伤，重新染色后上色率和纤维强度不同程度受到损伤。
发明内容
本发明的目的：原有染色假发由于自然褪色和颜色不适应，就会造成废弃现象，造成资源和成本的浪费；并且现有技术对染色假发重新漂洗工艺，多使用强酸强碱、有毒有害溶剂等化学处理方法，可降低原有色泽，但是并不能完全消除原有颜色，对假发也造成不同程度的损伤，重新染色后上色率和纤维强度不同程度受到损伤。为解决上述问题，本发明提供了一种染色假发低损伤漂洗工艺。
本发明是通过以下技术方案实现的：
一种染色假发低损伤漂洗工艺，包括以下步骤：
（1）老化处理：向去离子水中加入无水乙醇、甲苯和山茶精油搅拌混合，可对原染发剂中有机和无机成分进行不同程度的溶解，起到洗涤作用，混合溶液，将染色假发悬空至密闭老化室中，把混合溶液雾化后通入老化室升温至56-63℃，保持老化室湿度在90%-96%老化处理24-28h，可使原有染色剂成分快速出现老化与发质表面脱层，提高加速漂洗效率的效果，出后再将老化假发置于紫外光下照射1-2h，可加强染色剂老化速率，提高后续漂洗效率，老化假发；
（2）氧化：向去离子水中加入草酸、柠檬酸和乳酸搅拌混合，得混合酸液，将老化假发浸入混合酸液超声波振荡处理34-39min，即可起到对假发染色剂的脱洗作用，又可避免采用强酸对发质造成的损伤，出后再浸入质量浓度为1.7%-2.3%木兰花碱溶液中升温浸泡2-3h，可提高染发剂脱层效果，酸碱化假发；再将酸碱化假发悬挂于反应釜中通入其体积7%-9%的臭氧，升温处理1-2h，可对染色剂成分起到氧化脱层和漂白作用，促进染色剂成分与发质脱离，氧化假发；
（3）清洗：将假发浸入汽油中低速搅拌清洗17-22min，取出后使用清水洗净、烘干，得清洗假发；
（4）漂洗：将清洗假发浸入植物漂洗液中，置于变温箱中变温处理，先在63-67℃高温保存12-16min，再在-9℃--5℃低温保存10-13min，反复进行4-6次，具有对假发良好的漂洗效果，快速、洁净的脱洗假发原有染色剂成分，漂洗假发；
（5）醇洗：使用50%的乙醇溶液对漂洗假发清洗，得复原假发。
步骤（1）所述的混合溶液，其各配制成分质量计份为：去离子水100-120份、无水乙醇21-26份、甲苯9-13份、山茶精油5-9份。
步骤（2）所述的混合酸液，其各配制成分质量计份为：去离子水90-110份、草酸7-11份、柠檬酸5-8份、乳酸2-5份。
步骤（2）所述的超声波振荡，其频率为13-16Khz；所述的升温浸泡和升温处理，其温度为42-48℃。
步骤（3）所述的低速搅拌，其转速80-95r/min。
步骤（4）所述的植物漂洗液，其配制方法为：按质量计份称取商陆14-18份、番石榴10-13份、木瓜7-11份、蛇果叶5-8份、榆树叶3-7份、菠菜5-7份、三七叶3-6份、金银花1-2份，将上述原料粉碎碾磨，加入其总质量6-8倍的水蒸煮1-2h，再向其中加入水质量2%-3%的EM菌剂发酵2-3天，离心过滤得上清液，浓缩至原体积的1/4，得植物漂洗液。
本发明相比现有技术具有以下优点：老化处理，混合溶剂中采用去离子水、乙醇、甲苯和山茶精油作为溶剂，可对原染发剂中有机和无机成分进行不同程度的溶解，起到洗涤作用，采用高温高湿环境处理，可使原有染色剂成分快速出现老化与发质表面脱层，提高加速漂洗效率的效果；而采用紫外灯照射，可加强染色剂老化速率，提高后续漂洗效率。氧化，混合酸液中采用草酸、柠檬酸和乳酸混合对假发进行酸洗，即可起到对假发染色剂的脱洗作用，又可避免采用强酸对发质造成的损伤，同样采用木兰花碱对假发进行碱洗，具有较好的碱洗效果，可提高染发剂脱层效果，具有意想不到的效果；而使用低浓度臭氧对假发进行氧化处理，可对染色剂成分起到氧化脱层和漂白作用，促进染色剂成分与发质脱离，并且可避免高浓度臭氧对发质本身的损伤。漂洗，以商陆、番石榴等植物成分为提取原料，采用蒸煮、发酵和浓缩提取成分，所得植物漂洗液具有对假发良好的漂洗效果，快速、洁净的脱洗假发原有染色剂成分，具有意想不到的漂洗效果，即环保又降低了化工试剂对假发发质的损伤，并且漂洗后的假发上色率高纤维强度影响不大。
具体实施方式
实施例1：
一种染色假发低损伤漂洗工艺，包括以下步骤：
（1）老化处理：向去离子水中加入无水乙醇、甲苯和山茶精油搅拌混合，可对原染发剂中有机和无机成分进行不同程度的溶解，起到洗涤作用，混合溶液，将染色假发悬空至密闭老化室中，把混合溶液雾化后通入老化室升温至57℃，保持老化室湿度在91%老化处理25h，可使原有染色剂成分快速出现老化与发质表面脱层，提高加速漂洗效率的效果，出后再将老化假发置于紫外光下照射1.5h，可加强染色剂老化速率，提高后续漂洗效率，老化假发；
（2）氧化：向去离子水中加入草酸、柠檬酸和乳酸搅拌混合，得混合酸液，将老化假发浸入混合酸液超声波振荡处理35min，即可起到对假发染色剂的脱洗作用，又可避免采用强酸对发质造成的损伤，出后再浸入质量浓度为1.8%木兰花碱溶液中升温浸泡2.5h，可提高染发剂脱层效果，酸碱化假发；再将酸碱化假发悬挂于反应釜中通入其体积7.1%的臭氧，升温处理1.5h，可对染色剂成分起到氧化脱层和漂白作用，促进染色剂成分与发质脱离，氧化假发；
（3）清洗：将假发浸入汽油中低速搅拌清洗18min，取出后使用清水洗净、烘干，得清洗假发；
（4）漂洗：将清洗假发浸入植物漂洗液中，置于变温箱中变温处理，先在64℃高温保存13min，再在-6℃低温保存11min，反复进行4次，具有对假发良好的漂洗效果，快速、洁净的脱洗假发原有染色剂成分，漂洗假发；
（5）醇洗：使用50%的乙醇溶液对漂洗假发清洗，得复原假发。
步骤（1）所述的混合溶液，其各配制成分质量计份为：去离子水102份、无水乙醇22份、甲苯10份、山茶精油6份。
步骤（2）所述的混合酸液，其各配制成分质量计份为：去离子水91份、草酸8份、柠檬酸6份、乳酸3份。
步骤（2）所述的超声波振荡，其频率为14Khz；所述的升温浸泡和升温处理，其温度为43℃。
步骤（3）所述的低速搅拌，其转速83r/min。
步骤（4）所述的植物漂洗液，其配制方法为：按质量计份称取商陆15份、番石榴11份、木瓜8份、蛇果叶6份、榆树叶4份、菠菜5.2份、三七叶4份、金银花1.1份，将上述原料粉碎碾磨，加入其总质量6.5倍的水蒸煮1.5h，再向其中加入水质量2.1%的EM菌剂发酵2天，离心过滤得上清液，浓缩至原体积的1/4，得植物漂洗液。
实施例2：
一种染色假发低损伤漂洗工艺，包括以下步骤：
（1）老化处理：向去离子水中加入无水乙醇、甲苯和山茶精油搅拌混合，可对原染发剂中有机和无机成分进行不同程度的溶解，起到洗涤作用，混合溶液，将染色假发悬空至密闭老化室中，把混合溶液雾化后通入老化室升温至62℃，保持老化室湿度在95%老化处理27h，可使原有染色剂成分快速出现老化与发质表面脱层，提高加速漂洗效率的效果，出后再将老化假发置于紫外光下照射2h，可加强染色剂老化速率，提高后续漂洗效率，老化假发；
（2）氧化：向去离子水中加入草酸、柠檬酸和乳酸搅拌混合，得混合酸液，将老化假发浸入混合酸液超声波振荡处理38min，即可起到对假发染色剂的脱洗作用，又可避免采用强酸对发质造成的损伤，出后再浸入质量浓度为2.2%木兰花碱溶液中升温浸泡3h，可提高染发剂脱层效果，酸碱化假发；再将酸碱化假发悬挂于反应釜中通入其体积8.7%的臭氧，升温处理2h，可对染色剂成分起到氧化脱层和漂白作用，促进染色剂成分与发质脱离，氧化假发；
（3）清洗：将假发浸入汽油中低速搅拌清洗21min，取出后使用清水洗净、烘干，得清洗假发；
（4）漂洗：将清洗假发浸入植物漂洗液中，置于变温箱中变温处理，先在66℃高温保存15min，再在-8℃低温保存12min，反复进行6次，具有对假发良好的漂洗效果，快速、洁净的脱洗假发原有染色剂成分，漂洗假发；
（5）醇洗：使用50%的乙醇溶液对漂洗假发清洗，得复原假发。
步骤（1）所述的混合溶液，其各配制成分质量计份为：去离子水109份、无水乙醇25份、甲苯12份、山茶精油8份。
步骤（2）所述的混合酸液，其各配制成分质量计份为：去离子水108份、草酸10份、柠檬酸7份、乳酸4份。
步骤（2）所述的超声波振荡，其频率为15Khz；所述的升温浸泡和升温处理，其温度为47℃。
步骤（3）所述的低速搅拌，其转速94r/min。
步骤（4）所述的植物漂洗液，其配制方法为：按质量计份称取商陆17份、番石榴12份、木瓜10份、蛇果叶7份、榆树叶6份、菠菜6.7份、三七叶5.6份、金银花1.8份，将上述原料粉碎碾磨，加入其总质量7.5倍的水蒸煮2h，再向其中加入水质量2.9%的EM菌剂发酵3天，离心过滤得上清液，浓缩至原体积的1/4，得植物漂洗液。
对比1：
本对比1与实施例1比较，未使用步骤（1）中老化处理方法，其他步骤与实施例1相同。
对比2：
本对比2与实施例2比较，未使用步骤（2）中混合酸液和木兰花碱，其他步骤与实施例2相同。
对比3：
本对比3与实施例1比较，未使用步骤（4）中植物漂洗液，其他步骤与实施例1相同。
对比4：
本对比4与实施例2比较，未使用步骤（4）中变温处理，其他步骤与实施例2相同。
对照组：对照组采用传统强酸强碱等试剂对染色假发漂洗。
对实施例1、实施例2、对比1、对比2、对比3、对比4和对照组实验所得假发，统计各假发脱色率、纤维强度（原假发纤维强度为4.37N/dtex）和重新染色后上色率进行比较。
实验数据：
项目 脱色率% 纤维强度N/dtex 上色率%
实施例1 99.87 4.21 97.3
实施例2 99.75 4.15 97.8
对比1 94.64 3.87 94.2
对比2 92.34 3.69 95.5
对比3 86.35 3.49 91.9
对比4 94.39 3.8 96.1
对照组 74.25 3.14 89.2
综合结果：本发明方法对染色假发漂洗工艺，与对照组比较，脱色率提高了25.62%，纤维强度较原假发发质降低0.16N/dtex，较对照组提高1.07N/dtex，重新染色上色率提高8.6%；具有漂洗效果、方法简单、安全环保，并且对原假发发质损伤程度低的特点。

Claims (6)

1.一种染色假发低损伤漂洗工艺，其特征在于，包括以下步骤：
（1）老化处理：向去离子水中加入无水乙醇、甲苯和山茶精油搅拌混合，得混合溶液，将染色假发悬空至密闭老化室中，把混合溶液雾化后通入老化室升温至56-63℃，保持老化室湿度在90%-96%老化处理24-28h，取出后再将老化假发置于紫外光下照射1-2h，得老化假发；
（2）氧化：向去离子水中加入草酸、柠檬酸和乳酸搅拌混合，得混合酸液，将老化假发浸入混合酸液超声波振荡处理34-39min，取出后再浸入质量浓度为1.7%-2.3%木兰花碱溶液中升温浸泡2-3h，得酸碱化假发；再将酸碱化假发悬挂于反应釜中通入其体积7%-9%的臭氧，升温处理1-2h，得氧化假发；
（3）清洗：将假发浸入汽油中低速搅拌清洗17-22min，取出后使用清水洗净、烘干，得清洗假发；
（4）漂洗：将清洗假发浸入植物漂洗液中，置于变温箱中变温处理，先在63-67℃高温保存12-16min，再在-9℃--5℃低温保存10-13min，反复进行4-6次，得漂洗假发；
（5）醇洗：使用50%的乙醇溶液对漂洗假发清洗，得复原假发。
2.如权利要求1所述的染色假发低损伤漂洗工艺，其特征在于，步骤（1）所述的混合溶液，其各配制成分质量计份为：去离子水100-120份、无水乙醇21-26份、甲苯9-13份、山茶精油5-9份。
3.如权利要求1所述的染色假发低损伤漂洗工艺，其特征在于，步骤（2）所述的混合酸液，其各配制成分质量计份为：去离子水90-110份、草酸7-11份、柠檬酸5-8份、乳酸2-5份。
4.如权利要求1所述的染色假发低损伤漂洗工艺，其特征在于，步骤（2）所述的超声波振荡，其频率为13-16Khz；所述的升温浸泡和升温处理，其温度为42-48℃。
5.如权利要求1所述的染色假发低损伤漂洗工艺，其特征在于，步骤（3）所述的低速搅拌，其转速80-95r/min。
6.如权利要求1所述的染色假发低损伤漂洗工艺，其特征在于，步骤（4）所述的植物漂洗液，其配制方法为：按质量计份称取商陆14-18份、番石榴10-13份、木瓜7-11份、蛇果叶5-8份、榆树叶3-7份、菠菜5-7份、三七叶3-6份、金银花1-2份，将上述原料粉碎碾磨，加入其总质量6-8倍的水蒸煮1-2h，再向其中加入水质量2%-3%的EM菌剂发酵2-3天，离心过滤得上清液，浓缩至原体积的1/4，得植物漂洗液。
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